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Articles

Simultaneous determination of three pesticides and their metabolites in unprocessed foods using ultraperformance liquid chromatography-tandem mass spectrometry

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Pages 273-281 | Received 10 Jul 2017, Accepted 19 Sep 2017, Published online: 01 Dec 2017

References

  • Cheng Y, Dong F, Liu X, Xu J, Meng W, Liu N, Chen Z, Tao Y, Zheng Y. 2014. Simultaneous determination of fipronil and its major metabolites in corn and soil by ultra-performance liquid chromatography-tandem mass spectrometry. Anal Methods. 6:1788–1795.
  • Di Muccio A, Fidente P, Barbini DA, Dommarco R, Seccia S, Morrica P. 2006. Application of solid-phase extraction and liquid chromatography–mass spectrometry to the determination of neonicotinoid pesticide residues in fruit and vegetables. J Chromatogr A. 1108:1–6.
  • Dong F, Chen X, Liu X, Xu J, Li Y, Shan W, Zheng Y. 2012b. Simultaneous determination of five pyrazole fungicides in cereals, vegetables and fruits using liquid chromatography/tandem mass spectrometry. J Chromatogr A. 1262:98–106.
  • Duhan A, Kumari B, Duhan S. 2015. Determination of residues of fipronil and its metabolites in cauliflower by using gas chromatography-tandem mass spectrometry. Bull Environ Contam Toxicol. 94:260–266.
  • Filho NF, Nascimento CA, Faria EO, Cruvinel AR, Oliveira JM. 2012. Within-laboratory validation of a multiresidue method for the analysis of 98 pesticides in mango by liquid chromatography-tandem mass spectrometry. Food Addit Contamin A. 29:641–656.
  • Golge O, Kabak B. 2015. Evaluation of QuEChERS sample preparation and liquid chromatography-triple-quadrupole mass spectrometry method for the determination of 109 pesticide residues in tomatoes. Food Chem. 176:319–332.
  • Gunasekara AS, Truong T, Goh KS, Spurlock F, Tjeerdema RS. 2007. Environmental fate and toxicology of fipronil. J Pestic Sci. 32:189–199.
  • Hanot V, Goscinny S, Deridder M. 2015. A simple multi-residue method for the determination of pesticides in fruits and vegetables using a methanolic extraction and ultra-high-performance liquid chromatography-tandem mass spectrometry: optimization and extension of scope. J Chromatogr A. 1384:53–66.
  • Kadar A, Faucon J-P. 2006. Determination of traces of fipronil and its metabolites in pollen by liquid chromatography with electrospray ionization− tandem mass spectrometry. J Agric Food Chem. 54:9741–9746.
  • Kaur R, Mandal K, Kumar R, Singh B. 2015. Analytical method for determination of fipronil and its metabolites in vegetables using the QuEChERS method and gas chromatography/mass spectrometry. Journal of Aoac International. 98:464. doi: 10.5740/jaoacint.13-066
  • Kiljanek T, Niewiadowska A, Semeniuk S, Gaweł M, Borzęcka M, Posyniak A. 2016. Multi-residue method for the determination of pesticides and pesticide metabolites in honeybees by liquid and gas chromatography coupled with tandem mass spectrometry—honeybee poisoning incidents. J Chromatogr A. 1435:100–114.
  • Lehotay SJ, Mastovská K, Yun SJ. 2005. Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes. J AOAC Int. 88:630–638.
  • Lesueur C, Knittl P, Gartner M, Mentler A, Fuerhacker M. 2008. Analysis of 140 pesticides from conventional farming foodstuff samples after extraction with the modified QuECheRS method. Food Control. 19:906–914.
  • Li M, Li P, Wang L, Feng M, Han L. 2015. Determination and dissipation of fipronil and its metabolites in peanut and soil. J Agric Food Chem. 63:4435–4443.
