Method validation, storage stability and field trial for residues of florasulam and pyroxsulam in cereal by liquid chromatography with tandem mass spectrometry

References

• Afridi IA, Parveen Z, Masud SZ. 2001. Stability of organophosphate and pyrethroid pesticides on wheat in storage. J Stored Prod Res. 37(2):199–204.
   PubMed Web of Science ®Google Scholar
• Anastassiades M, Lehotay SJ, Stajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and Bdispersive solid-phase extraction for the determination of pesticide residues in produce. J AOAC Int. 86(2):412–431.
   PubMed Web of Science ®Google Scholar
• Beddington J. 2009. Food security: contributions from science to a new and greener revolution. Philos Trans R Soc B: Biol Sci. 365(1537):61–71.
   Web of Science ®Google Scholar
• Casado J, Santillo D, Johnston P. 2018. Multi-residue analysis of pesticides in surface water by liquid chromatography quadrupole-Orbitrap high resolution tandem mass spectrometry. Anal Chim Acta. 1024:1–17.
   PubMed Web of Science ®Google Scholar
• DeBoer GJ, Thornburgh S, Ehr RJ. 2006. Uptake, translocation and metabolism of the herbicide florasulam in wheat and broadleaf weeds. Pest Manag Sci. 62(4):316–324.
   PubMed Web of Science ®Google Scholar
• [FAO] Food and Agriculture Organization of the United Nations. 2016. Manual on the submission and evaluation of pesticide residues data for the estimation of maximum residue limits in food and feed. Vols. 33–36. Rome (Italy): FAO.
   Google Scholar
• Dong B, Qian W, Hu J. 2015. Dissipation kinetics and residues of florasulam and tribenuron-methyl in wheat ecosystem. Chemosphere. 120:486–491.
   PubMed Web of Science ®Google Scholar
• [DAS] Dow AgroSciences. 2007. Pyroxsulam. Indianapolis (IN): DAS. Technical Bulletin Y45-356-001 (09/07), BOD 010–80111.
   Google Scholar
• Georgakopoulos P, Zachari R, Mataragas M, Athanasopoulos P, Drosinos EH, Skandamis PN. 2011. Optimisation of octadecyl (C18) sorbent amount in QuEChERS analytical method for the accurate organophosphorus pesticide residues determination in low-fatty baby foods with response surface methodology. Food Chem. 128(2):536–542.
   PubMed Web of Science ®Google Scholar
• Ghosh B, Bhattacharyya A, Mukherjee S, Das S, Bhattacharyya A. 2014. .Residual fate and persistence behaviour of a mixed herbicide formulation (pyroxsulam 4.5% OD + sulfosulfuron 75% WDG) in wheat plant and field soil. J Crop Weed. 10:407–413.
   Google Scholar
• Jabran K, Mahajan G, Sardana V, Chauhan BS. 2015. Allelopathy for weed control in agricultural systems. Crop Prot. 72:57–65.
   Web of Science ®Google Scholar
• Jackson R, Ghosh D, Paterson G. 2000. The soil degradation of the herbicide florasulam. Pest Manag Sci. 56(12):11.
   Web of Science ®Google Scholar
• Johnson TC, Vanheertum JC, Ouse DG, Pobanz MA, Arndt KE, Walker DK, Int PCT. 2002. N- (5, 7-dimethoxy [1, 2, 4] triazolo [1, 5-a] pyrimidin-2-yl) arylsulfonamide compounds and their use as herbicides. Appl. WO 2002/036595.
   Google Scholar
• Lehotay SJ, de Kok A, Hiemstra M, Bodegraven P. 2005. Validation of a fast and easy method for the determination of 229 pesticide residues in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection. J AOAC Int. 88:595–614.
   PubMed Web of Science ®Google Scholar
• Li Z, Guan W, Hong H, Ye Y, Ma Y. 2013. Determination and study on residue and dissipation of florasulam in wheat and soil under field conditions. Bull Environ Contam Toxicol. 90(3):280–284.
   PubMed Web of Science ®Google Scholar
• Liu X, Xu J, Li Y, Dong F, Li J, Song W, Zheng Y. 2011. Rapid residue analysis of four triazolopyrimidine herbicides in soil, water, and wheat by ultra-performance liquid chromatography coupled to tandem mass spectrometry. Anal Bioanal Chem. 399(7):2539–2547.
   PubMed Web of Science ®Google Scholar
• Lozowicka B, Kaczynski P, Paritova АЕ, Kuzembekova GB, Abzhalieva AB, Sarsembayeva NB, Alihan K. 2014. Pesticide residues in grain from Kazakhstan and potential health risks associated with exposure to detected pesticides. Food Chem Toxicol. 64:238–248.
   PubMed Web of Science ®Google Scholar
• Matuszewski BK, Constanzer ML, Chavez-Eng CM. 2003. Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLC−MS/MS. Anal Chem. 75(13):3019–3030.
   PubMed Web of Science ®Google Scholar
• Noble RM, Hamilton DJ, Osborne WJ. 1982. Stability of pyrethroids on wheat in storage. Pestic Sci. 13(3):246–252.
   Google Scholar
• Rodehutscord M, Rückert C, Maurer HP, Schenkel H, Schipprack W, Bach Knudsen KE, Mosenthin R. 2016. Variation in chemical composition and physical characteristics of cereal grains from different genotypes. Arch Anim Nutr. 70(2):87–107.
   PubMed Web of Science ®Google Scholar
• Su W, Xu H, Hao H, Wu R, Wang H, Lu C. 2017. Effect of environmental conditions on the degradation of florasulam in typical soils of northern China. J Environ Qual. 46(3):553–558.
   PubMed Web of Science ®Google Scholar
• [WHO] World Health Organization. 1997. Guidelines for predicting dietary intake of pesticide residues/prepared by the Global Environment Monitoring System – Food Contamination Monitoring and Assessment Programme (‎GEMS/Food)‎; in collaboration with the Codex Commitee on Pesticide Residues. Rev. ed. Geneva (Switzerland): Programme of Food Safety and Food Aid, World Health Organization. Global Environment Monitoring System. Food Contamination and Monitoring Programme & Joint FAO/WHO Codex Alimentarius Commission. Committee on Pesticide Residues.
   Google Scholar
• Taylor PJ. 2005. Matrix effects: the Achilles heel of quantitative high-performance liquid chromatography-electrospray-tandem mass spectrometry. Clin Biochem. 38(4):328–334.
   PubMed Web of Science ®Google Scholar
• Xu J, Zhang J, Dong F, Liu X, Zhu G, Zheng Y. 2015. A multiresidue analytical method for the detection of seven triazolopyrimidine sulfonamide herbicides in cereals, soybean and soil using the modified QuEChERS method and UHPLC-MS/MS. Anal Methods. 7(23):9791–9799.
   Web of Science ®Google Scholar
• Zhang Z, Feng M, Zhu K, Han L, Sapozhnikova Y, Lehotay SJ. 2016. Multiresidue analysis of pesticides in straw roughage by liquid chromatography–tandem mass spectrometry. J Agric Food Chem. 64(31):6091–6099.
   PubMed Web of Science ®Google Scholar
• Zhao W (2009). Liquefaction of crop stalks in sub- and supercritical alcohols, M.A. Thesis. China University of Mining and Technology.
   Google Scholar
• Zhou W, Yang S, Wang PG. 2017. Matrix effects and application of matrix effect factor. Bioanalysis. 9(23):1839–1844.
   PubMed Web of Science ®Google Scholar