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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 13
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Original Articles

Knoevenagel Condensation of Aromatic Aldehydes with Active Methylene Compounds using a Catalytic Amount of Iodine and K2CO3 at Room Temperature

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Pages 2209-2213 | Received 27 Sep 2006, Published online: 03 Jul 2007

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Read on this site (6)

Xiaoyu Zhang, Xiaoyan He & Sanhu Zhao. (2021) Preparation of a novel Fe3O4@SiO2@propyl@DBU magnetic core–shell nanocatalyst for Knoevenagel reaction in aqueous medium. Green Chemistry Letters and Reviews 14:1, pages 85-98.
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Sanhu Zhao, Dan Meng, Lingling Wei, Yongsheng Qiao & Fugui Xi. (2019) Novel DBU-based hydroxyl ionic liquid for efficient Knoevenagel reaction in water. Green Chemistry Letters and Reviews 12:3, pages 271-277.
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Faryal Chaudhry, Nadia Asif, Syed Salman Shafqat, Amir Azam Khan, Munawar Ali Munawar & Misbahul Ain Khan. (2016) Efficient ecofriendly synthesis of pyrazole acryloyl analogs by amino acid catalysis. Synthetic Communications 46:8, pages 701-709.
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M.B. Deshmukh, SureshS. Patil, S.D. Jadhav & P.B. Pawar. (2012) Green Approach for Knoevenagel Condensation of Aromatic Aldehydes with Active Methylene Group. Synthetic Communications 42:8, pages 1177-1183.
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Zhongqiang Zhou, Jiangyong Yuan & Rong Yang. (2009) Efficient Knoevenagel Condensation Catalyzed by 2-Hydroxyethylammonium Acetate Under Solvent-Free Conditions at Room Temperature. Synthetic Communications 39:11, pages 2001-2007.
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Articles from other publishers (32)

