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Original Articles

Synthesis of Stable Isotope-Labeled Precursors for the Biosyntheses of Capsaicinoids, Capsinoids, and Capsiconinoids

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Pages 1611-1614 | Received 10 Mar 2011, Accepted 10 May 2011, Published online: 22 May 2014

  • 1) Suzuki T and Iwai K, “Alkaloids” Vol. 23, ed. Brossi A, Academic Press, New York, pp. 227–299 (1984).
  • 2) del Rosario Abraham-Juárez M, del Carmen Rocha-Granados M, López MG, Rivera-Bustamante FR, and Ochoa-Alejo N, Planta, 227, 681–695 (2008).
  • 3) Stewart CJr, Kang BC, Liu K, Mazourek M, Moore SL, Yoo EY, Kim BD, Paran I, and Jahn MM, Plant J., 42, 675–688 (2005).
  • 4) Singh S, Jarret R, Russo V, Majetich G, Shimkus J, Bushway R, and Perkins B, J. Agric. Food Chem., 57, 3452–3457 (2009).
  • 5) Sutoh K, Kobata K, Yazawa S, and Watanabe T, Biosci. Biotechnol. Biochem., 70, 1513–1516 (2006).
  • 6) Tanaka Y, Hosokawa M, Otsu K, Watanabe T, and Yazawa S, J. Agric. Food Chem., 57, 5407–5412 (2009).
  • 7) Ohara M and Fukuda J, Pharmazie, 33, 467 (1978).
  • 8) 1H- and 13C-NMR spectra (tetramethylsilane was used as the internal standard) of all the compounds were recorded on a JEOL α-400 instrument (JEOL, Tokyo, Japan) at 399.65 and 100.40 MHz, respectively.
  • 9) APCI-MS analyses of all the compounds were performed with the API2000 system (Applied Biosystems, Carlsbad, CA, USA). Thirty μL/min of 10 μM compound was infused into the system with 200 μL/min of MeOH containing 0.1% acetic acid. The ion source was APCI and detection polarity was positive. The optimum parameters for the detection of each compound were tuned automatically by the Analyst software (Applied Biosystems).
  • 10) Krings U, Pilawa S, Theobald C, and Berger RG, J. Biotechnol., 85, 305–314 (2001).
  • 11) Gannett PM, Nagel DL, Reilly PJ, Lawson T, Sharpe J, and Toth B, J. Org. Chem., 53, 1064–1071 (1988).
  • 12) Quideau S and Ralph J, J. Agric. Food Chem., 40, 1108–1110 (1992).
  • 13) Fujiwake H, Suzuki T, Oka S, and Iwai K, Agric. Biol. Chem., 44, 2907–2912 (1980).

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