Electrochemical behavior and conversion to Fe₂O₃ nano particles of a neutral seven coordinated iron(III) complex with dipicolinic acid

References

• Zhang, X. M.; Tong, M. L.; Gong, M. L.; Chen, X. M. Supramolecular organisation of polymeric coordination chains into a three‐dimensional network with nanosized channels that clathrate large organic molecules. Eur. J. Inorg. Chem. 2003, 2003, 138–142. DOI: 10.1002/ejic.200390014.
   Google Scholar
• Thirumurugan, A.; Natarajan, S. Inorganic–organic hybrid compounds: synthesis and structures of new metal organic polymers synthesized in the presence of mixed dicarboxylates. Eur. J. Inorg. Chem. 2004, 2004, 762–770. DOI: 10.1002/ejic.200300594.
   Google Scholar
• Wen, Y. H.; Cheng, J. K.; Feng, Y. L.; Zhang, J.; Li, Z. J.; Yao, Y. G. Hydrothermal syntheses, crystal structures and characterizations of three new copper coordination polymers. Inorg. Chim. Acta 2005, 358, 3347–3354. DOI: 10.1016/j.ica.2005.05.004.
   Web of Science ®Google Scholar
• Murakami, K.; Tanemura, Y.; Yoshino, M. Dipicolinic acid prevents the copper-dependent oxidation of low density lipoprotein. J. Nutr. Biochem. 2003, 14, 99–103. DOI: 10.1016/S0955-2863(02)00252-8.
   PubMed Web of Science ®Google Scholar
• Gonzalez-Baró, A. C.; Castellano, E. E.; Piro, O. E.; Parajón-Costa, B. S. Synthesis, crystal structure and spectroscopic characterization of a novel bis (oxo-bridged) dinuclear vanadium (V)–dipicolinic acid complex. Polyhedron. 2005, 24, 49–55. DOI: 10.1016/j.poly.2004.09.032.
   Web of Science ®Google Scholar
• Morimoto, I.; Tanaka, S. Spectrophotometric determination of iron with 2, 6-pyridinedicarboxylic acid and 2, 4, 6-pyridinetricarboxylic acid. Anal. Chem. 1963, 35, 141–144. DOI: 10.1021/ac60195a010.
   Web of Science ®Google Scholar
• Setlow, B.; Setlow, P. Dipicolinic acid greatly enhances production of spore photoproduct in bacterial spores upon UV irradiation. Appl. Environ. Microbiol. 1993, 59, 640–643.
   PubMed Web of Science ®Google Scholar
• Laine, P.; Gourdon, A.; Launay, J. P. Chemistry of iron with dipicolinic acid. 1. Mononuclear complexes of iron (II) or iron (III). Inorg. Chem. 1995, 34, 5129–5137. DOI: 10.1021/ic00125a009.
   Web of Science ®Google Scholar
• Laine, P.; Gourdon, A.; Launay, J. P. Chemistry of iron with dipicolinic acid. 2. Bridging role of carboxylate groups in solid state structures. Inorg. Chem. 1995, 34, 5138–5149. DOI: 10.1021/ic00125a010.
   Web of Science ®Google Scholar
• Lainé, P.; Gourdon, A.; Launay, J. P.; Tuchagues, J. P. Chemistry of iron with dipicolinic acid. 3. Heptacoordinated iron in [(dipicH) 2FeII (OH2)] and [(Dipic) 2FeII2 (OH2) 6]. Cntdot. 2dipicH2. Inorg. Chem. 1995, 34, 5150–5155. DOI: 10.1021/ic00125a011.
   Web of Science ®Google Scholar
• Laine, P.; Gourdon, A.; Launay, J. P. Chemistry of iron with dipicolinic acid. 4. Mixed-ligand complexes of iron (III) and related compounds. Inorg. Chem. 1995, 34, 5156–5165. DOI: 10.1021/ic00125a012.
