Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 3
720
Views
28
CrossRef citations to date
0
Altmetric
Original Articles

Microwave Assisted Improved Synthesis of 6-Formylpterin and Other Heterocyclic Mono- and Di-aldehydes

&
Pages 475-480 | Received 19 Feb 2002, Published online: 17 Aug 2006

References

  • Hennkens , P.H.H. , Ottenhejm , H.C. and Rees , D.C. 1997 . Solid-phase organic reactions II: a review (tetrahedron report no. 418) . Tetrahedron , 53 : 5643 – 5678 .
  • Caddick , S. 1995 . Microwave assisted organic reactions . Tetrahedron , 51 : 10403 – 10432 .
  • Loupy , A. , Pettit , A. , Hamelin , J. , Texier-Boult , F. , Jacquault , P. and Mathe , D. 1998 . New solvent-free organic synthesis using focused microwaves . Synthesis , : 1213 – 1233 .
  • Verma , R.S. 1999 . Green Chem. , : 43 – 55 . For recent review on reactions under microwave irradiation without solvent: and the references therein
  • Thijssen , H.H.H. 1973 . A simple method for preparing 2-amino-4-hydroxy-6-formylpteridine a precursor of the pteridine substrate of dihydropteroate biosynthesis . Anal. Biochem. , 54 : 609 – 611 .
  • Pilato , R.S. , Erickson , K.A. , Greaney , M.A.E. , Stiefel , I. , Goswami , S.P. , Kilpatric , L. , Spiro , T.G. , Taylor , E.C. and Rhiengold , A.L. 1991 . Model complexes for molybdopterin-containing enzymes: preparation and crystallographic characterisation of a molybdenum-ene-1-perthiolate-2-thiolate (trithiolate) complex . J. Am. Chem. Soc. , 113 : 9372 – 9374 .
  • Goswami , S.P. 1993 . Molybdenum co-factor: its biological significance, structural and synthetic aspects . Heterocycles , 35 : 1552 – 1572 .
  • Goswami , S.P. and Adak , A.K. On asymmetric synthesis of Form Z, a precursor to molybdenum co-factor . CTDDR-2001 11–15th Feb . International Symposium on Current Trends in Drug Discovery Research , Abs # OP-XVIV-5 . Lucknow, , India : CDRI .
  • Pateman , J.A. , Coves , D.J. , Rever , B.M. and Roberts , D.B. 1964 . A common co-factor for nitrate reductase and xanthine dehydrogenase which also regulates the synthesis of nitrate reductase . Nature , 201 : 58
  • Hille , R. 1996 . The mononuclear molybdenum enzymes . Chem. Rev. , 96 : 2757 – 2816 .
  • Johnson , J.L. , Hainline , H.E. , Arison , B.H. and Rajagopalan , K.V. 1984 . The pterin component of the molybdenum cofactor . J. Biol. Chem. , 259 : 5414 – 5422 .
  • Taylor , E.C. and Roy , P.S. 1987 . A convenient synthesis of 6-formylpterin . Synth. Comm. , : 1865 – 1868 .
  • Kjaer , A. 1948 . 2-quinoxalinealdehyde and some derivatives . Acta. Chem. Scand. , 2 : 455
  • Gainer , H. 1959 . Synthesis of pyrazinoic acid . J. Org. Chem. , 23 : 691
  • Chandler , C.J. , Deady , L.W. , Reiss , J.A. and Tzimos , V. 1982 . The synthesis of macrocyclic polyether-diesters incorporating 1,10-phenanthrolino and 1,8-naphthyridino subunits . J. Heterocyclic Chem. , 19 : 1017 – 1019 .
  • Chandler , C.J. , Deady , L.W. and Reiss , J.A. 1981 . Synthesis of some 2,9-disubstituted-1,10-phenanthrolines . J. Hetero-cyclic Chem. , 18 : 599 – 602 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.