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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 19
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Original Articles

CONDENSATION OF AROMATIC ALDEHYDES WITH 5,5-DIMETHYL- 1,3-CYCLOHEXANEDIONE WITHOUT CATALYST

, , , , &
Pages 3063-3067 | Received 04 Apr 2001, Published online: 16 Aug 2006

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  • X-ray analysis of 3e: Empirical formula C23H25ClO3, F.W. 384.90, T = 293 K, monoclinic, space group P21/n, a = 6.048(1) Å, b = 19.543(4) Å, c = 17.420(3) Å, β = 97.29(1) Å, V = 2042.2(6) Å3, Z = 4, D c = 1.252 g cm−3, F(000) = 816, λ(MoKα) = 0.71069 Å, μ = 2.06 cm−1, 6<2θ<51°, R = 0.039, R w = 0.047, largest diff. peak 0.18 eÅ−3.
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