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- Crystal data for 1: C31H25N3O3, monoclinic, colorless crystal of 0.56 × 0.40 × 0.40 mm, space group p21/c (No.14), a = 12.317 (2)Å, b = 12.665 (2)Å, c = 16.781 (3)Å, α = 90°, β = 101.12 (2)°, γ = 90°, V= 2568.6 (7)Å3 (from 28 setting reflections with 2.71 < Θ < 15.69°), Z = 4, Dclac. = 1.261 Mg/m3, F(000) = 1024, μ = 0.082 mm−1. A set of 4729 data (2.03 < Θ < 25.00°) was collected, of these 4507 were unique (Rint = 0.0183). The structure was solved by direct methods and refined by full-matrix least squares (37 non-H atoms anisotropic, 353 variables) of all data, goodness-of-fit 0.916. Final R indices [I > 2*σ (I)], R1 = 0.0561, wR2 = 0.1668; R indices (all data), R1 = 0.1007, wR2 = 0.1851. SHELXS-86 and L-93 software were used