Nagaraj S. Naik, Swathi Divakar, Jyothi M. S., Srinivasa Budagumpi, R. Geetha Balakrishna & Mahesh Padaki. (2024) Biogenic derived egg shell and its derivatives as solid base heterogeneous catalysts for organic transformations: a comprehensive review. RSC Sustainability.
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Krishnappa B. Badiger & Kantharaju Kamanna. (2023) Microwave-accelerated Eco-friendly Performance of the Knoevenagel Condensation Reaction with Various Active Methylene Derivat-ives evaluation of Electrochemical Properties. Current Organocatalysis 10:2, pages 113-127.
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Ghobad Mansouri, Mino Abdizad, Amir Reza Abbasi & Sobhan Rezayati. (2022) Efficient and green one‐pot synthesis of Knoevenagel condensation catalyzed nano metal–organic frameworks in water. Applied Organometallic Chemistry 36:12.
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Sobhan Rezayati, Hamideh Haghighat & Ali Ramazani. (2022) Core/shell Nanostructure Fe3O4@SiO2@GPTMS/Schiff Base-Cu(II): A New and Recoverable Nanocatalyst for One-Pot Ecofriendly Synthesis of Knoevenagel Condensation and Polyhydroquinoline Derivatives. Silicon.
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Fatemeh Kalantari, Sobhan Rezayati, Ali Ramazani, Hamideh Aghahosseini, Katarzyna Ślepokura & Tadeusz Lis. (2022) Proline-Cu Complex Based 1,3,5-Triazine Coated on Fe 3 O 4 Magnetic Nanoparticles: A Nanocatalyst for the Knoevenagel Condensation of Aldehyde with Malononitrile . ACS Applied Nano Materials 5:2, pages 1783-1797.
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Jonas J. Koenig & Martin Breugst. 2021. Halogen Bonding in Solution. Halogen Bonding in Solution 237 268 .
Iqbal Azad, Tahmeena Khan, Rumana Ahmad, Azhar Kamal, Abdul Rahman Khan & Malik Nasibullah. (2021) A Simplistic Approach for Preparation of Alkylidenemalononitrile Derivatives: Characterization, In silico Studies, Quantum Chemical Evaluation, Molecular Docking, and In vitro Biological Activity Evaluation. Journal of Molecular Structure 1228, pages 129451.
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Suman Sangwan, Rajvir Singh, Susheel Gulati & Suprita Rana. (2021) Efficient and facile synthesis of pyrazoles using Guar-gum as organocatalyst and their in vitro herbicidal activity. Current Research in Green and Sustainable Chemistry 4, pages 100146.
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Ying Zhang, Hongsheng Lu, Baogang Wang, Na Wang & Dongfang Liu. (2020) pH-Responsive Non-Pickering Emulsion Stabilized by Dynamic Covalent Bond Surfactants and Nano-SiO 2 Particles . Langmuir 36:50, pages 15230-15239.
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Magda M.F. Ismail, Heba S.A. El-Zahabi, Rabab S. Ibrahim & Ahmed B.M. Mehany. (2020) Design and synthesis of novel tranilast analogs: Docking, antiproliferative evaluation and in-silico screening of TGFβR1 inhibitors. Bioorganic Chemistry 105, pages 104368.
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Robson Xavier Faria, Noemi de Jesus Hiller, Juliana Pimenta Salles, Jackson Antonio Lamounier Camargos Resende, Roberta Tosta Diogo, Natalia Lidmar von Ranke, Murilo Lamim Bello, Carlos Rangel Rodrigues, Helena Carla Castro & Daniela de Luna Martins. (2019) Arylboronic acids inhibit P2X7 receptor function and the acute inflammatory response. Journal of Bioenergetics and Biomembranes 51:4, pages 277-290.
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Martin Breugst & Daniel von der Heiden. (2018) Mechanisms in Iodine Catalysis. Chemistry – A European Journal 24:37, pages 9187-9199.
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Carmen A. Mak, Miquel A. Pericas & Eugenia Fagadar-Cosma. (2018) Functionalization of A3B-type porphyrin with Fe3O4 MNPs. Supramolecular assemblies, gas sensor and catalytic applications. Catalysis Today 306, pages 268-275.
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João Batista M. de Resende Filho, Gilvan P. Pires, João Marcos Gomes de Oliveira Ferreira, Ercules E. S. Teotonio & Juliana A. Vale. (2016) Knoevenagel Condensation of Aldehydes and Ketones with Malononitrile Catalyzed by Amine Compounds-Tethered Fe3O4@SiO2 Nanoparticles. Catalysis Letters 147:1, pages 167-180.
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SURESH PATIL, SWATI D JADHAV & M B DESHMUKH. (2013) Calcined eggshell (CES): An efficient natural catalyst for Knoevenagel condensation under aqueous condition. Journal of Chemical Sciences 125:4, pages 851-857.
