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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 18
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Original Articles

EFFICIENT AND CONVENIENT SYNTHESIS OF 3,4,5-TRIMETHOXYBENZALDEHYDE FROM p-CRESOL

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Pages 2809-2814 | Received 31 Jul 2001, Published online: 18 Oct 2011

REFERENCES

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  • Rao , D.V. and Stuber , F.A. 1983 . An Efficient Synthesis of 3,4,5-Trimethoxybenzaldehyde from Vanillin . Synthesis , : 308
  • Kitajima , N. , Takemura , K. , Moro-oka , Y. , Yoshikuni , T. , Akada , M. , Tomotaki , Y. and Taniguchi , M. 1988 . The Selective Liquid-Phase Oxidation of 3,4,5-Trimethoxytoluene to 3,4,5-Trimethoxybenzaldehyde . Bull. Chem. Soc. Jpn. , 61 ( 3 ) : 1035 – 1037 .
  • Manchand , P.S. , Belica , P.S. and Wong , H.S. 1990 . Synthesis of 3,4,5-Trimethoxybenzaldehyde . Synth. Commun. , 20 ( 17 ) : 2659 – 2666 .
  • Lindley , J. 1984 . Copper-assisted Nucleophilic Substitution of Aryl Halogen . Tetrahedron , 40 ( 9 ) : 1433 – 1456 .
  • Bebon-Rampal , C. and Vanhove , D. 1992 . Catalyseurs Supportés Pour l′ Alcoxylation de Molécules Aromatiques Substituées . Bull. Soc. Chim. Fr. , 129 ( 5 ) : 501 – 508 .
  • Aalten , H.L. , van Koten , G. , Grove , D.M. , Kuilman , T. , Piekstra , O.G. , Hulshof , L.A. and Sheldon , R.A. 1989 . The Copper Catalysed Reaction of Sodium Methoxide with Aryl Bromides. A Mechanistic Study Leading to a Facile Synthesis of Anisole Derivatives . Tetrahedron , 45 ( 17 ) : 5565 – 5578 .
  • de la Mare , P.B.D. and Newman , P.A. 1984 . Solvolytic Elimination and Hydrolysis Promoted by Aromatic Hydroxy Group. Part 1. The Reaction of 2,6-Dibromo-4-dibromomethylphenol and of 2,6-Dibromo-4-bromomethylenecyclohexa-2,5-dienone with Water in 95% 1,4-Dioxane . J. Chem. Soc., Perkin Trans. II , : 231 – 238 .
  • de la Mare , P.B.D. and Newman , P.A. 1984 . Solvolytic Elimination and Hydrolysis Promoted by Aromatic Hydroxy Group. Part 2. The Hydrolysis of 2-Bromo-4-dibromomethylphenol in 95% 1,4-Dioxane . J. Chem. Soc., Perkin Trans. II , : 1797 – 1802 .
  • Cuprous Chloride Needed no Deterioration, Just as well Freshly Prepared
  • Under our Work Conditions, Reaction Pressure was about 0.4 MPa

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