Method development and validation for low-level propineb and propylenethiourea analysis in baby food, infant formula and related matrices using liquid chromatography-tandem mass spectrometry

References

• [EC] European Commission. 2005. Commission Regulation (EC) no 396/2005 of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC. Off J Eur Union. L.70:1–16.
   Google Scholar
• [EC] European Commission. 2006a. Commission Directive 2006/141/EC of 22 December 2006 on infant formulae and follow-on formulae and amending directive 1999/21/EC. Off J Eur Union. L.401:1–33.
   Google Scholar
• [EC] European Commission. 2006b. Commission Directive 2006/125/EC of 5 December 2006 on processed cereal-based foods and baby foods for infants and young children. Off J Eur Union. 2006(L339):16–35.
   Google Scholar
• [EC] European Commission. 2017a. Commission Regulation (EU) 2017/171 of 30 January 2017 amending Annexes II, III and IV to Regulation (EC) No 396/2005 of the European parliament and of the council as regards maximum residue levels for aminopyralid, azoxystrobin, cyantraniliprole, cyflufenamid, cyproconazole, diethofencarb, dithiocarbamates, fluazifop-P, fluopyram, haloxyfop, isofetamid, metalaxyl, prohexadione, propaquizafop, pyrimethanil, Trichoderma atroviride strain SC1 and zoxamide in or on certain products. Off J Eur Union. L.70:45–111.
   Google Scholar
• [EC] European Commission. 2017b. Guidance document on analytical quality control and method validation procedures for pesticides residues analysis in food and feed. SANTE/11813/2017. [Internet]; [accessed 2018 Jun 1]. https://ec.europa.eu/food/sites/food/files/plant/docs/pesticides_mrl_guidelines_wrkdoc_2017-11813.pdf
   Google Scholar
• [EU] European Union. EU pesticide database. [Internet]; [accessed 2018 Jun 1]. http://ec.europa.eu/food/plant/pesticides/eu-pesticides-database/public/?event=homepage&language=EN
   Google Scholar
• [WHO] World Health Organization. 1988. Environmental health criteria 78. Dithiocarbamate Pesticides, Ethylenethiourea and Propylenethiourea: a general introduction. Geneva: WHO. ISBN 92 4 154278 0
   Google Scholar
• [WHO] World Health Organization. 1993. Pesticides residues in food, evaluations part II-Toxicology, Switzerland. [Internet]; [accessed 2018 Jun 1]. http://www.inchem.org/documents/jmpr/jmpmono/v93pr01.htm
   Google Scholar
• Anastassiades M, Kolberg DI, Benkenstein A, Eichhorn E, Zechmann S, Mack D, Wildgrube C, Sigalov I, Dörk D, Barth A 2017. Quick method for the analysis of numerous highly polar pesticides in foods of plant origin via LC-MS/MS involving simultaneous extraction with methanol (QuPPe-Method). [Internet]; [accessed 2018 Jun 1]. http://www.eurl-pesticides.eu/docs/public/tmplt_article.asp?CntID=887&LabID=200&Lang=EN
   Google Scholar
• Blasco C, Font G, Picó Y. 2004. Determination of dithiocarbamates and metabolites in plants by liquid chromatography-mass spectrometry. J Chromatogr A. 1028:267–276.
   PubMed Web of Science ®Google Scholar
• Bonnechere A, Hanot V, Van Loco J. 2011. A rapid and environmental friendly determination of the dithiocarbamate metabolites ethylenethiourea and propylenethiourea in fruit and vegetables by ultra high performance liquid chromatography tandem mass spectrometry. J Chromatogr A. 1218:4627–4631.
   PubMed Web of Science ®Google Scholar
• Crnogorac G, Schmauder S, Schwack W. 2008. Trace analysis of dithiocarbamate fungicide residues on fruits and vegetables by hydrophilic interaction liquid chromatography/tandem mass spectrometry. Rapid Commun Mass Spectrom. 22:2539–2546.
