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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 15
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Original Articles

p-Toluene Sulfonic Acid–Catalyzed, Solvent-Free Synthesis of Symmetrical Bisamides by Reaction Between Aldehydes and Amides

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Pages 2209-2214 | Received 02 Jun 2009, Published online: 07 Jul 2010

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Read on this site (6)

Ahmad Reza Moosavi-Zare, Hamid Goudarziafshar, Zahra Jalilian & Zahra Hajilouie. (2022) The Synthesis of gem-Bisamides Using a Carbocationic Catalytic System in Neutral Media. Organic Preparations and Procedures International 54:5, pages 440-448.
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Gurusamy Ramachandran, Ramachandran Saraswathi, Mayilvasagam Kumarraja, Palsamy Govindaraj & Thirumeni Subramanian. (2018) Efficient synthesis of symmetrical bisamides catalyzed by reusable hydroxyapatite. Synthetic Communications 48:2, pages 216-222.
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Karuppaiah Selvakumar, Thangamariyappan Shanmugaprabha, Murugan Kumaresan & Ponnusamy Sami. (2017) One-pot multi-component synthesis of N,N′-alkylidene bisamides and imidazoles using heteropoly-11-tungsto-1-vanadophosphoric acid supported on natural clay as catalyst: A green approach. Synthetic Communications 47:22, pages 2115-2126.
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Behrooz Maleki, Farrokhzad Mohammadi Zonoz & Hossien Ali Akhlaghi. (2015) An Efficient Synthesis of Symmetrical N,N′-Alkylidene bis-Amides Catalyzed by a Heteropolyacid. Organic Preparations and Procedures International 47:5, pages 361-367.
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Mahmood Tajbakhsh, Rahman Hosseinzadeh, Heshmatollah Alinezhad & Parizad Rezaee. (2013) Efficient Synthesis of Symmetrical Bisamides from Aldehydes and Amides Catalyzed by Silica-Bonded S-Sulfonic Acid Nanoparticles. Synthetic Communications 43:17, pages 2370-2379.
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Articles from other publishers (34)

