369
Views
4
CrossRef citations to date
0
Altmetric
Articles

Uncertainty of pesticide residue concentration determined from ordinary and weighted linear regression curve

, &
Pages 1324-1339 | Received 03 Jan 2018, Accepted 25 Feb 2018, Published online: 28 Mar 2018

References

  • Ambrus A. 2009. Estimation of sampling uncertainty for determination of pesticide residues in plant commodities. J Environ Sci Health B. 44(7):627–639.
  • Ambrus A, Jarju O, Soboleva E, Turcu MS 2002. Uncertainty of analyte concentration predicted by GLC and HPLC analysis. Paper presented at: 10th IUPAC Congress on Pesticide Chemistry; Basel, Switzerland.
  • Ambrus A, Zentai A, Sali J, Ficzere I. 2011. Hidden contributors to uncertainty and accuracy of results of residue analysis. Accred Qual Assur. 16:3–11.
  • Aysal P, Ambrus A, Lehotay SJ, Cannavan A. 2007. Validation of an efficient method for the determination of pesticide residues in fruits and vegetables using ethyl acetate for extraction. J Environ Sci Health. B. 42(5):481–490.
  • Barwick V. 2003. Preparation of calibration curve: a guide to best practice. Teddington, UK: National Measurement System: Valid Analytical Programme, LGC Publications, LGC/VAM/2003/032.
  • Chen S, Yu X, He X, Xie D, Fan Y, Peng J. 2009. Simplified pesticide multiresidues analysis in fish by low-temperature cleanup and solid phase extraction coupled with gas chromatography/mass spectrometry. Food Chem. 113(4):1297–1300.
  • [CAC] Codex Alimentarious Commission. 2010. Analysis of pesticide residues: portion of commodities to which Codex MRLS apply and which is analyzed. CAC/GL 41-1993. [accessed 2017 Dec 16]. http://www.codexalimentarius.org/standards/list-of-standards/en/
  • [CAC] Codex Alimentarius Commission. 2003. Guidelines on good laboratory practice in residue analysis. CAC/GL 40-1993, Revision 1. 1993. [accessed 2017 Feb 16]. http://www.codexalimentarius.org/standards/list-of-standards/en/
  • Ellison SRL, Williams A. 2012. Quantifying uncertainty in analytical measurement. 3rd ed. Eurachem/CITAC Guide. [accessed 2017 Dec 16]. http://www.eurachem.org
  • Esturk O, Yakar Y, Ayhan Z. 2014. Pesticide residue analysis in parsley, lettuce and spinach by LC-MS/MS. J Food Sci Tech. 51(3):458–466.
  • Georgakopoulos P, Mylona A, Athanasopoulos P, Drosinos EH, Skandamis PN. 2009. Evaluation of cost-effective methods in the pesticide residue analysis of non-fatty baby foods. Food Chem. 115(3):1164–1169.
  • Hernández-Borges J, Cabrera JC, Rodriguez-Delgado MA, Hernandez-Suarez EM, Sauco VG. 2009. Analysis of pesticide residues in bananas harvested in the Canary Islands (Spain). Food Chem. 113(1):313–319.
  • [ISO] International Organization for Standardization. 1996. ISO 11095:1996, Linear calibration using reference materials. Geneva: ISO.
  • Jian Wang J, Cheung W, Daniel Leung D. 2014. Determination of pesticide residue transfer rates (percent) from dried tea leaves to brewed tea. J Agric Food Chem. 62(4):966–983.
  • [JCGM] Joint Committee for Guides in Metrology. 2012. International vocabulary of metrology—basic and general concepts and associated terms (VIM). JCGM. 200:2012.
  • Konieczka P, Namie´Snik J. 2010. Estimating uncertainty in analytical procedures based on chromatographic techniques. J Chrom A. 1217(6):882–891.
  • Lehotay SJ, Mastovska K, Lightfield AR, Gates RA. 2010. Multianalyst, multi-matrix performance of the QuEChERS approach for pesticide residues in foods and feeds using HPLC/MS/MS analysis with different calibration techniques. J AOAC Int. 93(2):355–367.
