Investigation of stability of selective androgen receptor modulators in urine

References

• Adamowicz P, Malczyk A. 2019. Stability of synthetic cathinones in blood and urine. Forensic Sci Int. 295:36–45. doi:10.1016/j.forsciint.2018.12.001.
   PubMed Web of Science ®Google Scholar
• Berendsen BJA, Elbers IJW, Stolker AAM. 2011. Determination of the stability of antibiotics in matrix and reference solutions using a straightforward procedure applying mass spectrometric detection. Food Addit Contam. 28:1657–1666. doi:10.1080/19440049.2011.604045.
   PubMed Web of Science ®Google Scholar
• Cesbron N, Sydor A, Penot M, Prevost S, Le Bizec B, Dervilly-Pinel G. 2017. Analytical strategies to detect enobosarm administration in bovines. Food Addit Contam. 34:632–640. doi:10.1080/19440049.2016.1258122.
   PubMed Web of Science ®Google Scholar
• Choi SM, Lee B-M. 2015. Comparative safety evaluation of selective androgen receptor modulators and anabolic androgenic steroids. Expert Opin Drug Saf. 14:1773–1785. doi:10.1517/14740338.2015.1094052.
   PubMed Web of Science ®Google Scholar
• [CAC] Codex Alimentarius Commission. 2014. Guidelines for the design and implementation of national regulatory food safety assurance programme associated with the use of veterinary drugs in food producing animals. CAC/GL 71-2009. p. 1–42.
   Google Scholar
• [CRL] Community Reference Laboratories. 2007. Community Reference Laboratories (CRL) Guidance Paper (7 December 2007). CRLs View on State of the Art Analytical Methods for National Residue Control Plans. p. 1–8.
   Google Scholar
• CRL. 2010. Community Reference Laboratories Residues (CRLs) 20/1/2010. Guidelines for the validation of screening methods for residues of veterinary medicines (initial validation and transfer). p. 1–18.
   Google Scholar
• Croubels S, De Baere S, De Backer P. 2003. Practical approach for the stability testing of veterinary drugs in solutions and in biological matrices during storage. Anal Chim Acta. 483:419–427. doi:10.1016/S0003-2670(02)01479-4.
   Web of Science ®Google Scholar
• Cuhadar S, Koseoglu M, Atay A, Dirican A. 2013. The effect of storage time and freeze-thaw cycles on the stability of serum samples. Biochemia Med. 23:70–77. doi:10.11613/BM.2013.009.
   PubMed Web of Science ®Google Scholar
• Dalton JT, Miller DD, Kearbey JD 2016. SARMs and method of use thereof. US009278914B2, United States Patent. https://patentimages.storage.googleapis.com/5e/d2/77/51ddcb0a4e882e/US9278914.pdf.
   Google Scholar
• Dalton JT, Mukherjee A, Zhu Z, Kirkovsky L, Miller DD. 1998. Discovery of nonsteroidal androgens. Biochem Biophys Res Commun. 244:1–4. doi:10.1006/bbrc.1998.8209.
   PubMed Web of Science ®Google Scholar
• de Rijke E, Essers ML, Rijk JCW, Thevis M, Bovee TFH, van Ginkel LA, Sterk SS. 2013. Selective androgen receptor modulators: in vitro and in vivo metabolism and analysis. Food Addit Contam. 30:1517–1526. doi:10.1080/19440049.2013.810346.
   PubMed Web of Science ®Google Scholar
• [EC] European Commission. 1996. Council Directive 96/22/EC of 29 April 1996 concerning the prohibition on the use in stockfarming of certain substances having a hormonal or thyrostatic action and of beta-agonists, and repealing Directives 81/602/EEC, 88/146/EEC and 88/299/EEC.
   Google Scholar
• [EC] European Commission. 2002. Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and interpretation of results. Off J Eur Commun L. 221:8–36.
   Google Scholar
• [FEI] Fédération Equestre Internationale. 2019. 2019 Equine prohibited substances list. https://inside.fei.org/system/files/2019%20Equine%20Prohibited%20Substances%20List.pdf
   Google Scholar
• Gadaj A, Ventura E, Ripoche A, Mooney MH. 2019 Dec 30. Monitoring of selective androgen receptor modulators in bovine muscle tissue by ultra-high performance liquid chromatography-tandem mass spectrometry. Food Chem. 4:100056. doi:10.1016/j.fochx.2019.100056.
   Web of Science ®Google Scholar
• Gaugain M, Chotard M-P, Verdon E. 2013. Stability study for 53 antibiotics in solution and in fortified biological matrixes by LC/MS/MS. J AOAC Int. 96:471–480. doi:10.5740/jaoacint.12-062.
   PubMed Web of Science ®Google Scholar
• Geldof L, Pozo OJ, Lootens L, Morthier W, Van Eenoo P, Deventer K. 2017. In vitro metabolism study of a black market product containing SARM LGD-4033. Drug Test Anal. 9:168–178. doi:10.1002/dta.1930.
