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Separation Science and Technology Volume 39, 2005 - Issue 15
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Original Articles

Morphology and Size of Cycloolefin Copolymer Precipitated from Toluene Solution Using Compressed CO2 as Antisolvent

He‐An Fan Department of Chemical Engineering, National Tsing Hua University, Hsinchu, 300, Taiwan, ROC
&
Chung‐Sung Tan Department of Chemical Engineering, National Tsing Hua University, Hsinchu, 300, Taiwan, ROCCorrespondence[email protected]
Pages 3453-3469 | Received 01 Sep 2003, Accepted 01 Jun 2004, Published online: 08 Jul 2010

References

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  • Brekner , M. J. , Deckers , H. and Osan , F. Cycloolefin Copolymers Having Low Melt Viscosity and Low Optical Attenuation . US Patent 5,637,400 . 1997 .
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  • Tan , C. S. and Chang , W. W. 1998 . Precipitation of polystyrene from toluene with HFC‐134a by the GAS process . Ind. Eng. Chem. Res. , 37 ( 5 ) : 1821 – 1826 . [CROSSREF] [CSA]
  • Tan , C. S. and Lin , H. Y. 1999 . Precipitation of polystyrene by spraying polystyrene‐toluene solution in to compressed HFC‐134a . Ind. Eng. Chem. Res. , 38 ( 10 ) : 3898 – 3902 . [CROSSREF] [CSA]
  • Hsu , R. Y. , Tan , C. S. and Chen , J. M. 2002 . Formation of micron‐sized cycloolefin copolymer from toluene solution using compressed HFC‐134a as antisolvent . Appl. Polym. Sci. , 84 : 1657 – 1668 . [CROSSREF] [CSA]
  • Dixon , D. J. , Johnston , K. P. and Bodmeier , R. A. 1993 . Polymeric materials formed by precipitation with a compressed fluid antisolvent . AIChE , 39 : 127 – 139 . [CROSSREF]
  • Krause , B. , Mettinkhof , R. , van der Vget , N. F.A. and Wessling , M. 2001 . Microcellular foaming of amorphous high‐Tg polymers using carbon dioxide . Macromolecules , 34 : 874 – 884 . [CROSSREF] [CSA]
  • Dixon , D. J. , Luna‐Bárcenas , G. and Johnston , K. P. 1994 . Microcellular microspheres and microballoons by precipitation with a vapor‐liquid compressed fluid antisolvent . Polymer , 35 : 3998 – 4005 . [CROSSREF]
  • Lefebvre , A. H. 1989 . Atomization and Sprays New York : Hemisphere .
  • Mawson , S. , Kanakia , S. and Johnston , K. P. 1997 . Coaxial nozzle for control of particle morphology in precipitation with a compressed fluid antisolvent . Appl. Polym. Sci. , 64 : 2105 – 2118 .

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