38
Views
12
CrossRef citations to date
0
Altmetric
Original Articles

IMPROVEMENT IN QUANTITATIVE ACCURACY OF 13C DEPT INTEGRALS BY PARAMETER-OPTIMIZATION

, , &
Pages 2549-2563 | Received 06 Jul 2002, Accepted 13 Aug 2002, Published online: 02 Feb 2007

REFERENCES

  • Caer , V. , Trierweiler , M. , Jouitteau , C. and Martin , G.J. 1991 . Determination of Site-Specific Carbon Isotope Ratios at Natural Abundance by Carbon-13 Nuclear Magnetic Resonance Spectroscopy . Anal. Chem. , 63 : 2306 – 2313 .
  • Zhang , B.L. , Trierweiler , M. , Jouitteau , C. and Martin , G.J. 1999 . Consistency of NMR and Mass Spectrometry Determinations of Natural-Abundance Site-Specific Carbon Isotope Ratios . The Case of Glycerol. Anal. Chem. , 71 ( 13 ) : 2301 – 2306 .
  • Gutowsky , H.S. , Vold , R.L. and Wells , E.J. 1965 . Theory of Chemical Exchange Effects in Magnetic Resonance . J. Chem. Phys. , 43 : 4107
  • Doddrell , D.M. , Pegg , D.T. and Bendall , M.R. 1982 . Distortionless Enhancement of NMR Signals by Polarization Transfer . J. Magn. Res. , 48 : 323 – 327 .
  • Pegg , D.T. , Doddrell , D.M. and Bendall , M.R. 1982 . Proton-Polarization Transfer Enhancement of a Heteronuclear Spin Multiplet with Preservation of Phase Coherency and Relative Component Intensities . J. Chem. Phys. , 77 ( 6 ) : 2745 – 2752 .
  • Pegg , D.T. and Bendall , M.R. 1985 . Pulse-Sequence Cycles for Editing 13C Spectra When Using an Inhomogeneous Radiofrequency Field . J. Magn. Res. , 63 : 556 – 572 .
  • Pegg , D.T. and Bendall , M.R. 1984 . Self-Compensation for Pulse Error Effects in Editing 13C Spectra with a modified DEPT Sequence . J. Magn. Res. , 60 : 347 – 351 .
  • Bulsing , J.M. , Brooks , W.M. , Field , J. and Doddrell , D.M. 1984 . Polarization Transfer via an Intermediate Multiple-Quantum State of Maximum Order . J. Magn. Res. , 56 : 167 – 174 .
  • Bendall , M.R. and Pegg , D.T. 1983 . Complete Accurate Editing of Decoupled 13C Spectra Using DEPT and Quaternary-Only Sequence . J. Magn. Res. , 53 : 272 – 296 .
  • Schenker , K.V. and Philipsborn , W.V. 1985 . Optimization of INEPT and DEPT Experiments for Spin Systems with Hetero- and Homonuclear Couplings . J. Magn. Res. , 61 : 294 – 305 .
  • Pegg , D.T. 1989 . Some New Techniques in NMR . Contemporary Phys. , 30 ( 2 ) : 101 – 112 .
  • Sorensen , O.W. , Eich , G.W. , Levitt , M.H. , Bodenhausen , G. and Ernst , R.R. 1983 . Product Operator Formalism for the Description of NMR Pulse Experiments . Progress in NMR Spectroscopy , 16 : 163 – 192 .
  • Van den Ven , F.J.M. and Hilbers , C.W. 1983 . A Simple Formalism for the Description of Multiple-Pulse Experiments. Application to a Weakly Coupled Two Spin (I = 1/2) Systems . J. Magn. Res. , 54 : 512 – 520 .
  • Podkorytov , I.S. 1997 . Multipulse NMR. Part 2. Product Operator Description of the Weakly Coupled, wo-Spin 1/2 System . Concepts in Magnetic Resonance , 9 ( 3 ) : 117 – 137 .
  • Pegg , D.T. and Bendall , M.R. 1983 . Heisenberg Picture Approach to Polarization Transfer by the DEPT Sequence . J. Magn. Res. , 53 : 229 – 234 .
  • Martin , Y.L. 1994 . A Global Approach to Accurate and Automatic Quantitative Analysis of NMR Spectra by Complex Least-Squares Curve Fitting . J. Magn. Res. , 111 ( 1 ) : 1 – 10 . Series A
  • Simbrunner , J. and Zieger , G. 1995 . Analysis of Three-Component Composite 180° Pulses . J. Magn. Res. , Series B106 : 142

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.