  • Loco JV, Elskens M, Croux C, Beernaert H. 2002. Linearity of calibration curves: use and misuse of the correlation coefficient. Accred Qual Assur. 7(7):281–285.
  • Madureira FD, Oliveira FAS, Souza WR, Pontelo AP, Oliveira MLG, Silva G. 2012. A multi-residue method for the determination of 90 pesticides in matrices with a high water content by LC–MS/MS without clean-up. Food Addit & Contam. Part A. 29(4):665–678.
  • Malhat FM, Haggaga MN, Loutfyb NM, Osmanb MAM, Ahmedb MT. 2015. Residues of organochlorine and synthetic pyrethroid pesticides in honey, an indicator of ambient environment, a pilot study. Chemosphere. 120:457–461.
  • Miao Q, Kong W, Yang S, Yang M. 2013. Rapid analysis of multi-pesticide residues in lotus seeds by a modified QuEChERS-based extraction and GC–ECD. Chemosphere. 91:955–962.
  • Miller JN, Ambrus A. 2000. Manual on basic statistics. Training course notes. Vienna: FAO/IAEA Training and Reference Centre for Food and Pesticide Control.
  • Nantia EA, Moreno-González D, Manfo FPT, Gámiz-Gracia L, García-Campaña AM. 2017. QuEChERS-based method for the determination of carbamate residues in aromatic herbs by UHPLC-MS/MS. Food Chem. 216(1):334–341.
  • Núñez O, Ayala HG, Ferrer I, Moyano E, Galceran MT. 2012. Strategies for the multi-residue analysis of 100 pesticides by liquid chromatography-triple quadrupole mass spectrometry. J Chromatogr A. 1249:164–180.
  • Oliveira MLG, Madureira FD, Oliveira FAS, Pontelo AP, Silva G, Oliveira R. 2012. A multi-residue method for the determination of pesticides in high water content matrices by gas chromatography-single quadrupole mass spectrometry with electron ionisation (EI-GC/MS). Food Addit Contam. Part A. 29(4):657–664.
  • Raposo F. 2016. Evaluation of analytical calibration based on least-squares linear regression for instrumental techniques: a tutorial review. Trends Anal Chem. 77:167–185.
  • [SANTE] European Commision (EC) Director General for Food and Health Safety. 2017. Guidance document on analytical quality control and validation procedures for pesticide residues analysis in food and feed, Document No: SANTE 11813/2017. [accessed 2017 Dec 28]. https://ec.europa.eu/food/sites/food/files/plant/docs/pesticides_mrl_guidelines_wrkdoc_2017-11813.pdf
  • Schenk FJ, Wong JW. 2007. Determination of pesticides in food and vegetal origin. In: Tadeo JL, editor. Analysis of pesticides in food and environmental samples. New York (NY): CRC Press; p. 152–166.
  • Soboleva E, Ambrus A. 2004. Application of system suitability tests for quality assurance and performance optimisation of a gas chromatographic a system for pesticide residue analysis. J of Chromatography A. 1027(1–2):55–65.
  • Soboleva E, Jarju O, Ambrus A. 2004. Estimation of uncertainty of analytical results based on multiple peaks. J Chromatogr A. 41(5):161–166.
  • Štepán R, Hajšlová J, Kocourek V, Tichá J. 2004. Uncertainties of gas chromatographic measurement of troublesome pesticide residues in apples employing conventional and mass spectrometric detectors. Anal Chim Acta. 520:245–255.
  • Thompson M. 2005. Is my calibration linear? London: The Royal Society of Chemistry. Analytical Methods Committee AMCTB No. 3.
  • Yolci Omeroglu P, Ambrus A, Boyacioglu D. 2013a. Estimation of the uncertainties of extraction and clean-up steps in pesticide residue analysis of plant commodities. Food Addit Contam. Part A. 30(2):308–320.
  • Yolci Omeroglu P, Ambrus A, Boyacioglu D, Mazjik ES. 2013b. Uncertainty of sample size reduction step in pesticide residue analysis of large size crops. Food Addit Contam Part A. 30(1):116–126.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.