   PubMed Web of Science ®Google Scholar
• Crnogorac G, Schwack W. 2009. Residue analysis of dithiocarbamate fungicides. Trends Anal Chem. 28:40–50.
   Web of Science ®Google Scholar
• Danezis GP, Anagnostopoulos CJ, Liapis K, Koupparis MA. 2016. Multi-residue analysis of pesticides, plant hormones, veterinary drugs and mycotoxins using HILIC chromatography–MS/MS in various food matrices. Anal Chim Acta. 942:121–138.
   PubMed Web of Science ®Google Scholar
• Dhoot JS, Delrosario AR, Tampin BR. 1993. Simultaneous determination and confirmation of sodium N-methyldithiocarbamate (metham-sodium(R)) and methyl isothiocyanate in water by high-performance liquid-chromatography with diode-array detection. Int J Environ Anal Chem. 53:165–171.
   Web of Science ®Google Scholar
• Hayama T, Takada M. 2008. Simple and rapid method for the determination of ethylenebisdithiocarbamate fungicides in fruits and vegetables using liquid chromatography with tandem mass spectrometry. Anal Bioanal Chem. 392:969–976.
   PubMed Web of Science ®Google Scholar
• Kobayashi H, Hishida M, Matano O, Goto S. 1992. Effect of cysteine on the stability of ethylenethiourea and ethylenebis(dithiocarbamate) in crops during storage and/or analysis. J Agric Food Chem. 40:76–80.
   Web of Science ®Google Scholar
• Mastovska K, Zulkoski J, Deal E, Vaclavik L, Koesukwiwat U, Halbardier JF, Zweigenbaum J, Glauner T 2017. Improved LC-MS/MS pesticide residue analysis using triggered MRM and on-line dilution. Application Note 5991-7193EN, Agilent Technologies.
   Google Scholar
• Nakamura M, Noda S, Kosugi M, Ishiduka N, Mizukoshi K, Taniguchi M, Nemoto S. 2010. Determination of dithiocarbamates and milneb residues in foods by gas chromatography-mass spectrometry. Food Hyg Saf Sc. 51:213–219.
   PubMed Web of Science ®Google Scholar
• Nakazawa H, Tsuda Y, Ito K, Yoshimura Y, Kubo H, Homma H. 2004. Determination of dithiocarbamate fungicides by reversed‐phase ion‐pair liquid chromatography with chemiluminescence detection. J Liq Chromatogr Relat Technol. 27:705–713.
   Web of Science ®Google Scholar
• Ripolles C, Sancho JV, Lopez FJ, Hernandez F. 2012. Liquid chromatography coupled to tandem mass spectrometry for the residue determination of ethylenethiourea (ETU) and propylenethiourea (PTU) in water. J Chromatogr A. 1243:53–61.
   PubMed Web of Science ®Google Scholar
• Startin JR, Hird SJ, Sykes MD. 2005. Determination of ethylenethiourea (ETU) and propylenethiourea (PTU) in foods by high performance liquid chromatography–atmospheric pressure chemical ionisation–medium-resolution mass spectrometry. Food Addit Contam A. 22:245–250.
   PubMed Web of Science ®Google Scholar
• Tolgyesi L, Kele P, Torkos K. 2010. Determination of propylenethiourea, the main metabolite of propineb, in tomato by HILIC-MS. Chromatographia. 71:S75–S80.
   Web of Science ®Google Scholar
• Van Lishaut H, Schwack W. 2000. Selective trace determination of dithiocarbamate fungicides in fruits and vegetables by reversed-phase ion-pair liquid chromatography with ultraviolet and electrochemical detection. J AOAC Int. 83:720–727.
   PubMed Web of Science ®Google Scholar
• Zhou L, Xu J, Luan L, Ma J, Gong Y, Qin D, Pan C. 2013. Optimization and validation of a method based on derivatization with methylating agent followed by HPLC–DAD for determining dithiocarbamates residues. Acta Chromatogr. 25:613–625.
   Web of Science ®Google Scholar