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Review Article

Extraction and Analysis of Polyphenols: Recent trends

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Pages 227-249 | Received 20 Apr 2010, Accepted 02 Aug 2010, Published online: 12 Nov 2010

References

  • Adil HI, Cetin HI, Yener ME, Bayındırlı A. (2007). Subcritical (carbon dioxide + ethanol) extraction of polyphenols from apple and peach pomaces, and determination of the antioxidant activities of the extracts. J Supercrit Fluids, 43, 55–63.
  • Alonso SG, García-Romero E, Hermosín-Gutiérrez I. 2007. HPLC analysis of diverse grape and wine phenolics using direct injection and multidetection by DAD and fluorescence. J Food Comp Anal, 20, 618–626.
  • Alonso-Salces RM, Herrero C, Barranco A, Berrueta LA., Gallo B, Vicente F. 2005. Classification of apple fruits according to their maturity state by the pattern recognition analysis of their polyphenolic compositions. Food Chem, 93, 113–123.
  • Alonso-Salces RM, Barranco A, Abad B, Berrueta LA, Gallo B, Vicente F. 2004. Polyphenolic profiles of Basque cider apple cultivars and their technological properties. J Agri Food Chem, 52, 2938–2952.
  • Alonso-Salces RM, Korta E, Barranco A, Berrueta LA, Gallo B, Vicente F. 2001. Pressurized liquid extraction for the determination of polyphenols in apple. J Chromatogr A, 933, 37–43.
  • Andrade Seabra R, Ferreira M, Ferreres F, García-Viguera C. 1998. Analysis of non-coloured phenolics in port wines by capillary zone electrophoresis. Zeitschrift für Lebensmittelunterschang und-forschung, 206, 161–164.
  • Antolovich M, Prenzler P, Robards K, Ryan D. 2000. Sample preparation in the determination of phenolic compounds in fruits. Analyst, 125, 989–109.
  • AOAC Association of Official Analytical Chemists, Official Methods of Analysis, 12th ed., AOAC, Washington, DC, 1980.
  • Arce L, R’ıos A, Valca'rcel M. (1998a). Determination of anti-carcinogenic polyphenols present in green tea using capillary electrophoresis coupled to a flow injection system. J Chromatogr A, 827, 113–120.
  • Arce L, Tena MT, Rios A, Valcárce M. (1998b). Determination of trans-resveratrol and other polyphenols in wines by a continuous flow sample clean-up system followed by capillary electrophoresis separation. Anal Chim Acta, 359, 27–38.
  • Arts ICW, Hollman PCH. (2005). Polyphenols and disease risk in epidemiologic studies. Am J Clin Nutr, 81, 317S–325S.
  • Astadi IR, Astuti M, Santoso U, Nugraheni PS. (2009). In vitro antioxidant activity of anthocyanins of black soybean seed coat in human low density lipoprotein (LDL). Food Chem, 112, 659–663.
  • Barros L, Dueñas M, Ferreira ICFR, Baptist P, Santos-Buelga C. (2009). Phenolic acids determination by HPLC-DAD-ESI/MS in sixteen different Portuguese wild mushrooms species. Food Chem Toxicol, 47, 1076–1079.
  • Bartolomé A, Gómez-Cordov’es C. (1999). Barley spent grain: release of hydroxycinnamic acids (ferulic and p-coumaric acids) by commercial enzyme preparations. J Sci Food Agric, 79, 435–439.
  • Baydar NG, Özkan G, Sağdiç O. (2004). Total phenolic contents and antibacterial activities of grape (Vitis vinifera L.) extracts. Food Contrl 15, 335–339.
  • Berna A, Ch’afer A, Mont’on JB. (2001). High-pressure solubility data of the system resveratrol (3) +ethanol (2)+CO2 (1). J Supercriti Fluids, 19, 133–139.
  • Bonoli M, Pelillo Toschi TG, Lercker G. (2003). Analysis of green tea catechins: comparative study between HPLC and HPCE. Food Chem, 81, 631–638.
  • Borneman Z, Gokmen V, Nijhuis HH. (2001). Selective removal of polyphenols and brow colour in apple juices using PEPPVP membranes in a single ultrafiltration process. Sep Purif: Technol, 22/23, 53–61.
  • Borochov-Neori H, Judeinstein S, Tripler F, Harari M, Greenberg A, Shomer I, Holland D. (2009). Seasonal and cultivar variations in antioxidant and sensory quality of pomegranate (Punica granatum L.) fruit. J Food Comp Anal, 22, 189–195.
  • Bourgeois W, Burgess JE, Stultz RM. (2001). On-line monitoring of wastewater quality: a review. J Chem Tech BioTech, 76, 337–348.
  • Brachet A, Rudaz S, Mateus L, Christen P, Veuthey J-L. (2001). Optimisation of accelerated solvent extraction of cocaine and benzoylecgonine from coca leaves. J Separation Sci, 24, 865–887.
  • Bravo L. (1998). Polyphenols: chemistry, dietary sources, metabolism, and nutritional significance. Nutr Rev, 56, 317–333.
  • Buiarelli F, Cartoni G, Coccioli F, Levetsovitou Z. (1995). Determination of phenolic acids in wine by high-performance liquid chromatography with a microbore column. J Chromatogr A, 695, 229–235.
  • Bystrom L, Betty A, Lewis Brown DL, Rodriguez E, Obendorf RL. (2008). Characterisation of phenolics by LC–UV/Vis, LC–MS/MS and sugars by GC in Melicoccus bijugatus Jacq. ‘Montgomery’ fruits. Food Chem, 111, 1017–1024.
  • Camel V. (2001). Recent extraction techniques for solid matrices supercritical fluid extraction pressurised fluid extraction and microwave-assisted extraction: their potential and pitfalls. Analyst, 126, 1182–1193.
  • Campanella L, Favero G, Pastorino M, Tomassetti M. (1999). Monitoring the rancification process in olive oils using a biosensor operating in organic solvents. Biosens Bioelectron 14, 179–186.
