Investigation of the changes in properties and microstructure of graphene oxide-modified cement pastes due to hydrochloric acid attack

References

• Lin Y, Du H. Graphene reinforced cement composites: a review. Constr Build Mater. 2020;265:120312.
   Google Scholar
• Shah SP, Lomboy GR. Future research needs in self-consolidating concrete. J Sustainable Cem.-Based Mater. 2015;4(3–4):154–163.
   Google Scholar
• Dimov D, Amit I, Gorrie O, et al. Ultrahigh performance Nanoengineered graphene–concrete composites for multifunctional applications. Adv Funct Mater. 2018;28(23):1705183.
   Google Scholar
• Shah SP, Hou P, Konsta-Gdoutos MS. Nano-modification of cementitious material: toward a stronger and durable concrete. J Sustainable Cem.-Based Mater. 2016;5(1–2):1–22.
   Google Scholar
• Muthu M, Santhanam M. Effect of reduced graphene oxide, alumina and silica nanoparticles on the deterioration characteristics of Portland cement paste exposed to acidic environment. Cem Concr Compos. 2018;91:118–137.
   Google Scholar
• Chuah S, Li W, Chen SJ, et al. Investigation on dispersion of graphene oxide in cement composite using different surfactant treatments. Constr Build Mater. 2018;161:519–527.
   Google Scholar
• Raki L, Beaudoin JJ, Alizadeh R. Nanotechnology applications for sustainable cement-based products. Bittnar Z, Bartos PJM, Němeček J, Šmilauer V, Zeman J, editors. Berlin, Heidelberg: Publisher; 2009.
   Google Scholar
• Li D, Müller MB, Gilje S, et al. Processable aqueous dispersions of graphene nanosheets. Nat Nanotechnol. 2008;3(2):101–105.
   Google Scholar
• Ghazizadeh S, Duffour P, Skipper NT, et al. An investigation into the colloidal stability of graphene oxide nano-layers in alite paste. Cem Conc Res. 2017;99:116–128.
   Google Scholar
• Krauß P, Engstler J, Schneider JJ. A systematic study of the controlled generation of crystalline iron oxide nanoparticles on graphene using a chemical etching process. Beilstein J Nanotechnol. 2017;8:2017–2025.
   Google Scholar
• Compton OC, Nguyen ST. Graphene oxide, highly reduced graphene oxide, and graphene: versatile building blocks for carbon-based materials. Small. 2010;6(6):711–723.
   Google Scholar
• Zhao L, Guo X, Song L, et al. An intensive review on the role of graphene oxide in cement-based materials. Constr Build Mater. 2020;241:117939.
   Google Scholar
• Muthu M, Yang E-H, Unluer C. Resistance of graphene oxide-modified cement pastes to hydrochloric acid attack. Constr Build Mater. 2021;273:121990.
   Google Scholar
• Qin H, Wei W, Hang Hu Y. Synergistic effect of graphene-oxide-doping and microwave-curing on mechanical strength of cement. J Phys Chem Solids. 2017;103:67–72.
   Google Scholar
• Lv S, Ma Y, Qiu C, et al. Regulation of GO on cement hydration crystals and its toughening effect. Mag Concr Res. 2013;65(20):1246–1254.
   Google Scholar
• Zhao L, Guo X, Liu Y, et al. Hydration kinetics, pore structure, 3D network calcium silicate hydrate, and mechanical behavior of graphene oxide reinforced cement composites. Constr Build Mater. 2018;190:150–163.
   Google Scholar
• Das B, Eswar Prasad K, Ramamurty U, et al. Nano-indentation studies on polymer matrix composites reinforced by few-layer graphene. Nanotechnology. 2009;20(12):125705.
   Google Scholar
• Xu J-Z, Chen T, Yang C-L, et al. Isothermal crystallization of poly(l-lactide) induced by graphene nanosheets and carbon nanotubes: a comparative study. Macromolecules. 2010;43(11):5000–5008.