James Y. Becker. (2024) Anodic Oxidation of Aliphatic and Aromatic Amides, Bisamides and Related Derivatives. ChemElectroChem.
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Omkar Sharad Kamble, Rana Chatterjee, Shubhada Gad, Samarath Kansara, Sonal Ayakar, Amit Kumar Pandey & Rambabu Dandela. (2024) Solar-Assisted Green Synthesis, Molecular Docking, Antibacterial, and Cytotoxicity Studies of Symmetrical N, N’-Alkylidene Bisamides Bearing Lower E-Factors. American Journal of Heterocyclic Chemistry 10:1, pages 1-12.
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Jiaxu Fu, Yuandong Yue, Kejun Liu, Shuang Wang, Yiliang Zhang, Qing Su, Qiang Gu, Feng Lin & Yumin Zhang. (2022) PTSA-catalyzed selective synthesis and antibacterial evaluation of 1,2-disubstituted benzimidazoles. Molecular Diversity 27:2, pages 873-887.
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Hamdy Khamees Thabet, Mustafa Turki Ubeid, Mohamed Yousef Abu Shuheil & Mohd Imran. (2022) p-Toluene-sulfonic Acid-catalyzed One-pot, Three-component Synthesis of 4-(4-(Piperidin-1-yl)phenyl)-2-Thioxo-1,2,3,4Tetrahydro-5H-Chromeno[4,3-d]Pyrimidin-5-One. Oriental Journal Of Chemistry 38:2, pages 406-409.
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Hamid Goudarziafshar, Ahmad Reza Moosavi-Zare, Fatemeh Hosseinabadi & Zahra Jalilian. (2022) Nano-[Mn-PSMP]Cl2 as a new Schiff base complex and catalyst for the synthesis of N,N'-alkylidene bisamides. Research on Chemical Intermediates 48:4, pages 1423-1437.
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Xue-Jiao Lv, Yong-Chao Ming, Hui-Chun Wu & Yan-Kai Liu. (2021) Brønsted acid-catalyzed dynamic kinetic resolution of in situ formed acyclic N , O -hemiaminals: cascade synthesis of chiral cyclic N , O -aminals . Organic Chemistry Frontiers 8:22, pages 6309-6316.
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Pawan Kumar, Princy Gupta & Chandan Sharma. (2021) Surface modified novel magnetically tuned halloysite functionalized sulfonic acid: synthesis, characterization and catalytic activity. Catalysis Science & Technology 11:11, pages 3775-3786.
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Dalila Venzke, Tais Poletti, Bruno N. Rosa, Lucas M. Berneira, Nathalia P.K. de Lima, Tiago F. de Oliveira, Neftalí L.V. Carreño, Kristiane de C. Mariotti, Leonardo S. Duarte, Sabrina M. Nobre & Claudio M.P. Pereira. (2021) Preparation of fluorescent bisamides: A new class of fingermarks developers. Chemical Data Collections 33, pages 100680.
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Rajesh Nandi, Prakash K. Mandal, Anirban Kayet, Tamalika Bhattachariya, Sukla Ghosh & Dilip K. Maiti. (2020) Benzimidates as gem -Diamidation and Amidoindolyzation Cascade Synthons with a Hydrated Ni II Catalyst . Organic Letters 22:9, pages 3474-3478.
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Tatiana Golub, Gui-yuan Dou, Cheng-chu Zeng & James Y. Becker. (2019) One-Pot Anodic Conversion of Symmetrical Bisamides of Ethylene Diamine to Unsymmetrical gem -Bisamides of Methylene Diamine . Organic Letters 21:19, pages 7961-7964.
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Hamid Reza Saadati-Moshtaghin. (2019) Immobilization of dihydrogen phosphate onto rice husk ash as a highly efficient and green catalyst for the synthesis of symmetrical N,N′-alkylidene bisamides. Research on Chemical Intermediates 45:5, pages 3077-3087.
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Abdolkarim Zare, Masoud Sadeghi-Takallo, Mostafa Karami & Alireza Kohzadian. (2019) Synthesis, characterization and application of nano-N,N,N′,N′-tetramethyl-N-(silica-n-propyl)-N′-sulfo-ethane-1,2-diaminium chloride as a highly efficient catalyst for the preparation of N,N′-alkylidene bisamides. Research on Chemical Intermediates 45:5, pages 2999-3018.
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Abdolkarim Zare, Roghayyeh Khanivar, Navid Irannejad‐Gheshlaghchaei & M. Hassan Beyzavi. (2019) A Nanostructured Organic‐Inorganic Hybrid Material: Preparation, Characterization and Catalytic Performance for the Synthesis of N , N ′‐Alkylidene Bisamides . ChemistrySelect 4:13, pages 3953-3960.
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Yue CaoDongheng ZhouYongmin Ma. (2019) Selectfluor-mediated oxidative methylenation of amide with N , N -dimethylpropanamide for N , N ′-methylenebisamide synthesis . Canadian Journal of Chemistry 97:1, pages 37-41.
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Bagher Mohammadi & Bahareh Rezaei Khorrami. (2017) A simple and one-pot multi-component reaction to the synthesis of methylenebisamides. Monatshefte für Chemie - Chemical Monthly 149:6, pages 1089-1092.
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Hamid Reza Saadati-Moshtaghin, Farrokhzad Mohammadi Zonoz & Mostafa M. Amini. (2018) Synthesis and characterization of ZnO incorporated magnetically recoverable KIT-6 as a novel and efficient catalyst in the preparation of symmetrical N, N′-alkylidene bisamides. Journal of Solid State Chemistry 260, pages 16-22.