  • Cao Y, Zhang X, Ding X, Fang Y, Ye J. (2001a). Determination of caffeine, epicatechin and ascorbic acid in tea samples by capillary zone electrophoresis with electrochemical detection. Chin J Anal Chem, 29, 1072–1075.
  • Cao Y, Zhang X, Fang Y, Ye J. (2001b). Determination of phenolic compounds in red wine by capillary zone electrophoresis with electrochemical detection. Chem J Chinese Univ, 22, 2011–2013.
  • Capannesi C, Palchetti I, Mascini M, Parenti A. (2000). Electrochemical sensor and biosensor for polyphenols detection in olive oils. Food Chem, 71, 553– 562.
  • Carrasco-Pancorbo A, Neusüss C, Pelzing M, Segura-Carretero A, Fernández-Gutiérrez A. (2007). CE- and HPLC-TOF-MS for the characterization of phenolic compounds in olive oil. Electrophoresis, 28, 806–21.
  • Chafer A, Fornari T, Berna A, Stateva RP. (2004). Solubility of quercetin in supercritical CO2 + ethanol as a modifier: measurements and thermodynamic modeling. J Supercrti Fluids, 32, 89–96.
  • Chassagne D, Crouzet J, Bayonove CL, Baumes RL. (1998). Identification of Passion Fruit Glycosides by Gas Chromatography/Mass Spectrometry. J Agric Food Chem, 46, 4353–4357.
  • Chavan UD, Shahidi F, Naczk M. (2001). Extraction of condensed tannins from beach pea (Lathyrus maritimus L.) as affected by different solvents. Food Chem, 75, 509–512
  • Chee KK, Wong MK, Lee HK. (1996). Optimization of microwave-assisted solvent extraction of polycyclic aromatic hydrocarbons in marine sediments using a microwave extraction system with high-performance liquid chromatography fluorescence detection and gas chromatography-mass spectrometry. J Chromatogr A, 723, 59– 271.
  • Chemat F, Tomao V, Virot M. (2008). Ultrasound-assisted extraction in food analysis, in: S. Ötles (Ed.), Handbook of Food Analysis Instruments, Taylor & Francis, CRC Press, 85–103.
  • Chen F, Sun Y, Zhao G, Liao X, Hu X, Wu J, Wang Z. (2007). Optimization of ultrasound-assisted extraction of anthocyanins in red raspberries and identification of anthocyanins in extract using high-performance liquid chromatography–mass spectrometry. Ultrasonics Sonochem, 14, 767–778.
  • Chen Q, Zhao J, Liu M, Cai J, Liu J. (2008). Determination of total polyphenols content in green tea using FT-NIR spectroscopy and different PLS algorithms. J Pharma Biomed Anal, 46, 568–573.
  • Chethan S, Malleshi NG. (2007). Finger millet polyphenols: Optimization of extraction and the effect of pH on their stability. Food Chem, 105, 862–87.
  • Chirinos R, Campos D, Costa N, Arbizu C, Pedreschi R, Larondelle Y. (2008). Phenolic profiles of andean mashua (Tropaeolum tuberosum Ruíz and Pavón) tubers: Identification and evaluation of their antioxidant capacity contribution. Food Chem, 106, 1285–1298.
  • Choi ES, Noh MJ, Yoo KP. (1998). Solubilities of o-, m- and p-coumeric acid isomers in carbon dioxide at 308.15–323.15K and 8.5–25Mpa. J Chem Eng Data, 43, 6–8.
  • Chu Y, Sun J, Wu X, Liu RH. (2002). Antioxidant and antiproliferatve activity of common vegetables. J Agric Food Chem, 50, 6910–6916.
  • Chung S, Champagne ET. (2008). Using phenolic compounds to reduce the allergenic properties of peanut extracts and peanut butter slurries. J Allergy Clini Imm, 121,S249.
  • Cikalo MG, Bartle KD, Robson MM, Myers P, Euerby MR. (1998). Capillary electrochromatography. Analyst, 123, 87R–102R.
  • Conway WD, Petrovski RG. (1995). Modern Countercurrent Chromatography, (Eds.), ACS Symposium Series, vol. 593, American Chemical Society, Washington, DC.
  • Cozzolino D, Kwiatkowskia MG, Parkera M, Cynkara WU, Dambergsa RG, Gishena M, Herdericha MJ. (2004). Prediction of phenolic compounds in red wine fermentations by visible and near infrared spectroscopy. Anal Chimi Acta, 513, 73–80.
  • Cuyckens F, Claeys M. (2004). Mass spectrometry in the structural analysis of flavonoids. J Mass Spectrom, 39, 1–15.
  • Dall’Orto VC, Danilowicz C, Rezzano I, Del Carlo M, Mascini M. (1999). Comparison between three amperometric sensors for phenols determination in olive oil samples. Anal Lett, 32, 1981–1990.
  • Degenhart D, Hofmann S, Knapp H, Winterhalter P. (2000). Preparative isolation of anthocyanins by high-speed countercurrent chromatography and application of the color activity concept to red wine. J Agric Food Chem, 48, 5812–5818.
  • Del Rio D, Costa LG, Lean MEG, Crozier A. (2010). Polyphenols and health: What compounds are involved? Nutr Metabol Cardiovasc Diseases, 20, 1–6.
  • Didenko YT, Suslick KS. (2002). The energy efficiency of formation of photons, radicals and ions during single-bubble cavitation. Nature, 418, 394–397.
  • Du Q, Zheng J, Xu Y. (2008). Composition of anthocyanins in mulberry and their antioxidant activity. J Food Comp Anal, 21, 390–395.
  • Ehala S, Vaher A, Kaljurand A. (2005). Characterization of Phenolic Profiles of Northern European Berries by Capillary Electrophoresis and Determination of their Antioxidant Activity. J Agric Food Chem, 53, 6484–6490.
  • Elfahmi, Ruslan K, Batterman S, Bos R, Kayser O, Herman J, Woerdenbag Quax WJ. (2007). Lignan profile of Piper cubeba, an Indonesian medicinal plant. Biochem System Ecol, 35, 397–402.