   PubMed Web of Science ®Google Scholar
• Hansson A, Knych H, Stanley S, Berndtson E, Jackson L, Bondesson U, Thevis M, Hedeland M. 2018. Equine in vivo-derived metabolites of the SARM LGD-4033 and comparison with human and fungal metabolites. J Chromatogr B. 1074–1075:91–98. doi:10.1016/j.jchromb.2017.12.010.
   PubMed Web of Science ®Google Scholar
• Hansson A, Knych H, Stanley S, Thevis M, Bondesson U, Hedeland M. 2016. Investigation of the selective androgen receptor modulators S1, S4 and S22 and their metabolites in equine plasma using high-resolution mass spectrometry. Rapid Commun Mass Spectrom. 30:833–842. doi:10.1002/rcm.7512.
   PubMed Web of Science ®Google Scholar
• [IFHA] International Federation of Horseracing Authorities. 2019. International Agreement on Breeding, Racing and Wagering (IABRW). Article 6A Prohibited substances. https://www.ifhaonline.org/resources/ifAgreement.pdf
   Google Scholar
• Jiménez C, Ventura R, Segura J, De La Torre R. 2004. Protocols for stability and homogeneity studies of drugs for its application to doping control. Anal Chim Acta. 515:323–331. doi:10.1016/j.aca.2004.03.045.
   Web of Science ®Google Scholar
• Kerrigan S 2011. Sampling, storage and stability. Clarke´s Analysis of Drug and Poisons. p. 445–457. https://pdfs.semanticscholar.org/a919/b24c9667844c627ab9f61df157bc0856dff2.pdf.
   Google Scholar
• Narayanan R, Coss CC, Dalton JT. 2018. Development of selective androgen receptor modulators (SARMs). Mol Cell Endocrinol. 465:134–142. doi:10.1097/OGX.0000000000000256.Prenatal.
   PubMed Web of Science ®Google Scholar
• Rojas D, Dervilly-Pinel G, Cesbron N, Penot M, Sydor A, Prévost S, Le Bizec B. 2017. Selective androgen receptor modulators: comparative excretion study of bicalutamide in bovine urine and faeces. Drug Test Anal. 9:1017–1025. doi:10.1002/dta.2113.
   PubMed Web of Science ®Google Scholar
• European Commission Directorate General for Health and Food Safety. 2017. SANTE/11813/2017. Guidance document on analytical quality control and method validation procedures for pesticide residues and analysis in food and feed. https://ec.europa.eu/food/sites/food/files/plant/docs/pesticides_mrl_guidelines_wrkdoc_2017-11813.pdf
   Google Scholar
• Schmidt KS, Mankertz J. 2018. In-house validation of a liquid chromatography–tandem mass spectrometry method for the determination of selective androgen receptor modulators (SARMS) in bovine urine. Food Addit Contam. 35:1292–1304. doi:10.1080/19440049.2018.1471222.
   PubMed Web of Science ®Google Scholar
• Sobolevsky T, Dikunets M, Rodchenkov G 2015. Metabolism study of the selective androgen receptor modulator LGD-4033. 33rd Cologne Workshop on Dope Analysis, Manfred-Donike Institute, Cologne, Germany. p. 75–79.
   Google Scholar
• Stefanelli P, Barbini DA, Amendola G, Generali T, Girolimetti S, Pelosi P, Santilio A. 2015. A survey on long-term stability of stock standard solutions in pesticide residue analysis. Food Anal Methods. 8:1164–1172. doi:10.1007/s12161-014-9994-4.
   Web of Science ®Google Scholar
• Thevis M, Volmer DA. 2018. Mass spectrometric studies on selective androgen receptor modulators (SARMs) using electron ionization and electrospray ionization/collision-induced dissociation. Eur J Mass Spectrom. 24:145–156. doi:10.1177/1469066717731228.
   PubMed Web of Science ®Google Scholar
• Ventura E, Gadaj A, Monteith G, Ripoche A, Healy J, Botrè F, Sterk SS, Buckley T, Mooney MH. 2019 Apr 22. Development and validation of a semi-quantitative ultra-high performance liquid chromatography-tandem mass spectrometry method for screening of selective androgen receptor modulators in urine. J Chromatogr A. 1600:183–196. doi:10.1016/j.chroma.2019.04.050.
   PubMed Web of Science ®Google Scholar
• Ventura R, Jiménez C, Closas N, Segura J, De La Torre R. 2003. Stability studies of selected doping agents in urine: caffeine. J Chromatogr B. 795:167–177. doi:10.1016/S1570-0232(03)00557-9.
   PubMed Web of Science ®Google Scholar
• [WADA] World Anti-Doping Agency. 2019. The 2019 Prohibited List International Standard. https://www.wada-ama.org/sites/default/files/wada_2019_english_prohibited_list.pdf
   Google Scholar