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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 21
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Original Articles

A Rapid and Convenient Synthesis of 1,1-Diacetates from Aldehydes and Acetic Anhydride Catalyzed by PVC-FeCl3 Catalyst

Yi-Qun Li Department of Chemistry, Jinan University, Guangzhou, 510632, P R China
Pages 3913-3917 | Accepted 21 Dec 1999, Published online: 04 Dec 2007

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Sedigheh Pargaleh Brojeni, Mojtaba Baghernejad, Dariush Saberi & Khodabakhsh Niknam. (2013) Silica immobilized sulfuric acid ([3-(propyl)sulfanyl]propyl]ester and N-propylsulfamic acid as recyclable catalysts for chemoselective synthesis of 1,1-diacetates. Green Chemistry Letters and Reviews 6:1, pages 69-75.
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Mohammad Reza Nabid, Seyed Jamal Tabatabaei Rezaei & Mahvash Abedi. (2010) Conjugate Polymer-Supported Acid Catalysts: An Efficient and Reusable Catalyst for the Synthesis of Geminal Diacetates (Acylals) Under Solvent-Free Conditions. Synthetic Communications 41:2, pages 191-199.
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Yurngdong Jahng & MotiurA. F. M. Rahman. (2006) Simple Synthesis of Geminal Diacetates (Acylals) of Aromatic Aldehydes. Synthetic Communications 36:9, pages 1213-1220.
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Hossein Eshghi & Zinat Gordi. (2004) PHOSPHORUS PENTOXIDE-MONTMORILLONITE K-10 AS CATALYST FOR THE PREPARATION OF 1,1-DIACETATES UNDER SOLVENT-FREE CONDITIONS. Phosphorus, Sulfur, and Silicon and the Related Elements 179:7, pages 1341-1346.
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Articles from other publishers (21)