  • Eskilsson SC, Bjorklund E. (2000). Analytical-scale microwave assisted extraction. J Chromatogr A, 902, 227–250.
  • Falla FS, Larini GAC, Roux L, Quina FH, Moro LFL, Nascimento CAO. (2006). Characterization of crude petroleum by NIR. J Petroleum Sci Eng, 51, 127–137.
  • Fayad PB, Prvost M, Sauv S. (2010). Laser Diode Thermal Desorption/Atmospheric Pressure Chemical Ionization Tandem Mass Spectrometry Analysis of Selected Steroid Hormones in Wastewater: Method Optimization and Application. Anal Chem, 82, 639–645.
  • Fernandes CIS, Rebelo MJF. (2009). Polyphenolic Biosensors. Application in Red Wines. Portugaliae Electrochimi Acta, 27, 457–462.
  • Fiamegos YC, Stkas CD, Pilidis GA, Karayannis MI. (2000). Synthesis and analytical applications of 4-aminopyrazolone derivatives as chromogenic agents for the spectrophotometric determination of phenols. Anal Chimi Acta, 403, 315–323.
  • Foucault AP, Chevolot L. (1998). Counter-current chromatography: instrumentation, solvent selection and some recent applications to natural product purification. J Chromatogr A, 808, 3–22.
  • Frazier RA, Papadopoulou A. (2003). Recent advances in the application of capillary electrophoresis for food analysis. Electrophoresis, 24, 4095–4105.
  • Gallardo C, Jiménez L, García-Conesa MT. (2006). Hydroxycinnamic acid composition and in vitro antioxidant activity of selected grain fractions. Food Chem, 99, 455–463.
  • Garcia AA, Bonen J, Ramirez-Vick M, Sadaka, Vuppu A. (1999). Bioseparation Process Science, Blackwell Science Inc., Malden, UK.
  • Gawdzik B, Gawdzik J, Czerwinska-Bill V. (1990). Use of polymeric sorbents for the pre-concentration of priority pollutant phenols from water for high-performance liquid-chromatographic analysis. J Chromatogr, 509, 135–140.
  • Germano MP, Angelo VD, Biasini T, Sanogo R, De Pasquale R, Catania S.(2006). Evaluation of the antioxidant properties and bioavailability of free and bound phenolic acids from Trichilia emetica Vahl. J Ethnopharma, 105, 368–373.
  • Gerothanassis IP, Exarchou V, Lagouri V, Troganis A, Tsimidou M, Boskou D. (1998). Methodology for identification of phenolic acids in complex phenolic mixtures by high resolution two-dimensional nuclear magnetic resonance. Application to methanolic extracts of two oregano species. J Agri Food Chem, 46, 4185–4192.
  • Gfrerer M, Lankmayr E. (2005). Screening, optimization and validation of microwave-assisted extraction for the determination of persistent organochlorine pesticides. Anal Chimi Acta, 533, 203–211.
  • Ghindilis AL, Gavrilova VP, Yaropolov AI. (1992). Laccase-based biosensor for determination of polyphenols: determination of catechols in tea. Biosens Bioelectron, 7, 127–131.
  • Gibson TD. (1999). Biosensors: the stability problem. Analusis, 27, 630–638.
  • Gioacchini AM, Roda A, Galletti GC, Bocchini P, Manetta AC, Baraldini M. (1996). High-performance liquid chromatographic-electrospray mass spectrometric analysis of phenolic acids and aldehydes. J Chrom A, 730, 31–37.
  • Glowniak K, ZgoÂrka G, Kozyra M. (1996). Solid-phase extraction and reversed-phase high-performance liquid chromatography chromatography of free phenolic acids in some Echinacea species. J Chromatogr A, 730, 25– 29.
  • Goldstein JL, Swain T. (1963). Changes in tannins in ripening fruits. Phytochem, 2, 371–383.
  • Goli AH, Barzegar M, Sahari MA. (2004). Antioxidant activity and total phenolic compounds of pistachio (Pistachia vera) hull extracts. Food Chem, 92, 521–525.
  • Goli AH, Barzegar M, Sahari MA. (2005). Antioxidant activity and total phenolic compounds of pistachio (Pistachia vera) hull extracts. Food Chem, 92, 521–525.
  • Gruz J, Novák O, Strnad M. (2008). Rapid analysis of phenolic acids in beverages by UPLC–MS/MS. Food Chem, 111, 789–794.
  • Guerrero MS, Torres JS, Nunez MJ. (2008). Extraction of polyphenols from white distilled grape pomace: optimization and modelling. Bioresour Tech, 99, 1311–1318.
  • Gurdial GS, Foster NR, Yun SL, Tilly KD. (1993). Phase behaviour of supercritical fluid-entrainer systems, in: Kiran E., Brennecke. JF. (Eds.), Supercritical Fluid Engineering Science: Fundamentals and Applications, ACS Symposium Series, Washington, DC, 34–39.
  • Haarhaus U, Swidersky P, Schneider GM. (1995). High-pressure investigations on the solubility of dispersion dyestuffs in supercritical gases by VIS/NIR-spectroscopy. Part I — 1,4-Bis-(octadecylamino)-9,10-anthraquinone and disperse orange in CO2 and N2O Up to 180 MPa. The J Supercriti Fluids, 8, 100–106.
  • Hall MN, Robertson A, Scotter CNG. (1988). Near-infrared reflectance prediction of quality, theaflavin content and moisture content of black tea. Food Chem, 27, 61–75.
  • Halliwell B, Gutteridge JMC. (2001). Free Radicals in Biology and Medicine. Oxford University Press, Oxford.
  • Hallman PCH, Katan MB. (1997). Absorption, metabolism and health effects of dietary flavonoids in man. Biomed Pharmother, 51, 305–316.
  • Harborne JB, Baxter H, Moss GPA. (1999). Handbook of Bioactive Compounds from Plants. Taylor and Francis, London.