  • Li M, Liu X, Dong F, Xu J, Kong Z, Li Y, Zheng Y. 2013. Simultaneous determination of cyflumetofen and its main metabolite residues in samples of plant and animal origin using multi-walled carbon nanotubes in dispersive solid-phase extraction and ultrahigh performance liquid chromatography–tandem mass spectrometry. J Chromatogr A. 1300:95–103.
  • Liu X, Xu J, Dong F, Li Y, Song W, Zheng Y. 2011. Residue analysis of four diacylhydrazine insecticides in fruits and vegetables by Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method using ultra-performance liquid chromatography coupled to tandem mass spectrometry. Anal Bioanal Chem. 401:1051–1058.
  • Matuszewski BK, Constanzer MLC, Chavezeng CM. 2003. Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLC−MS/MS. Anal Chem. 75:3019–3030.
  • Morrissey CA, Mineau P, Devries JH, Sanchez-Bayo F, Liess M, Cavallaro MC, Liber K. 2015. Neonicotinoid contamination of global surface waters and associated risk to aquatic invertebrates: a review. Environ Int. 74:291–303.
  • Paramasivam M, Chandrasekaran S. 2013. Determination of fipronil and its major metabolites in vegetables, fruit and soil using QuEChERS and gas chromatography-mass spectrometry. Int J Environ Anal Chem. 93:1203–1211.
  • Payá P, Anastassiades M, Mack D, Sigalova I, Tasdelen B, Oliva J, Barba A. 2007. Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection. Anal Bioanal Chem. 389:1697–1714.
  • Peng X-T, Li Y-N, Xia H, Peng L-J, Feng Y-Q. 2016. Rapid and sensitive detection of fipronil and its metabolites in edible oils by solid-phase extraction based on humic acid bonded silica combined with gas chromatography with electron capture detection. J Sep Sci. 39:2196–2203.
  • Rahman MM, Farha W, Abd El-Aty AM, Kabir MH, Im SJ, Jung D-I, Choi J-H, Kim S-W, Son YW, Kwon C-H, et al. 2015. Dynamic behaviour and residual pattern of thiamethoxam and its metabolite clothianidin in Swiss chard using liquid chromatography–tandem mass spectrometry. Food Chem. 174:248–255.
  • Tomlin CDS, Tomlin CDS. 2009. The pesticide manual: a world compendium. British Crop Protection Council.
  • van der Sluijs JP, Simon-Delso N, Goulson D, Maxim L, Bonmatin J-M, Belzunces LP. 2013. Neonicotinoids, bee disorders and the sustainability of pollinator services. Curr Opin Environ Sustain. 5:293–305.
  • Wang T, Hu J, Liu C. 2014. Simultaneous determination of insecticide fipronil and its metabolites in maize and soil by gas chromatography with electron capture detection. Environ Monit Assess. 186:2767–2774.
  • Wu X, Xu J, Dong F, Liu X, Li Y, Zheng Y. 2014. Simultaneous determination of oxathiapiprolin and two metabolites in fruits, vegetables and cereal using a modified quick, easy, cheap, effective, rugged, and safe method and liquid chromatography coupled to tandem mass spectrometry. J Chromatogr A. 1329:30–37.
  • Wu X, Yu Y, Xu J, Dong F, Liu X, Du P, Wei D, Zheng Y. 2017. Residue analysis and persistence evaluation of fipronil and its metabolites in cotton using high-performance liquid chromatography-tandem mass spectrometry. PloSone. 12:e0173690.
  • Zhang H, Wang J, Li L, Wang Y. 2017. Determination of 103 pesticides and their main metabolites in animal origin food by QuEChERS and liquid chromatography–tandem mass spectrometry. Food Anal Methods. 10:1826–1843.
  • Zhang M, Bian K, Zhou T, Song X, Liu Q, Meng C, He L. 2016. Determination of residual fipronil in chicken egg and muscle by LC–MS/MS. J Chromatogr B. 1014:31–36.

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