Sobhan Rezayati & Ali Ramazani. (2020) Metal-based Lewis acid catalysts for conversion of a variety of aldehydes with acetic anhydride to gem 1,1-diacetates. Research on Chemical Intermediates 46:7, pages 3757-3799.
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Ali Rahmatpour & Sara Mohammadian. (2013) Polystyrene-supported TiCl4 as a novel, efficient and reusable polymeric Lewis acid catalyst for the chemoselective synthesis and deprotection of 1,1-diacetates under eco-friendly conditions. Comptes Rendus Chimie 16:10, pages 912-919.
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Da-He Fan, Hui Wang, Xing-Xing Mao & Yong-Miao Shen. (2010) An Efficient and Chemoselective Procedure for Acylal Synthesis. Molecules 15:9, pages 6493-6501.
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Giovanni Sartori & Raimondo Maggi. (2010) Update 1 of: Protection (and Deprotection) of Functional Groups in Organic Synthesis by Heterogeneous Catalysis. Chemical Reviews 110:3.
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Ajayan Vinu, Josena Justus, Veerappan Vaithilingam Balasubramanian, Shivappa Basappa Halligudi, Katsuhiko Ariga & Toshiyuki Mori. (2008) Synthesis of Fructone and Acylal Using Hexagonally Ordered Mesoporous Aluminosilicate Catalyst. Collection of Czechoslovak Chemical Communications 73:8-9, pages 1112-1124.
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Liang Yin, Zhan-Hui Zhang & Yong-Mei Wang. (2007) A stable intermediate: a new insight into the mechanism of Lewis acids-promoted formation of acylals from aldehydes. Tetrahedron Letters 48:17, pages 3119-3122.
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Motiur A. F. M. Rahman & Yurngdong Jahng. (2007) Preparation of Geminal Diacylates (Acylals) of Aldehydes – Scope and Reactivity of Aldehydes with Acid Anhydrides. European Journal of Organic Chemistry 2007:2, pages 379-383.
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Jianmin Wang, Liang Yan, Guang Qian, Keli Yang, Haitao Liu & Xiaolai Wang. (2006) Heteropolyacid encapsulated into mesoporous silica framework for an efficient preparation of 1,1-diacetates from aldehydes under a solvent-free condition. Tetrahedron Letters 47:47, pages 8309-8312.
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Vinod T. Kamble, Vasant S. Jamode, Neeta S. Joshi, Ankush V. Biradar & Rameshchandra Y. Deshmukh. (2006) An efficient method for the synthesis of acylals from aldehydes using silica-supported perchloric acid (HClO4–SiO2). Tetrahedron Letters 47:31, pages 5573-5576.
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Peipei Sun & Zhixin Hu. (2019) A simple and efficient method for the synthesis of gem-diacetates from aldehydes and ketones catalysed by gallium triiodide. Journal of Chemical Research 2005:10, pages 659-660.
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Masoud Salavati-Niasari & Samansa Hydarzadeh. (2005) An effective method for the selective synthesis of geminal diacetates (acylals) from aromatic aldehydes using alumina-supported InCl3. Journal of Molecular Catalysis A: Chemical 237:1-2, pages 254-258.
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Weike Su & Jin Can. (2019) Zn(OTf) 2 .6H 2 O catalysed acylation of aldehydes: Preparation of 1,1-diacetates and α-chloroalkyl esters . Journal of Chemical Research 2005:2, pages 88-90.
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István Ledneczki, Mária Darányi, Ferenc Fülöp & Árpád Molnár. (2005) SAC-13 silica nanocomposite solid acid catalyst in organic synthesis. Catalysis Today 100:3-4, pages 437-440.
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Hossein Eshghi & Parvaneh Shafieyoon. (2005) P 2 O 5 /SiO 2 as an Efficient Reagent for Selective Deprotection of 1,1-Diacetates under Solvent-Free Conditions . Journal of the Chinese Chemical Society 52:1, pages 155-157.
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Veerababurao Kavala & Bhisma�K. Patel. (2005) Reinvestigation of the Mechanism ofgem-Diacylation: Chemoselective Conversion of Aldehydes to Variousgem-Diacylates and Their Cleavage under Acidic and Basic Conditions. European Journal of Organic Chemistry 2005:2, pages 441-451.
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Giovanni Sartori, Roberto Ballini, Franca Bigi, Giovanna Bosica, Raimondo Maggi & Paolo Righi. (2003) Protection (and Deprotection) of Functional Groups in Organic Synthesis by Heterogeneous Catalysis. Chemical Reviews 104:1, pages 199-250.
Crossref
G Smitha & Ch.Sanjeeva Reddy. (2003) A facile and efficient ZrCl 4 catalyzed conversion of aldehydes to geminal-diacetates and dipivalates and their cleavage. Tetrahedron 59:48, pages 9571-9576.
Crossref
Gustavo P. Romanelli, Horacio J. Thomas, Graciela T. Baronetti & Juan C. Autino. (2003) Solvent-free catalytic preparation of 1,1-diacetates from aldehydes using a Wells–Dawson acid (H6P2W18O62·24H2O). Tetrahedron Letters 44:6, pages 1301-1303.
Crossref
Xinying Zhang, Lingjun Li & Guisheng Zhang. (2003) An efficient and green procedure for the preparation of acylals from aldehydes catalyzed by Fe 2 (SO 4 ) 3 ·xH 2 O . Green Chem. 5:5, pages 646-648.
Crossref
Marc D Carrigan, Kyle J Eash, Matthew C Oswald & Ram S Mohan. (2001) An efficient method for the chemoselective synthesis of acylals from aromatic aldehydes using bismuth triflate. Tetrahedron Letters 42:46, pages 8133-8135.
Crossref
Yi‐Qun Li. (2010) ChemInform Abstract: A Rapid and Convenient Synthesis of 1,1‐Diacetates from Aldehydes and Acetic Anhydride Catalyzed by PVC—FeCl 3 Catalyst. . ChemInform 32:3.
Crossref

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