  • Hoffsommer JC, Glover DF, Hazzard CY. (1980). Quantitative analysis of polynitrophenols in the micro and nano gram range by reversed-phase high-performance ion chromatography. J Chromatogr, 195, 435–440.
  • Hoong YB, Pizzi A, Tahir AD, Pasch H. (2010). Characterization of Acacia mangium polyflavonoid tannins by MALDI-TOF mass spectrometry and CP-MAS 13C NMR. Eur Polymer J, 46, 1268–1277.
  • Horie H, Yamauchi Y, Kohata K. (1998). Analysis of organic anions in tea infusions using capillary electrophoresis. J Chromatogr A, 817, 139–144.
  • Hossain MM. (2005). Membrane Processing of Echinacea purpurea Herb Juice Extract. Develop Chem Eng Mineral Proces, 13 , 71–78.
  • Hsu CL, Wu CH, Huang SL, Yen GC. (2009). Phenolic compounds rutin and o-coumaric acid ameliorate obesity induced by high-fat diet in rats. J Agric Food Chem, 57, 425–31.
  • Huang MT, Ma W, Yen P, Xie JG, Han J, Frenkel K, Grunberger D, Conney AH. (1996). Inhibitory effects of caffeic acid phenethyl ester (CAPE) on 12-O-tetradecanoylphorbol-13-acetate-induced tumor promotion in mouse skin and the synthesis of DNA, RNA and protein in HeLa cells. Carcinogenesis, 17, 761–765.
  • Huang Z, Fasco MJ, Kaminsky LS. (1997). Inhibition of estrone sulfatase in human liver microsomes by quercetin and other flavonoids. J Steroid Biochem Mol Biol, 63, 9–15.
  • Huntley AL. (2009). The health benefits of berry flavonoids for menopausal women: Cardiovascular disease, cancer and cognition. Maturitas, 63, 297–301.
  • Imabayashi S, Kong YT, Watanabe M. (2001). Amperometric biosensor for polyphenols based on horseradish peroxidase immobilized on gold electrodes. Electroanalysis, 13, 408–412.
  • Inoue KH, Hagerman AE. (1988). Determination of gallotannin with rhodanine. Anal Biochem, 169, 363–369.
  • Jeller AH, Silva DHS, Lião LM, Bolzani VS, Furlan M. (2004). Antioxidant phenolic and quinonemethide triterpenes from Cheiloclinium cognatum. Phytochemistry, 65, 1977–1982.
  • Kamangerpour A, Ashraf-Khorassani M, Taylor LT, McNair HM, Chorida L. (2002). Supercritical fluid chromatography of polyphenolic compounds in grape seed extract. Chromatographia, 55, 417–421.
  • Kaufmann B, Christen P. (2002). Recent extraction techniques for natural products: Microwave-assisted extraction and pressurized solvent extraction. Phytochem Anal, 13, 105–113.
  • Keller H, Hohlfeld H, Wray V, Hahabrock K, Scheel D, Strack D. (1996). Changes in the accumulation of soluble and cell wall-bound phenolics in elicitor-treated cell suspension cultures and fungus-infected leaves of Solanum tuberosum. Phytochemistry, 42, 389–396.
  • King P, Ma G, Miao W, Jia Q, McDougall B, Reinecke ME, Cornell C, Kuan J, Kim T, Robinson W. (1999). Structure−Activity Relationships: Analogues of the Dicaffeoylquinic and Dicaffeoyltartaric Acids as Potent Inhibitors of Human Immunodeficiency Virus Type 1 Integrase and Replication. J Med Chem, 42, 497–509.
  • Klejdus B, Vitamvásová D, Kubá V. (1999). Reversed-phase high-performance liquid chromatographic determination of isoflavones in plant materials after isolation by solid-phase extraction. J Chromatogr A, 839, 261–263.
  • Klejdus B, Kubá V. (2000). High performance liquid chromatographic determination of phenolic compounds in seed exudates of Festuca arundinacea and F. pratense. Phytochem Anal, 11, 375–379.
  • Köhler N, Wray V, Winterhalter P. (2008). Preparative isolation of procyanidins from grape seed extracts by high-speed counter-current chromatography. J Chromatogr A, 1177, 114–125.
  • Kool MM, Comeskey Daniel J, Cooney, Janine M McGhie Tony K. (2010). Structural identification of the main ellagitannins of a boysenberry (Rubus loganbaccus × baileyanus Britt.) extract by LC–ESI-MS/MS, MALDI-TOF-MS and NMR spectroscopy. Food Chem, 119, 1535–1543.
  • Koshihara Y, Neichi T, Murota S, Laob A, Fujimoto S, Tatsuno T. (1984). Caffeic acid is a selective inhibitor for leukotriene biosynthesis. Biochem Biophys Acta, 792, 92–97.
  • Kramer R. (1998). Chemometric Techniques for Quantitative Analysis, Dekker, New York, NY.
  • Krygier K, Sosulski F, Hogge L. (1982). Free, esterified, and insoluble-bound phenolic acids. 1. Extraction and purification procedure. J Agric Food Chem, 30, 330–333.
  • Kulys J, Vidziunaite R. (2003). Amperometric biosensors based on recombinant laccases for phenols determination. Biosens Bioelectron, 18, 319–25.
  • Lai JP, Lim YH, Su J, Shen HM, Ong CN. (2007). Identification and characterization of major flavonoids and caffeoylquinic acids in three Compositae plants by LC/DAD–APCI/MS. J Chromatogra B, 848, 215–225.
  • Lamaison JLC, Carnet A. (1990). The amount of main flavonoids in flowers and leaves of Crataegus monogyna Jacq. and Crataegus laevigata (Poiret) DC. (Rosaceae). Pharmaceutica Acta Helvetiae, 65, 315–320.
  • Landbo AK, Meyer AS. (2001). Enzyme-assisted extraction of antioxidative phenols from black currant juice press residues (Ribes nigrum). J Agric Food Chem, 49, 3169–3177.
  • Lapornik B, Prošek M, Golc Wondra A. (2005). Comparison of extracts prepared from plant by-products using different solvent and extraction time. J Food Eng, 71, 214–222.
