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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 4
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Original Articles

ON the silylation of diarylcarbinols

, , , &
Pages 707-713 | Received 05 Jul 1995, Published online: 21 Nov 2007

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Read on this site (18)

Razieh Oladee, Daryoush Zareyee & Mohammad A. Khalilzadeh. (2021) KF/clinoptilolite NPs: An efficient and heterogeneous catalyst for chemoselective silylation of alcohols and phenols. Phosphorus, Sulfur, and Silicon and the Related Elements 196:8, pages 731-737.
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Behzad Zeynizadeh & Serve Sorkhabi. (2018) Fast and efficient method for Silylation of alcohols and phenols with HMDS in the presence of bis-thiourea complexes of cobalt, nickel, copper and zinc chlorides. Phosphorus, Sulfur, and Silicon and the Related Elements 193:3, pages 127-135.
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Yulia M. Sadykova, Larisa M. Sadikova, Alena V. Zalaltdinova, Natalia V. Dalmatova, Alexander R. Burilov, Michael A. Pudovik & Oleg G. Sinyashin. (2016) Phosphorus-containing bicyclic phosphonates in silylation and acetylation reactions. Phosphorus, Sulfur, and Silicon and the Related Elements 191:3, pages 493-495.
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F. Shirini & M. Mashhadi-Nejad. (2012) Cu(NO3)2 · 3 H2O as an Efficient Reagent for the Chemoselective Trimethylsilylation of Primary Alcohols and Oxidation of Trimethylsilyl Ethers. Phosphorus, Sulfur, and Silicon and the Related Elements 187:3, pages 376-381.
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Ramin Ghorbani-Vaghei & Seyedeh Mina Malaekehpoor. (2010) Silylation of Alcohols and Phenols Using Hexamethyldisilazane Catalyzed by N,N’-Diiodo-N,N’-1,2-ethanediyl Bis(p-toluenesulfonamide) Under Solvent-Free and Microwave Conditions. Phosphorus, Sulfur, and Silicon and the Related Elements 185:3, pages 582-587.
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Batool Akhlaghinia. (2009) Novel and Highly Efficient Protection of Aliphatic Alcohols and Phenols with Hexamethyldisilazane in the Presence of La(NO3)3·6 H2O. Phosphorus, Sulfur, and Silicon and the Related Elements 184:10, pages 2530-2535.
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F. Shirini, K. Marjani, H. Taherpour Nahzomi & M.A. Zolfigol. (2007) Silica Triflate as a New, Efficient, and Reusable Reagent for the Chemoselective Silylation of Alcohols and Phenols and Deprotection of Silyl Ethers. Phosphorus, Sulfur, and Silicon and the Related Elements 183:1, pages 168-177.
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Hossein Ghafuri, Bagher Eftekhari-Sis & MohammedM. Hashemi. (2007) Silica Sulfuric Acid as a Reusable Catalyst for Efficient and Simple Silylation of Hydroxyl Groups Using Hexamethyldisilazane (HMDS). Phosphorus, Sulfur, and Silicon and the Related Elements 182:7, pages 1645-1651.
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Ardeshir Khazaei, Amin Rostami, Sadegh Rahmati & Marjan Mahboubifar. (2007) N,N′-Dibromo-N,N′-1,2-ethanediylbis (Benzene Sulfonamide) as a Novel N-Bromo Reagent–Catalyzed Trimethylsilylation of Alcohols and Phenol With Hexamethyldisilazane in Both Solution and Solvent-Free Conditions. Phosphorus, Sulfur, and Silicon and the Related Elements 182:3, pages 537-544.
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Vrushali H. Jadhav, K. S. Ajish Kumar, Vinod D. Chaudhari & Dilip D. Dhavale. (2007) Facile Method for Trimethylsilylation of Alcohols using Hexamethyldisilazane and Ammonium Thiocyanate under Neutral Conditions. Synthetic Communications 37:8, pages 1363-1370.
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MahidehS. Khalili, Hossein Ghafuri, Samaneh Mojahedi-Jahromi & MohammedM. Hashemi. (2007) Simple and Practical Protocol for the Silylation of Phenol Derivatives Using Reusable NaHSO4 Dispread on Silica Gel Under Neutral Conditions. Phosphorus, Sulfur, and Silicon and the Related Elements 182:1, pages 175-179.
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Farhad Shirini & Esmail Mollarazi. (2006) Trimethylsilylation of Alcohols and Phenols using KBr as an Efficient and Reusable Catalyst. Synthetic Communications 36:8, pages 1109-1115.
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Farhad Shirini, Mohammad Ali Zolfigol & Masoumeh Abedini. (2005) Al(HSO4)3 as an Efficient Reagent for the Selective Trimethylsilylation of Primary Alcohols Under Solvent-Free Conditions. Phosphorus, Sulfur, and Silicon and the Related Elements 180:10, pages 2299-2302.
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Batool Akhlaghinia, Mozafar Asadi, Elham Safaee & Mozhgan Heydarpoor. (2004) HEXAMETHYLDISILAZANE IN THE PRESENCE OF N,N′,N″,N‴-TETRAMETHYLTETRA-2,3-PYRIDINOPORPHYRAZINATO COPPER (II) IS A NEW, MILD AND HIGHLY EFFICIENT REAGENT FOR SILYLATION OF ALCOHOLS AND PHENOLS. Phosphorus, Sulfur, and Silicon and the Related Elements 179:10, pages 2099-2104.