   Google Scholar
• Gong K, Pan Z, Korayem AH, et al. Reinforcing effects of graphene oxide on portland cement paste. J Mater Civ Eng. 2015;27(2):A4014010.
   Google Scholar
• Mokhtar MM, Abo-El-Enein SA, Hassaan MY, et al. Mechanical performance, pore structure and micro-structural characteristics of graphene oxide nano platelets reinforced cement. Constr Build Mater. 2017;138:333–339.
   Google Scholar
• Long W-J, Zheng D, Duan H-B, et al. Performance enhancement and environmental impact of cement composites containing graphene oxide with recycled fine aggregates. J Clean Prod. 2018;194:193–202.
   Google Scholar
• Zhou C, Li F, Hu J, et al. Enhanced mechanical properties of cement paste by hybrid graphene oxide/carbon nanotubes. Constr Build Mater. 2017;134:336–345.
   Google Scholar
• Muthu M, Ukrainczyk N, Koenders E. Effect of graphene oxide dosage on the deterioration properties of cement pastes exposed to an intense nitric acid environment. Constr Build Mater. 2021;269:121272.
   Google Scholar
• Qureshi TS, Panesar DK. Impact of graphene oxide and highly reduced graphene oxide on cement based composites. Constr Build Mater. 2019;206:71–83.
   Google Scholar
• Mohammed A, Sanjayan JG, Duan WH, et al. Incorporating graphene oxide in cement composites: a study of transport properties. Constr Build Mater. 2015;84:341–347.
   Google Scholar
• Mohammed A, Sanjayan JG, Nazari A, et al. The role of graphene oxide in limited long-term carbonation of cement-based matrix. Constr Build Mater. 2018;168:858–866.
   Google Scholar
• Jin M, Jiang L, Lu M, et al. Monitoring chloride ion penetration in concrete structure based on the conductivity of graphene/cement composite. Constr Build Mater. 2017;136:394–404.
   Google Scholar
• Du H, Dai Pang S. Enhancement of barrier properties of cement mortar with graphene nanoplatelet. Cem Concr Res. 2015;76:10–19.
   Google Scholar
• Guo K, Miao H, Liu L, et al. Effect of graphene oxide on chloride penetration resistance of recycled concrete. Nanotechnol Rev. 2019;8(1):681–689.
   Google Scholar
• Du HJ, Pang SD. Transport of water and chloride ion in cement composites modified with graphene nanoplatelet. KEM. 2014;629–630:162–167.
   Google Scholar
• Schwotzer M, Scherer T, Gerdes A. Immediate impact on the rim zone of cement based materials due to chemical attack: a focused ion beam study. Mater Charact. 2015;99:77–83.
   Google Scholar
• Gutberlet T, Hilbig H, Beddoe RE. Acid attack on hydrated cement—effect of mineral acids on the degradation process. Cem Concr Res. 2015;74:35–43.
   Google Scholar
• Vafaei M, Allahverdi A, Dong P, et al. Durability performance of geopolymer cement based on fly ash and calcium aluminate cement in mild concentration acid solutions. J Sustainable Cem. Based Mater. 2019;8(5):290–308.
   Google Scholar
• Pavlík V. Corrosion of hardened cement paste by acetic and nitric acids (part II): formation and chemical composition of the corrosion products layer. Cem Concr Res. 1994;24(8):1495–1508.
   Google Scholar
• Ramaswamy KP, Santhanam M. A study of deterioration of cement paste due to acid attack using X-ray computed micro-tomography. Adv Cem Res. 2018;30(3):123–138.
   Google Scholar
• Baroghel-Bouny V, Thiery M, Dierkens M, et al. Aging and durability of concrete in lab and in field conditions – pore structure and moisture content gradients between inner and surface zones in RC structural elements. J Sustainable Cem.-Based Mater. 2017;6(3):149–194.