  • Larger PJ, Jonesb AD, Dacombe C. (1998). Separation of tea polyphenols using micellar electrokinetic chromatography with diode array detection. J Chromatogr A, 799, 309–320.
  • Lay-Keow N, Michel H. (2003). Effects of moisture content in cigar tobacco on nicotine extraction similarity between Soxhlet and focused open-vessel microwave-assisted techniques. J Chromatogr A, 1011, 213–219.
  • Le Bourvellec C, Guyot S, Renard CMGC. (2009). Interactions between apple (Malus x domestica Borkh.) polyphenol and cell walls modulate the extractability of polysaccharides. Carbohydrate Polymers, 75, 251–261.
  • Le Floch F, Tena MT, R’ıos A, Valc’arcel M. (1998). Supercritical fluid extraction of phenol compounds from olive leaves. Talanta, 46, 1123– 1130.
  • Letellier M, Budzinski H. (1999). Microwave assisted extraction of organic compounds. Analusis, 27, 259–271.
  • Li W, Qu H. (2010). Rapid quantification of phenolic acids in Radix Salvia Miltrorrhiza extract solutions by FT-NIR spectroscopy in transflective mode. J Pharm Biomed Anal, 52, 425–431.
  • Liggins J, Bluck LJC, Coward A, Bingham SA. (1998). Extraction and quantification of daidzein and genistein in food. Anal Biochem, 264, 1–7.
  • Liu B, Zhu Y. (2007). Extraction of flavonoids from flavonoid-rich parts in tartary buckwheat and identification of the main flavonoids. J Food Eng, 78, 584–587.
  • Liu AH, Guo Hui, Ye Min, Lin Yan-Hua, Sun Jiang-Hao, Man Xu, Guo De-An. (2007). Detection, characterization and identification of phenolic acids in Danshen using high-performance liquid chromatography with diode array detection and electrospray ionization mass spectrometry. J Chromatography A, 1161, 170–182.
  • Liu Z, Wang J, Shen P, Wang C, Shen Y. (2006). Microwave-assisted extraction and high-speed counter-current chromatography purification of ferulic acid from Radix Angelicae sinensis. Separa Purifi Tech, 52, 18–21.
  • Longares-Patron A, Canizares-Mac MP. (2006). Focused microwaves assisted extraction and simultaneous spectrophotometric determination of vanillin and p-hydroxybenzaldehyde from Vanilla fragans. Talanta, 69, 882–887.
  • Louli V, Ragoussis N, Magoulas K. (2004). Recovery of phenolic antioxidants from wine industry by-products. Bioresour Tech, 92, 201–208.
  • Luque-Garcia JL, Luque de Castro MD. (2003). Ultrasound: a powerful tool for leaching. Trends Anal Chem, 22, 41–47.
  • Maier G, Frei M, Wucherpfennig K, Dietrich H, Ritter G. (1994). Innovative processes for production of ultra filtered apple juices and concentrates. Fruit Process, 5, 134–1 38.
  • Marinova EM, Yanishlieva NV. (1997). Antioxidative activity of extracts from selected species of the family Lamiacea in sunflower oil. Food Chem, 58, 245–248.
  • Marston A, Hostettmann K. (2007). Natural products - High-Speed Countercurrent Chromatography. Encycl Separ Sci, 3415–3424.
  • Martino E, Ramaiola I, Urbano M, Bracco F, Collina S. (2006). Microwave-assisted extraction of coumarin and related compounds from Melilotus officinalis (L.) Pallas as an alternative to Soxhlet and ultrasound-assisted extraction. J Chromatogr A, 1125, 147–151.
  • Mauryaa A, Srivastava SK. (2009). Large-scale separation of clavine alkaloids from Ipomoea muricata by pH-zone-refining centrifugal partition chromatography. J Chromatography B, 877, 1732–1736.
  • McDougall GJ, Fyffe S, Dobson P, Stewart D. (2007). Anthocyanins from red cabbage – stability to simulated gastrointestinal digestion. Phytochem, 68, 1285–1294.
  • McMurrough I, McDowell J. (1978). Chromatographic separation and automated analysis of flavanols. Anal Biochem, 91, 92–100.
  • Mello LD, Kubota LT. (2007). Biosensors as a tool for the antioxidant status evaluation. Talanta, 72, 335–348.
  • Meyer AS, Jepsen SM, Sørensen NS. (1998). Enzymatic release of antioxidants for human low-density lipoprotein from grape pomace. J Agric Food Chem, 46, 2439–2446.
  • Moane S, Park S, Lunte CE, Smyth MR. (1998). Detection of phenolic acids in beverages by capillary electrophoresis with electrochemical detection. Analyst, 123, 1931–1936.
  • Moder M, Schrader S, Franck U, Popp P. (1997). Determination of phenolic compounds in waste water by solid-phase micro extraction. Fresenius' J of Anal Chem, 357, 326–332.
  • Mudnic I, Darko Modun Vesna, Rastija, Jonatan Vukovic, Ivica Brizic, Visnja Katalinic Bernard, Kozina, Marica Medic-Saric Mladen, Boban. (2010). Antioxidative and vasodilatory effects of phenolic acids in wine. Food Chem, 119, 1205–1210.
  • Munteanu F, Lindgren A, Emneus J, Gorton L, Ruzgas T, Csöregi E, Ciucu A, Van Huystee RB, Gazaryan G, Lagrimini L. (1998). Bioelectrochemical monitoring of phenols and aromatic amines in flow injection using novel plant peroxidases. Anal Chem, 70, 2596–2600.
  • Murga R, Ruiz R, Beltr’an S, Cabezas JL. (2000). Extraction of natural complex phenols and tannins from grape seeds by using supercritical mixtures of carbon dioxide and alcohol. J Agric Food Chem, 48, 3408– 3412.
  • Murga R, Sanz MT, Beltran S, Cabezas JL. (2003). Solubility of three hydroxycinnamic acids in supercritical carbon dioxide. J Supercriti Fluids, 27, 239–245.
