SYNTHESIS OF SELENIUM-DERIVATIZED NUCLEOSIDES AND OLIGONUCLEOTIDES FOR X-RAY CRYSTALLOGRAPHY

REFERENCES

• Nissen , P. , Hansen , J. , Ban , N. , Moore , P. B. and Steitz , T. A. 2000 . The Structural Basis of Ribosome Activity in Peptide Bond Synthesis . Science , 289 : 920 – 930 .
   Google Scholar
• Ban , N. , Nissen , P. , Hansen , J. , Capel , M. , Moore , P. B. and Steitz , T. A. 1999 . Placement of Protein and RNA Structures into a 5 A-Resolution Map of the 50S Ribosomal Subunit . Nature , 400 : 841 – 847 .
   Google Scholar
• Golden , B. L. , Gooding , A. R. , Podell , E. and Cech , T. R. 1998 . A Preorganized Active Site in the Crystal Structure of the Tetrahymena Ribozyme . Science , 282 : 259 – 264 .
   Google Scholar
• Cate , J. H. , Gooding , A. R. , Podell , E. , Zhou , K. , Golden , B. L. , Szewczak , A. A. , Kundrot , C. E. , Cech , T. R. and Doudna , J. A. 1996 . RNA Tertiary Structure Mediation by Adenosine Platforms . Science , 273 : 1696 – 1699 .
   Google Scholar
• Kim , R. , Holbrook , E. L. , Jancarik , J. , Pandit , J. , Weng , X. , Bohm , A. and Kim , S.-H. 1994 . High-Resolution Crystals and Preliminary X-ray Diffraction Studies of a Catalytic RNA . Acta Cryst. , D50 : 290 – 292 .
   Google Scholar
• Holbrook , S. Personal Communication ,
   Google Scholar
• Egli , c. Personal Communication ,
   Google Scholar
• Usman , N. , Egli , M. and Rich , A. 1992 . Large Scale Chemical Synthesis, Purification and Crystallization of RNA-DNA Chimeras . Nucleic Acids Res. , 20 : 6695 – 6699 .
   Google Scholar
• Pley , H. W. , Flaherty , K. M. and Mckay , D. B. 1994 . Three-dimensional Structure of a Hammerhead Ribozyme . Nature , 372 : 68 – 74 .
   Google Scholar
• Naber , N. , Matuska , M. , Sablin , E. P. , Pate , E. and Cooke , R. 1995 . A Novel Adenosine Triphosphate Analog with a Heavy Atom to Target the Nucleotide Binding Site of Proteins . Protein Science , 4 : 1824 – 1831 .
   Google Scholar
• Hendrickson , W. A and Ogata , C. M. 1997 . Phase Determination from Multiwavenlength Anomalous Diffraction Measurements . Methods in Enzymology, Part A , 276 : 494 – 523 .
   Google Scholar
• Hendrickson , W. A. , Pahler , A. , Smith , J. L. , Satow , Y. , Merritt , E. A. and Phizackerley , R. P. 1989 . Crystal Structure of Core Streptavidin Determined from Multiwavelength Anomalous Diffraction of Synchrotron Radiation . Proc. Natl. Acad. Sci. USA , 86 : 2190 – 2194 .
   Google Scholar
• Yang , W. , Hendrickson , W. A. , Crouch , R. J. and Satow , Y. 1990 . Structure of Ribonuclease H Phased at 2 A Resolution by MAD Analysis of the Selenomethionyl Protein . Science , 249 : 1398 – 1405 .
   Google Scholar
• Ferre-D'Amare , A. R. , Zhou , Kaihong and Doudna , J. A. 1998 . Crystal Structure of a Hepatitis Delta Virus Ribozyme . Nature , 395 : 567 – 574 .
   Google Scholar
• Hale , K. J. and Manaviazar , S. 1994 . Novel Pyranoid Glycals Derived from D-Fructose . Tetrahedron Lett. , 35 : 8873 – 8876 .
   Google Scholar
• Kawashima , E. , Toyama , K. , Ohshima , K. , Kainosho , M. , Kyogoku , Y. and Ishido , Y. 1995 . Novel Synthesis of 2′-deoxy[5′-2H]Ribonucleosides Derivatives from 5′-O-Ac-2′-deoxy-5′-PhSe-ribonucleoside Derivatives . Tetrahedron Lett. , 36 : 6699 – 6700 .
   Google Scholar
• Andreadou , I. , Menge , W. M.P.B. , Commandeur , J. N.M. , Worthington , E. A. and Vermeulen , N. P.E. 1996 . Synthesis of Novel Se-Substituted Selenocysteine Derivatives as Potential Kidney Selective Prodrugs of Biologically Active Selenol Compounds: Evaluation of Kinetics of -Elimination Reactions in Rat Renal Cytosol . J. Med. Chem. , 39 : 2040 – 2046 .
   Google Scholar
• Mautner , H. C. 1956 . The Synthesis and Properties of Some Selenopurines and Selenopyrimidines . J. Am. Chem. Soc. , 78 : 5292 – 5294 .
   Google Scholar
• Richert , C. , Roughton , A. L. and Benner , A. S. 1996 . Nonionic Analogs of RNA with Dimethylene Sulfone Bridges . J. Am. Chem. Soc. , 118 : 4518 – 4531 .
   Google Scholar
• Huang , Z. , Schneider , K. C. and Benner , S. A. 1991 . Building Blocks for Oligonucleotide Analogues with Dimethylene Sulfide, Sulfoxide, and Sulfone Groups Replacing Phosphodiester Linkages . J. Org. Chem. , 56 : 3869 – 3882 .
   Google Scholar
• Jakiwczyk , O. M. , Kristoff , E. M. and McPhee , D. 1993 . Convenient Preparation of Dialkyl Diselenides: A Large Scale Synthesis of bis-(2-hydroxyethyl) Diselenide . Synthetic Communication , 23 : 195 – 199 .
   Google Scholar
• Tang , X.-Q. , Liao , X. and Piccirilli , J. A. 1999 . 2′-C-Branched Ribonucleosides: Synthesis of the Phosphoramidite Derivatives of 2′-C-Methylcytidine and Their Incorporation into Oligonucleotides . J. Org. Chem. , 64 : 747 – 754 .
   Google Scholar