   Google Scholar
• Alexander M, Bertron A, De Belie N. Performance of cement-based materials in aggressive aqueous environments. Dordrecht, Netherlands: Springer; 2013.
   Google Scholar
• Türkel S, Felekoǧlu B, Dulluç S. Influence of various acids on the physico-mechanical properties of pozzolanic cement mortars. Sadhana. 2007;32(6):683–691.
   Google Scholar
• De Ceukelaire L. The effects of hydrochloric acid on mortar. Cem Concr Res. 1992;22(5):903–914.
   Google Scholar
• Chandra S. Hydrochloric acid attack on cement mortar - an analytical study. Cem Concr Res. 1988;18(2):193–203.
   Google Scholar
• Pavlík V. Corrosion of hardened cement paste by acetic and nitric acids part I: calculation of corrosion depth. Cem Concr Res. 1994;24(3):551–562.
   Google Scholar
• Israel D, Macphee DE, Lachowski E. Acid attack on pore-reduced cements. J Mater. Sci. 1997;32(15):4109–4116.
   Google Scholar
• Midgley H, Illston J. The penetration of chlorides into hardened cement pastes. Cem Concr Res. 1984;14(4):546–558.
   Google Scholar
• SS EN 197-1. Cement - Part 1: composition, specifications and conformity criteria for common cement. Singapore: Singapore Standards Council; 2014. p. 46. https://www.nlb.gov.sg/biblio/201398199
   Google Scholar
• ASTM C1702-17. Standard test method for measurement of heat of hydration of hydraulic cementitious materials using isothermal conduction calorimetry. Pennsylvania: ASTM International; 2017.
   Google Scholar
• Muthu M, Kumar S, Yang E-H, et al. Degradation of carbonated reactive MgO-based concrete exposed to nitric acid. J CO2 Util. 2020;36:210–219.
   Google Scholar
• Ukrainczyk N, Muthu M, Vogt O, et al. Geopolymer, calcium aluminate, and Portland cement-based mortars: comparing degradation using acetic acid. Materials. 2019;12(19):3115.
   Google Scholar
• Li X, Liu Z, Lv Y, et al. Influence of graphene oxide on hydration characteristics of tricalcium silicate. Adv Cem Res. 2019;31(10):448–456.
   Google Scholar
• Rehman SKU, Ibrahim Z, Jameel M, et al. Assessment of rheological and piezoresistive properties of graphene based cement composites. Int J Concr Struct Mater. 2018;12(1):64.
   Google Scholar
• Wang Q, Wang J, Lv C-x, et al. Rheological behavior of fresh cement pastes with a graphene oxide additive. New Carbon Mater. 2016;31(6):574–584.
   Google Scholar
• Scrivener K, Snellings R, Lothenbach B. A practical guide to microstructural analysis of cementitious materials. Ohio: Taylor & Francis Group; 2016.
   Google Scholar
• Wang Q, Wang J, Lu C-X, et al. Influence of graphene oxide additions on the microstructure and mechanical strength of cement. New Carbon Mater. 2015;30(4):349–356.
   Google Scholar
• Long W-J, Ye TH, Gu Y-C, et al. Inhibited effect of graphene oxide on calcium leaching of cement pastes. Constr Build Mater. 2019;202:177–188.
   Google Scholar
• Chen Z, Xu Y, Hua J, et al. Mechanical properties and shrinkage behavior of concrete-containing graphene-oxide nanosheets. Materials. 2020;13(3):590.
   Google Scholar
• Bertron A, Escadeillas G, Duchesne J. Cement pastes alteration by liquid manure organic acids: chemical and mineralogical characterization. Cem Concr Res. 2004;34(10):1823–1835.
   Google Scholar
• Devi SC, Khan RA. Influence of graphene oxide on sulfate attack and carbonation of concrete containing recycled concrete aggregate. Constr Build Mater. 2020;250:118883.
   Google Scholar