  • Naczk M, Shahidi F. (2004). Extraction and analysis of phenolics in food. J Chromatogr A, 1054, 95–111.
  • Naczk M, Shahidi F. (2006). Phenolics in cereals, fruits and vegetables: occurrence, extraction and analysis. J Pharma Biomed Anal, 41, 1523–1542.
  • Nahar L, Sarker SD. (2005). Supercritical Fluid Extraction. Methods in Biotechnology, Vol. 20, Natural Products Isolation, 2nd ed. Edited by: SD. Sarker, Z. Latif, and AI. Gray Humana Press Inc., Totowa, NJ. 47–76.
  • Nakabayashi R, Kusano M, Kobayashi M, Tohge T, Yonekura-Sakakibara K, Kogure N, Yamazaki N, Kitajima M, Saito K, Takayama H. (2009). Metabolomics-oriented isolation and structure elucidation of 37 compounds including two anthocyanins from Arabidopsis thaliana. Phytochem, 70, 1017–1029.
  • Nardini M, Cirillo E, Natella F, Mencarelli D, Comisso A, Scaccini C. (2002). Detection of bound phenolic acids: prevention by ascorbic acid and ethylenediaminetetraacetic acid of degradation of phenolic acids during alkaline hydrolysis. Food Chem, 79, 119–124.
  • Nawaz H, Shi J, Mittal GS, Kakuda Y. (2006). Extraction of polyphenols from grape seeds and concentration by ultrafiltration. Separa Purifi Tech, 48, 176–181.
  • Nevado JJB, Peñalvo GC, Robledo VR, Martínez GV. (2009). New CE–ESI-MS analytical method for the separation, identification and quantification of seven phenolic acids including three isomer compounds in virgin olive oil. Talanta, 79, 1238–1246.
  • Okuda T. (2005). Systematics and health effects of chemically distinct tannins in medicinal plants. Phytochem, 66, 2012–2031.
  • Osborne BG, Fearn T, Hindle PH. (1993). Practical NIR Spectroscopy: with applications in food and beverage analysis. Second edition. Longman Group UK Limited.
  • Palma M, Taylor LT. (1999). Extraction of polyphenolic compounds from grape seeds with near critical carbon dioxide. J Chromotogr A, 849, 117–124.
  • Pan L, Pawliszyn J. (1997). Derivatization/Solid-Phase Micro extraction: New Approach to Polar Analytes. Anal Chem, 69, 196–205.
  • Pan X, Niu G, Liu H. (2003). Microwave-assisted extraction of tea polyphenols and tea caffeine from green tea leaves. Chem Eng Process, 42, 129–133.
  • Pan Y, Zhang L, Chen G. (2001). Separation and determination of protocatechuic aldehyde and protocatechuic acid in Salvia miltiorhiza by capillary electrophoresis with amperometric detection. Analyst, 126, 1519–1523.
  • Pazourek J, Gonzalez G, Revilla AL, Havel J. (2000). Separation of polyphenols in Canary Islands wine by capillary zone electrophoresis without preconcentration. J Chromatogr A, 874, 111–119.
  • Pekić B, Kovač V, Alonso E, Revilla E. (1998). Study of the extraction of proanthocyanidins from grape seeds. Food Chem, 61, 201–206.
  • Peng Y, Chu Q, Liu F, Ye J. (2004). Determination of Phenolic Constituents of Biological Interest in Red Wine by Capillary Electrophoresis with Electrochemical Detection. J Agric Food Chem, 52, 153–156.
  • Peng YY, Liu FH, Ye JN. (2005). Determination of Phenolic Acids and Flavones in Lonicera japonica Thumb. by Capillary Electrophoresis with Electrochemical Detection. Electroanalysis, 17, 356–362.
  • Pietta PG. (2000). Flavonoids as Antioxidants. J Nat Prod, 63, 1035–1042.
  • Pinelo M, Arnous A, Meyer AS. (2006). Upgrading of grape skins: significance of plant cell-wall structural components and extraction techniques for phenol release. Trends in Food Sci Tech, 17, 579–590.
  • Porter LW. (1989). In Harborne, JB, 1989. Ed. Methods in plant biochemistry, I: plant phenolics, London: Academic press: 389.
  • Potter DW, Pawliszyn J. (1994). Rapid determination of polyaromatic hydrocarbons and polychlorinated biphenyls in water using solid-phase microextraction and GC/MS. Environ Sci Technol, 28, 298–305.
  • Prodanov M, Garrido I, Vacas V, Lebrón-Aguila R, Dueñas M, Gómez-Cordovés C, Bartolome B. (2008). Ultrafiltration as alternative purification procedure for the characterization of low and high molecular-mass phenolics from almond skins. Analytica Chimica Acta, 609, 241–251.
  • Proestos C, Komaitis M. (2008). Application of microwave-assisted extraction to the fast extraction of plant phenolic compounds. LWT-Food Sci Tech, 41, 652–659.
  • Proestos C, Sereli D, Komaitis M. (2006). Determination of phenolic compounds in aromatic plants by RP-HPLC and GC-MS. Food Chem, 95, 44–52.
  • Pueyo IU, Calvoa MI. (2009). Assay conditions and validation of a new UV spectrophotometric method using microplates for the determination of polyphenol content. Fitoterapia, 80, 465–467.
  • Qu H, Madl RL, Takemoto DJ, Baybutt RC, Wang W. (2005). Lignans Are Involved in the Antitumor Activity of Wheat Bran in Colon Cancer SW480 Cells. J Nutr, 135, 598–602.
  • Ramachandra G, Virupaksha TK, Shadaksharaswamy M. (1977). Relationship between tannin levels and in-vitro protein digestibility in finger millet (Eleusine coracana Gaertn). J Agric Food Chem, 25, 1101–1104.
  • Rasooly A. (2001). Surface plasmon resonance analysis of Staphylococcal enterotoxin B in food. Food Protectants, 64, 37–43.
  • Renard CMGC, Baron A, Guyot S, Drilleau JF. (2001). Interactions between apple cell walls and native apple polyphenol: quantification and some consequences. Inter J Biol Macromol, 29, 115–125.