   Web of Science ®Google Scholar
• Tabatabaee, M.; Abbasi, F.; Kukovec, B. M.; Nasirizadeh, N. Preparation and structural, spectroscopic, thermal, and electrochemical characterizations of iron (III) compounds containing dipicolinate and 2-aminopyrimidine or acridine. J. Coor. Chem. 2011, 64, 1718–1728. DOI: 10.1080/00958972.2011.580843.
   Web of Science ®Google Scholar
• Tabatabaee, M.; Dadkhodaee, M.; Kukovec, B. M. Different coordination environments of iron (III) and pseudopolymorphism in complexes with dipicolinic acid and 2-amino-6-picoline. The influence of molar ratio and solvent type. Polyhedron 2013, 51, 316–322. DOI: 10.1016/j.poly.2012.12.033.
   Web of Science ®Google Scholar
• Tabatabaee, M.; Afraziyan, S.; Nasirizadeh, N. Synthesis and characterization a novel co-crystal of acridinium bis (pyridine-2, 6-dicarboxylato) iron (III), acridine, and water molecule,{[(Hacr)[Fe (pydc) 2]} 2· acr· H2O. Synth. React. Inorg. Met.-Org. Chem. 2013, 43, 1181–1185. DOI: 10.1080/15533174.2012.756901.
   Web of Science ®Google Scholar
• Petříček, V.; Dušek, M.; Palatinus, L. Crystallographic computing system JANA2006: general features. Z. Kristallogr. 2014, 229, 345–352. DOI: 10.1515/zkri-2014-1737.
   Web of Science ®Google Scholar
• Palatinus, L.; Chapuis, G. SUPERFLIP–a computer program for the solution of crystal structures by charge flipping in arbitrary dimensions. J Appl Crystallogr 2007, 40, 786–790. DOI: 10.1107/S0021889807029238.
   Web of Science ®Google Scholar
• Nakamoto, K. (1986.) Infrared and Raman Spectra of Inorganic and Coordination Compounds, 4th ed.; Wiley Interscience: New York.
   Google Scholar
• Kukovec, B. M.; Popović, Z.; Kozlevčar, B.; Jagličić, Z. 3D supramolecular architectures of copper (II) complexes with 6-methylpicolinic and 6-bromopicolinic acid: synthesis, spectroscopic, thermal and magnetic properties. Polyhedron 2008, 27, 3631–3638. DOI: 10.1016/j.poly.2008.09.011.
   Web of Science ®Google Scholar
• Ju, H.; Shen, C. Electrocatalytic reduction and determination of dissolved oxygen at a poly (nile blue) modified electrode. Electroanalysis 2001, 13, 789–793. DOI: 10.1002/1521-4109(200105)13:8/9 < 789::AID-ELAN789 > 3.0.CO;2-G.
   Web of Science ®Google Scholar
• Sharp, M.; Petersson, M.; Edström, K. Preliminary determinations of electron transfer kinetics involving ferrocene covalently attached to a platinum surface. J. Electroanal. Chem. 1979, 95, 123–130. DOI: 10.1016/S0022-0728(79)80227-2.
   Web of Science ®Google Scholar
• Laviron, E. General expression of the linear potential sweep voltammogram in the case of diffusionless electrochemical systems. J. Electroanal. Chem. 1979, 101, 19–28. DOI: 10.1016/S0022-0728(79)80075-3.
   Web of Science ®Google Scholar
• Mohammadi, S. Z.; Khorasani-Motlagh, M.; Jahani, S.; Yousefi, M. Synthesis and characterization of α-Fe2O3 nanoparticles by microwave method. Int. J. Nanosci. Nanotechnol. 2012, 8, 87–92.
   Google Scholar
• Ahmadi Golsefidi, M.; Abbasi, F.; Abrodi, M.; Abbasi, Z. Synthesis, characterization and photocatalytic activity of Fe2O3-TiO2 nanoparticles and nanocomposites. J. Nanostruct. 2016, 6, 64–69. DOI: 10.7508/jns.2016.01.010.
   Web of Science ®Google Scholar