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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 19
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Original Articles

STUDIES TOWARD THE SYNTHESIS OF CONTIGNASTEROL: FUNCTIONALIZATION OF THE STEROIDAL A,B RING SYSTEM

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Pages 2991-3002 | Received 14 Sep 2001, Published online: 16 Aug 2006

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  • Compound 2: 1H NMR (400 MHz, CD3OD) 4.04 (br s, 1H), 3.82 (m, 1H), 3.63 (dd, J = 8.6, 11.6 Hz, 1H), 3.17 (dd, J = 9.6, 8.8 Hz, 1H), 2.39 (dd, J = 8.3, 17.4 Hz, 1H), 2.29 (m, 1H), 1.98 (br m, 4H), 1.70 (m, 3H), 1.53 (m, 2H), 1.37 (m, 4H), 1.19 (dt, J = 3.9, 13.8 Hz, 1H), 1.08 (s, 3H), 0.87 (s, 3H).

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