  • Renault JH, Ghédira K, Thépenier P, Lavaud C, Zèches-Hanrot M, Le Men-Olivier L. (1997). Dammarane saponins from Zizyphus lotus. Phytochemistry, 44, 1321–1327.
  • Rice-Evans CA, Miller NJ, Paganga G. (1996). Structure-antioxidant activity relationships of flavonoids and phenolic acids. Free Radic Biol Med, 20, 933–956.
  • Richter BE, Jones BA, Ezzell JL, Porter NL, Avdalovic N, Pohl C. (1996). Accelerated solvent extraction: A technique for sample preparation. Anal Chem, 68, 1033−1039.
  • Rodriguez-Saona LE, Fredrick S, Michael A, McLaughlin, Elizabeth M. (2001). Rapid analysis of sugars in fruit juices by FT-NIR spectroscopy. Carbohydrate Research, 336, 63–74.
  • Romani A, Minunni M, Mulinacci N, Pinelli P, Vincieri FF, Carlo MD, Mascini M. (2000). Comparison among differential pulse voltammetry, amperometric biosensor and HPLC/DAD analysis for polyphenols determination. J Agric Food Chem, 48, 1197– 1203.
  • Ryan D, Robar Ds K, Enzier P, Antolovich M. (1999). Applications of mass spectrometry to plant phenols. Trends Anal Chem, 18, 362–372.
  • Salah N, Miller NJ, Paganga G, Tijburg L, Bolwell GP, Rice-Evans C. (1995). Polyphenolic Flavanols as Scavengers of Aqueous Phase Radicals and as Chain-Breaking Antioxidants. Arch Biochem Biophy, 322, 339–346.
  • Santana CM, Ferrera ZS, Padrón MET, Rodríguez JJS. (2009). Methodologies for the extraction of phenolic compounds from environmental samples: New Approaches. Molecules, 14, 298–320.
  • Scheper T, Hitzmann B, Stärk E, Ulber R, Faurie R, Sosnitza P, Reardon KF. (1999). Bioanalytics: detailed insight into bioprocesses. Anal Chim Acta, 400, 121–134.
  • Schulz H, Engelhardt UH, Wengent A, Drews HH, Lapczynski S. (1999). Application of NIRS to the simultaneous prediction alkaloids and previous termphenolic substance in green tea leaves. J Agric Food Chem, 47, 5064–5067.
  • Sermento LAV, Machado RAF, Petrus JCC, Tamanini TR, Bolzan A. (2008). Extraction of polyphenols from cocoa seeds and concentration through polymeric membranes. The J Supercriti Fluids, 45, 64–69.
  • Shadkami F, Sandra Estevez, Robert Helleur. (2009). Analysis of catechins and condensed tannins by thermally assisted hydrolysis/methylation-GC/MS and by a novel two step methylation. J Anal Applied Pyrolysis, 85, 54–65.
  • Shahidi F, Naczk M. (1995). Food phenolics: Sources, chemistry, effects, and applications. Technnomic publishing Co. Lancaster, PA.
  • Shahidi F, Wanasundara PKJPD. (1992). Phenolic antioxidants. Crit Rev Food Sci Nutri, 32, 67–103.
  • Shi P, He Q, Song Y, Qu H, Cheng Y. (2007). Characterization and identification of isomeric flavonoid O-diglycosides from genus Citrus in negative electrospray ionization by ion trap mass spectrometry and time-of-flight mass spectrometry. Analy Chimi Acta, 598, 110–118.
  • Sinelli N, Spinardi A, Egidio VD, Mignani I, Casiraghi E. (2008). Evaluation of quality and nutraceutical content of blueberries (Vaccinium corymbosum L.) by near and mid-infrared spectroscopy. Postharv Biol Tech, 50, 31–36.
  • Singh R, Akhtar N, Haqqi TM. (2010). Green tea polyphenol epigallocatechi3-gallate: Inflammation and arthritis. Life Sci, 86, 907–918.
  • Sondheimer E, Kertesz Z. (1948). Anthocyanin Pigments. Anal Chem, 20, 245–248.
  • Sørensen HR, Pedersen S, Anders VN, Meyer AS. (2005). Efficiencies of designed enzyme combinations in releasing arabinose and xylose from wheat arabinoxylan in an industrial ethanol fermentation residue. Enzy Micro Tech, 36, 773–784.
  • Sripriya G, Chandrashekaran K, Murty VS, Chandra TS. (1996). ESR spectroscopic studies on free radical quenching action of finger millet (Eleusine coracana). Food Chem, 57, 537–540.
  • Stalikas CD. (2007). Extraction, separation, and detection methods for phenolic acids and flavonoids. J Separa Sci, 30, 3268–3295.
  • Stevanato R, Fabris S, Bertelle M, Gregoris E, Momo F. (2009). Phenolic content and antioxidant properties of fermenting musts and fruit and vegetable fresh juices. Acta Alimentaria, 38, 193–203.
  • Strack D, Wray V. (1994). The anthocyanins. In The Flavonoids: Advances in Research Since1986. (Harborne JB., ed.). Chapman and Hall, London.
  • Sun T, Ho C. (2005). Antioxidant activities of buckwheat extracts. Food Chem, 90, 743–749.
  • Swain T, Hillis WE. (1959). The phenolic constituents of Prunus domestica. I. - The quantitative analysis of phenolic constituents. J Sci Food Agric, 10, 63–68.
  • Tagliazucchi V, Verzelloni E, Bertolini D, Angela C. (2010). In vitro bio-accessibility and antioxidant activity of grape polyphenols. Food Chem, 120, 599–606.
  • Tasioula-Margari M, Okogeri O. (2001). Simultaneous determination of phenolic compounds and tocopherols in virgin olive oil using HPLC and UV detection. Food Chem, 74, 377–383.
  • Terao J. (2008). Highlight on polyphenols and health. Arch Biochem Biophy, 476, 101–105.