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Richard C. LarockRichard C. Larock & Tuanli Yao. 2018. Comprehensive Organic Transformations. Comprehensive Organic Transformations 1 85 .
Alexandre F. Trindade & Jeffrey W. Bode. (2016) Irreversible Conjugation of Aldehydes in Water To Form Stable 1,2,4-Oxadiazinan-5-ones. Organic Letters 18:17, pages 4210-4213.
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Raziyeh Pyrzehi-Bakhshani & Alireza Hassanabadi. (2016) Ultrasound-Promoted Synthesis of Symmetrical Bisamides by Reaction between Aromatic Aldehydes and Amides Catalysed by P-Toluenesulfonic Acid. Journal of Chemical Research 40:1, pages 35-37.
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R. Tayebee, B. Maleki, F. M. Zonoz, R. M. Kakhki & T. Kunani. (2016) Mild, efficient, and environmentally friendly synthesis of symmetrical N,N′-alkylidenebisamides under solvent-free conditions catalyzed by H 7 [(P 2 W 17 O 61 )Fe III (H 2 O)] . RSC Advances 6:25, pages 20687-20694.
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Najmedin Azizi & Masoumeh Alipour. (2015) Eco-efficiency and scalable synthesis of bisamides in deep eutectic solvent. Journal of Molecular Liquids 206, pages 268-271.
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Jeffrey W. Bode, Gabriel Schäfer & Lukas Leu. (2015) Synthesis of Unsymmetrical, gem-Disubstituted Bisamides. HETEROCYCLES 90:2, pages 1375.
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Behrooz Maleki & Mehdi Baghayeri. (2015) Synthesis of symmetrical N,N′-alkylidene bis-amides catalyzed by silica coated magnetic NiFe 2 O 4 nanoparticle supported polyphosphoric acid (NiFe 2 O 4 @SiO 2 -PPA) and its application toward silver nanoparticle synthesis for electrochemical detection of glucose . RSC Advances 5:97, pages 79746-79758.
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Manmeet Kour & Satya Paul. (2015) Sulfonated carbon/nano-metal oxide composites: a novel and recyclable solid acid catalyst for organic synthesis in benign reaction media. New Journal of Chemistry 39:8, pages 6338-6350.
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Balu L. Gadilohar, Haribhau S. Kumbhar & Ganapati S. Shankarling. (2015) Choline peroxydisulfate oxidizing Bio-TSIL: triple role player in the one-pot synthesis of Betti bases and gem-bisamides from aryl alcohols under solvent-free conditions. New Journal of Chemistry 39:6, pages 4647-4657.
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Mohammad Reza Mohammad Shafiee. (2014) One-pot preparation of N,N′-alkylidene bisamide derivatives catalyzed by silica supported polyphosphoric acid (SiO2-PPA). Journal of Saudi Chemical Society 18:2, pages 115-119.
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Arash Mouradzadegun, Somayeh Elahi & Fatemeh Abadast. (2014) Synthesis of a 3D-network polymer supported Bronsted acid ionic liquid based on calix[4]resorcinarene via two post-functionalization steps: a highly efficient and recyclable acid catalyst for the preparation of symmetrical bisamides. RSC Adv. 4:59, pages 31239-31248.
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Yi Zhang, Zhihao Zhong, Yingmei Han, Ruirui Han & Xu Cheng. (2013) A convenient synthesis of bisamides with BF3 etherate as catalyst. Tetrahedron 69:52, pages 11080-11083.
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BIBI FATEMEH MIRJALILI & MOHAMMAD ALI MIRHOSEINI. (2014) Tandem synthesis of N,N′-alkylidenebisamides promoted by nano-SnCl4.SiO2. Journal of Chemical Sciences 125:6, pages 1481-1486.
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Zahed Karimi-Jaberi & Baharak Pooladian. (2012) A mild, efficient, and environmentally friendly synthesis of N,N′-arylidene bisamides using B(HSO4)3 under solvent-free conditions. Monatshefte für Chemie - Chemical Monthly 144:5, pages 659-663.
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Hongshe Wang & June Zeng. (2012) An Efficient Synthesis of Symmetrical Bisamides Catalysed by Molecular iodine under Neutral Conditions. Journal of Chemical Research 36:8, pages 447-449.
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Mohammad Reza Mohammad Shafiee. (2011) Silica-supported barium chloride (SiO 2 –BaCl 2 ) — Efficient and heterogeneous catalyst for the environmentally friendly preparation of N , N ′-alkylidene bisamides under solvent-free conditions . Canadian Journal of Chemistry 89:5, pages 555-561.
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Mohammad Anary‐Abbasinejad, Mohammad H. Mosslemin, Alireza Hassanabadi & Safiyeh Tajik Safa. (2010) ChemInform Abstract: p‐Toluene Sulfonic Acid‐Catalyzed Solvent‐Free Synthesis of Symmetrical Bisamides by Reaction Between Aldehydes and Amides.. ChemInform 41:51.
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Mohammad Anary-Abbasinejad, Alireza Hassanabadi & Motahareh Heidari-Barfeh. (2010) p -Toluene Sulfonic Acid-Catalysed Microwave Synthesis of Symmetrical Bisamides by Reaction between Aromatic Aldehydes and Amides . Journal of Chemical Research 34:8, pages 478-480.
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