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Farhad Shirini, Mohammad Ali Zolfigol & Kamal Mohammadi. (2003) A Mild and Efficient Method for Chemoselective Silylation of Alcohols Using Hexamethyldisilazane in the Presence of Silica Chloride. Phosphorus, Sulfur, and Silicon and the Related Elements 178:7, pages 1567-1570.
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Christophe Waterlot, Anne Legrand, Benoit Rigo & Daniel Couturier. (2000) 1H and 13C NMR Determination of 1-Naphtyl-Polymethoxylated Diphenylwiethanes. Spectroscopy Letters 33:2, pages 211-226.
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Nagaraj Anbu, Chellappa Vijayan & Amarajothi Dhakshinamoorthy. (2019) A simple and efficient room temperature silylation of diverse functional groups with hexamethyldisilazane using CeO2 nanoparticles as solid catalysts. Molecular Catalysis 474, pages 110357.
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Mohammad Ali Zolfigol, Sami Sajjadifar, Arash Ghorbani-Choghamarani & Farzaneh Tami. (2018) Application of a novel nano-immobilization of ionic liquid on an MCM-41 system for trimethylsilylation of alcohols and phenols with hexamethyldisilazane. Research on Chemical Intermediates 44:11, pages 7093-7106.
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S. S. Mochalov, A. N. Fedotov, E. V. Trofimova & N. S. Zefirov. (2017) Synthesis of symmetrical α-alkyl- and α-arylalkylbenzyl and diarylmethyl ethers by HCl-catalyzed intermolecular dehydration. Russian Journal of Organic Chemistry 53:10, pages 1514-1519.
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Alina Ghinet, Philippe Gautret, Nathalie Van Hijfte, Bertrand Ledé, Jean‐Pierre Hénichart, Elena Bîcu, Ulrich Darbost, Benoît Rigo & Adam Daïch. (2014) Eaton’s Reagent‐Mediated Domino π‐Cationic Arylations of Aromatic Carboxylic Acids to Iasi‐Red Polymethoxylated Polycyclic Aromatic Hydrocarbons: Products with Unprecedented Biological Activities as Tubulin Polymerization Inhibitors. Chemistry – A European Journal 20:32, pages 10117-10130.
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Abdolreza Abri & Somayeh Ranjdar. (2014) Preparation of Nano Silica Supported Sodium Hydrogen Sulfate: As an Efficient Catalyst for the Trimethyl, Triethyl and t ‐Butyldimethyl Silylations of Aliphatic and Aromatic Alcohols in Solution and under Solvent‐free Conditions . Journal of the Chinese Chemical Society 61:8, pages 929-934.
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Ali Rahmatpour, Ali Vakili & Setare Azizian. (2013) Polystyrene-Gallium Trichloride Complex: A Mild, Highly Efficient, and Recyclable Polymeric Lewis Acid Catalyst for Chemoselective Silylation of Alcohols and Phenols with Hexamethyldisilazane. Heteroatom Chemistry 24:6, pages 443-451.
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Marjan Jereb & Dejan Vražič. (2013) Iodine-catalyzed disproportionation of aryl-substituted ethers under solvent-free reaction conditions. Organic & Biomolecular Chemistry 11:12, pages 1978.
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Shadab Gharaati, Majid Moghadam, Shahram Tangestaninejad, Valiollah Mirkhani & Iraj Mohammadpoor-Baltork. (2012) Highly efficient and selective trimethylsilylation of alcohols and phenols with hexamethyldisilazane catalyzed by polystyrene-bound tin(IV) porphyrin. Polyhedron 35:1, pages 87-95.
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Santosh T. Kadam & Sung Soo Kim. (2009) Mild and efficient silylation of alcohols and phenols with HMDS using Bi(OTf)3 under solvent-free condition. Journal of Organometallic Chemistry 694:16, pages 2562-2566.
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Christophe Waterlot, Daniel Couturier, Marc De Backer & Benoît Rigo. (2000) A study of hydrogenation of benzhydrols in the presence of catalytic amount of triflic acid. Canadian Journal of Chemistry 78:9, pages 1242-1246.
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Anne Legrand, Benoît Rigo, Jean‐Pierre Hénichart, Bernadette Norberg, Fabrice Camus, FranÇOis Durant & Daniel Couturier. (2009) Studies on pyrrolidinones. Synthesis and cyclization of N ‐[α‐naphthyl‐(3,4,5‐trimethoxyphenyl)‐methyl]pyroglutamic acid . Journal of Heterocyclic Chemistry 37:2, pages 215-227.
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Anne Legrand, Benoît Rigo, Philippe Gautret, Jean‐Pierre Henichart & Daniel Couturier. (2009) Studies on pyrrolidinone. Synthesis of aza analogs of podophyllotoxin and related compounds. Journal of Heterocyclic Chemistry 36:5, pages 1263-1270.
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Benoît Rigo, Philippe Gautret, Anne Legrand, Jean Pierre Hénichart & Daniel Couturier. (2009) Studies on pyrrolidinones. Synthesis of N ‐benzhydrylpyroglutamic acids and esters . Journal of Heterocyclic Chemistry 35:3, pages 567-573.
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P. GAUTRET, S. EL‐GHAMMARTI, A. LEGRAND, D. COUTURIER & B. RIGO. (2010) ChemInform Abstract: Silylation of Diarylcarbinols.. ChemInform 27:24.
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