  • Termentzi A, Kefalas P, Kokkalou E. (2008). LC–DAD–MS (ESI+) analysis of the phenolic content of Sorbus domestica fruits in relation to their maturity stage. Food Chem, 106, 1234–1245.
  • Thurbide KB, Hughes DM. (2000). A Rapid Method for Determining the Extractives Content of Wood Pulp. Indus Eng Chem Res, 39, 3112– 3115.
  • Tian S, Nakamura K, Kayahara H. (2004). Analysis of phenolic compounds in white rice, brown rice and germinated brown rice. J Agric Food Chem, 52, 4808–4813.
  • Tothill IE. (2001). Biosensors developments and potential applications in the agricultural diagnosis sector. Comput Electr Agric, 30, 205–218.
  • Tsuda T, Ohshima K, Kawakishi S, Osawa T. (1994). Antioxidative pigments isolated from seeds of Phaseolus vulgaris L. J Agric Food Chem, 42, 248– 251.
  • Vaher M, Koel M. (2003). Separation of polyphenolic compounds extracted from plant matrices using capillary electrophoresis. J Chromato A, 990, 225–230.
  • Van de Voort FR. (1992). Fourier transform infrared spectroscopy applied to food analysis. Food Res Inte, 25, 397–403.
  • Vanharanta M, Voutilainen S, Lakka TA, Lee AV, Adlercreutz H, Salonen HT. (1999). Risk of acute coronary events according to serum concentrations of enterolactone: a prospective population-based case-control study. Lancet, 354, 2112–2115.
  • Velasco-García MN, Mottram T. (2003). Biosensor technology addressing agricultural problems. Review paper. Biosys Eng, 84, 1–12.
  • Venkatesh MS, Raghavan GS. (2004). An overview of microwave processing and dielectric properties of agri-food materials. Biosys Eng, 88, 1–18.
  • Vinas P, Campillo N, Martinez-Castillo N, Hernandez-Cordoba. (2009). Solid-phase microextraction on-fiber derivatization for the analysis of some polyphenols in wine and grapes using gas chromatography-mass spectrometry. J Chromatography A, 1216, 1279–1284.
  • Virot M, Tomao V, Le Bourvellec C, Renard CM, Chemat F. (2009). Towards the industrial production of antioxidants from food processing by-products with ultrasound-assisted extraction. Ultrason. Sonochem, 17, 1066–1074.
  • Viswanath V, Urooj A, Malleshi NG. (2009). Evaluation of antioxidant and antimicrobial properties of finger millet polyphenols (Eleusine coracana). Food Chem, 114, 340–346.
  • Wang H, Cao G, Prior RL. (1997). Oxygen radical absorbing capacity of anthocyanins. J Agric Food chem, 45, 304–309.
  • Wang L, Weller CL. (2006). Recent advances in extraction of nutraceuticals from plants. Trends in Food Sci Tech, 17, 300–312.
  • Wang X, Geng Y, Li F, Shi X, Liu J. (2006). Large-scale separation of alkaloids from Corydalis decumbens by pH-zone-refining counter-current chromatography. J Chromatogr A, 111, 267–270.
  • Wang X, He Y, Qiana L. (2007). Determination of polyphenol components in herbal medicines by micellar electrokinetic capillary chromatography with Tween 20. Talanta, 74, 1–6.
  • Weisz GM, Kammerer RD, Carle R. (2009). Identification and quantification of phenolic compounds from sunflower (Helianthus annuus L.) kernels and shells by HPLC-DAD/ESI-MSn. Food Chem, 115, 758–765.
  • Wilson TC, Hagerman HE. (1990). Quantitative determination of ellagic acid. J Agric Food chem, 38, 1678–1683.
  • Wolfender JL, Rodriguez S, Hostettmann K. (1998). Liquid chromatography coupled to mass spectrometry and nuclear magnetic resonance spectroscopy for the screening of plant constituents. J Chromatography, 794, 299–316.
  • Wong RWK, Hägg U, Samaranayake L, Yuen MKC, Seneviratne CJ, Kao R. (2010). Antimicrobial activity of Chinese medicine herbs against common bacteria in oral biofilm- A pilot study. Inter J Oral and Maxillofacial Surgery, 39, 599–605.
  • Wu J, Hughes CS, Picard P, Letarte S, Gaudreault M, Lévesque JF, Nicoll-Griffith DA, Batema KP. (2007). High-throughput Cytochrome P450 Inhibition Assays Using Laser Diode Thermal Desorption-Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry. Anal Chem, 79, 4657–4665.
  • Wu J, Lin L, Chau F. (2001). Ultrasound-assisted extraction of ginseng saponins from ginseng roots and cultured ginseng cells. Ultrason Sonochem, 8, 347–352.
  • Yu J, Vasanthan T, Temelli F. (2001). Analysis of phenolic acids in barley by high-performance liquid chromatography. J Agric Food Chem, 49, 4352–4358
  • Zaporozhets OA, Krushynska OA, Lipkovska NA, Barvinchenko VN. (2004). A new test method for the evaluation of total antioxidant activity of herbal products. J Agric Food Chem, 52, 21–25.
  • Zeece MG. (1992). Capillary electrophoresis: A new analytical tool for food analysis. Trends Food Sci Tech, 6, 10–12.
  • Zhang MH, Luypaert J, Xu QS, Massart DL. (2004). Determination of total antioxidant capacity in green tea by NIRS and multivariate calibration. Talanta, 62, 25–35.
  • Zheng HZ, Lee HR, Lee SH, Kim CS, Chung SK. (2008). Pectinase assisted extraction of polyphenol from apple pomace. Chinese J Anal Chem, 36, 306–310.
  • Zhishen J, Mengcheng T, Jianming W. (1999). The determination of flavonoid contents in mulberry and their scavenging effects on superoxide radicals. Food Chem, 64, 555–559.
  • Žiaková A, Branšteterová E. (2002). Application of different preparation techniques for extraction of phenolic antioxidants from lemon balm (Melissa officinalis) before HPLC analysis. J Liquid Chromatogr RT, 25, 3017– 3032.

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