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Brad Andersh, Elizabeth T. Nguyen, Ryan J. Van Hoveln, Dylan K. Kemmerer, David A. Baudo, Jessica A. Graves, Mollie E. Roark & Wayne B. Bosma. (2013) Investigation of the Mechanism for the Preparation of 6-Phenyl-2,4-dioxotetrahydropyrans by the Potassium Carbonate Promoted Condensation between Acetoacetate Esters and Benzaldehyde. The Journal of Organic Chemistry 78:9, pages 4563-4567.
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BANDITA DATTA & MOHAMED AFZAL PASHA. (2013) I2/K2CO3: An efficient catalyst for the synthesis of 5-aryl-2,6-dicyano-3-methylanilines. Journal of Chemical Sciences 125:2, pages 291-294.
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R. Motamedi. (2013) Solvent-free synthesis of novel 5-oxo-5H-chromeno[4,3-b]pyridine derivatives. Chemistry of Heterocyclic Compounds 48:12, pages 1839-1843.
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Sanhu Zhao, Xiaoju Wang & Liwei Zhang. (2013) Rapid and efficient Knoevenagel condensation catalyzed by a novel protic ionic liquid under ultrasonic irradiation. RSC Advances 3:29, pages 11691.
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Zeba N. Siddiqui, T. N. Mohammed Musthafa, Shagufta Praveen & Farheen Farooq. (2010) Zn(Proline)2-catalyzed Knoevenagel condensation under solvent-free/aqueous conditions and biological evaluation of products. Medicinal Chemistry Research 20:9, pages 1438-1444.
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Yi-Ming Ren & Chun Cai. (2011) The Michael Addition of Active Methylene Compounds to Chalcone Derivatives using a Catalytic Amount of Iodine and K 2 CO 3 at Room Temperature . Journal of Chemical Research 35:3, pages 176-178.
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Sadok LetaiefYun LiuChristian Detellier. (2011) Zirconium oxide nanoparticles coated on sepiolite by sol–gel process — Their application as a solvent-free catalyst for condensation reactions. Canadian Journal of Chemistry 89:3, pages 280-288.
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Marjan Jereb, Dejan Vražič & Marko Zupan. (2011) Iodine-catalyzed transformation of molecules containing oxygen functional groups. Tetrahedron 67:7, pages 1355-1387.
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Zhong-Xian Li, Xiao-Pei Liu, Zhen Qiu, Dan Xu & Xue-Jun Yu. (2011) An Efficient Iodine-Catalysed Knoevenagel Condensation Reaction in the Presence of Acetic Anhydride. Journal of Chemical Research 35:1, pages 35-36.
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Li-Yan Zeng & Chun Cai. (2009) Iodine Catalyzed One-Pot Multicomponent Synthesis of a Library of Compounds Containing Tetrazolo[1,5- a ]pyrimidine Core . Journal of Combinatorial Chemistry 12:1, pages 35-40.
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An-Guo Ying, Li-Min Wang, Le-Le Wang, Xin-Zhi Chen & Wei-Dong Ye. (2010) Green and Efficient Knoevenagel Condensation Catalysed by a DBU Based ionic Liquid in Water. Journal of Chemical Research 34:1, pages 30-33.
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Manas Chakrabarty, Ajanta Mukherji, Shiho Arima, Yoshihiro Harigaya & Guillaume Pilet. (2008) Expeditious reaction of ninhydrin with active methylene compounds on montmorillonite K10 clay. Monatshefte für Chemie - Chemical Monthly 140:2, pages 189-197.
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Manas Chakrabarty, Ratna Mukherjee, Shiho Arima & Yoshihiro Harigaya. (2009) Reaction of Isatins with Active Methylene Compounds on Neutral Alumina: Formation of Knoevenagel Condensates and Other Interesting Products. HETEROCYCLES 78:1, pages 139.
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Yi-Ming Ren & Chun Cai. (2008) Three-components condensation catalyzed by molecular iodine for the synthesis of 2,4,6-triarylpyridines and 5-unsubstituted-3,4-dihydropyrimidin-2(1H)-ones under solvent-free conditions. Monatshefte für Chemie - Chemical Monthly 140:1, pages 49-52.
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Yi-Ming Ren & Chun Cai. (2008) Convenient and efficient method for synthesis of substituted 2-amino-2-chromenes using catalytic amount of iodine and K2CO3 in aqueous medium. Catalysis Communications 9:6, pages 1017-1020.
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Yi-Ming Ren, Yi-Zhong Zhu & Chun Cai. (2008) Iodine/aqueous NH 4 OAc: An Improved Reaction System for Direct Oxidative Conversion of Aldehydes and Alcohols Into Nitriles . Journal of Chemical Research 2008:1, pages 18-19.
Crossref
Yi‐Ming Ren & Chun Cai. (2007) ChemInform Abstract: Knoevenagel Condensation of Aromatic Aldehydes with Active Methylene Compounds Using a Catalytic Amount of Iodine and K 2 CO 3 at Room Temperature. . ChemInform 39:1.
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