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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 8
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Original Articles

Facile Method for Trimethylsilylation of Alcohols using Hexamethyldisilazane and Ammonium Thiocyanate under Neutral Conditions

Vrushali H. Jadhav Garware Research Centre, Department of Chemistry, University of Pune, Pune, India
,
K. S. Ajish Kumar Garware Research Centre, Department of Chemistry, University of Pune, Pune, India
,
Vinod D. Chaudhari Garware Research Centre, Department of Chemistry, University of Pune, Pune, India
&
Dilip D. Dhavale Garware Research Centre, Department of Chemistry, University of Pune, Pune, IndiaCorrespondence[email protected]
Pages 1363-1370 | Received 22 Sep 2006, Published online: 13 Apr 2007

Citations (15)

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Behzad Zeynizadeh & Serve Sorkhabi. (2018) Fast and efficient method for Silylation of alcohols and phenols with HMDS in the presence of bis-thiourea complexes of cobalt, nickel, copper and zinc chlorides. Phosphorus, Sulfur, and Silicon and the Related Elements 193:3, pages 127-135.
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Jun-Tao Hou, Hong-Li Chen & Zhan-Hui Zhang. (2010) Rapid and Efficient Trimethylsilyl Protection of Hydroxyl Groups Catalyzed by Niobium(V) Chloride. Phosphorus, Sulfur, and Silicon and the Related Elements 186:1, pages 88-93.
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Amin Rostami, Firoz Ahmad-Jangi, Mohammad Rezgar Zarebin & Jamal Akradi. (2010) Green and Efficient Procedure for the Trimethylsilylation of Hydroxy Groups and Their Regeneration Using Sulfamic Acid as Recyclable Catalyst. Synthetic Communications 40:10, pages 1500-1507.
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F. Shirini, G.H. Imanzadeh, A.R. Mousazadeh, I. Mohammadpoor-Baltork, A.R. Aliakbar & M. Abedini. (2010) (PhCH2PPh3)+Br3 −: A Versatile Reagent for the Preparation, Deprotection, and Oxidation of Trimethylsilyl Ethers. Phosphorus, Sulfur, and Silicon and the Related Elements 185:3, pages 641-646.
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Ramin Ghorbani-Vaghei & Seyedeh Mina Malaekehpoor. (2010) Silylation of Alcohols and Phenols Using Hexamethyldisilazane Catalyzed by N,N’-Diiodo-N,N’-1,2-ethanediyl Bis(p-toluenesulfonamide) Under Solvent-Free and Microwave Conditions. Phosphorus, Sulfur, and Silicon and the Related Elements 185:3, pages 582-587.
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Articles from other publishers (10)

Krzysztof Kuciński, Hanna Stachowiak, Dariusz Lewandowski, Marcin Gruszczyński, Paulina Lampasiak & Grzegorz Hreczycho. (2022) A review of the R3Si–NH–SiR3–type disilazanes: From synthesis to applications. Journal of Organometallic Chemistry 961, pages 122127.
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Mohammad Galehassadi & Samira Pourreza. (2018) Base and Catalyst-Free Preparation of Silyl Ethers in the Choline Chloride/Urea Deep Eutectic Solvent (DES). Journal of Inorganic and Organometallic Polymers and Materials 29:2, pages 541-549.
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Veronika Nagy, Attila Agócs, József Deli, Gergely Gulyás-Fekete, Tünde-Zita Illyés, Tibor Kurtán, Erika Turcsi, Szabolcs Béni, Miklós Dékány, Andreas Ballot & Gábor Vasas. (2018) Carotenoid glycoside isolated and identified from cyanobacterium Cylindrospermopsis raciborskii. Journal of Food Composition and Analysis 65, pages 6-10.
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Marjan Jereb. (2012) Highly atom economical uncatalysed and I2-catalysed silylation of phenols, alcohols and carbohydrates, using HMDS under solvent-free reaction conditions (SFRC). Tetrahedron 68:20, pages 3861-3867.
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Arash Ghorbani-Choghamarani, Hamid Goudarziafshar & Parisa Zamani. (2011) Polyvinylpolypyrrolidoniume tribromide as new and metal-free catalyst for the formylation and trimethylsilylation of hydroxyl group. Chinese Chemical Letters.
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Arash GHORBANI-CHOGHAMARANI & Masoomeh NOROUZI. (2011) Protection of Hydroxyl Groups as a Trimethylsilyl Ether by 1,1,1,3,3,3-Hexamethyldisilazane Promoted by Aspartic Acid as an Efficient Organocatalyst. Chinese Journal of Catalysis 32:3-4, pages 595-598.
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Arash Ghorbani-Choghamarani, Mohammad Ali Zolfigol, Maryam Hajjami, Khorshid Darvishi & Laleh Gholamnia. (2010) Protection of hydroxy groups as trimethylsilyl ethers using 1,1,1,3,3,3-hexamethyldisilazane (HMDS) catalyzed by poly(4-vinylpyridinium tribromide). Collection of Czechoslovak Chemical Communications 75:5, pages 607-615.
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Arash Ghorbani‐Choghamarani, Mohammad Ali Zolfigol, Maryam Hajjami & Shila Jafari. (2013) Trimethylsilylation of Hydroxyl Group with 1,1,1,3,3,3‐Hexamethyldisilazane (HMDS) Catalyzed by Tribromomelamine (TBM). Journal of the Chinese Chemical Society 55:6, pages 1208-1213.
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Mohammad M. Mojtahedi, M. Saeed Abaee & Mohammad Eghtedari. (2008) Superparamagnetic iron oxide as an efficient and recoverable catalyst for rapid and selective trimethylsilyl protection of hydroxyl groups. Applied Organometallic Chemistry 22:9, pages 529-532.
Crossref
Vrushali H. Jadhav, K. S. Ajish Kumar, Vinod D. Chaudhari & Dilip D. Dhavale. (2007) Facile Method for Trimethylsilylation of Alcohols Using Hexamethyldisilazane and Ammonium Thiocyanate under Neutral Conditions.. ChemInform 38:41.
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