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Journal of Wood Chemistry and Technology Volume 14, 1994 - Issue 1
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Original Articles

Quantitative Phosphorus-31 NMR Analysis of Six Soluble Lignins

Dimitris S. Argyropoulos Department of Chemistry, McGill University Pulp and Paper Research Centre, 3420 University St., Montreal, Quebec, Canada, H3A 2A7
Pages 65-82 | Published online: 20 Aug 2006

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Roberta Dagher, Véronic Landry & Tatjana Stevanovic. (2020) Contribution to understanding the color development on wood surfaces treated with iron salts by a combination of analytical methods. Journal of Wood Chemistry and Technology 40:4, pages 223-234.
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Tor Sewring, Julie Durruty, Lynn Schneider, Helen Schneider, Tuve Mattsson & Hans Theliander. (2019) Acid Precipitation of Kraft Lignin from Aqueous Solutions: The Influence of pH, Temperature, and Xylan. Journal of Wood Chemistry and Technology 39:1, pages 1-13.
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Mikhail Balakshin & Ewellyn Capanema. (2015) On the Quantification of Lignin Hydroxyl Groups With 31P and 13C NMR Spectroscopy. Journal of Wood Chemistry and Technology 35:3, pages 220-237.
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Yuan-Zong Lai & Yoshito Ohtani. (2003) On the Determination of β-Aryl Ether Units in Wood Lignin by an Ozonation Method. Journal of Wood Chemistry and Technology 23:3-4, pages 293-303.
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Denilson da Silva Perez, ManuelG. H. Terrones, Stéphane Grelier, Aziz Nourmamode, Alain Castellan, Reinaldo Ruggiero & AntônioE. H. Machado. (1998) Peroxyformic Acid Pulping of Eucalyptus Grandis Wood Chips and Sugar Cane Bagasse in one Stage and Characterization of the Isolated Lignins. Journal of Wood Chemistry and Technology 18:3, pages 333-365.
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Peter M. Froass, Arthur J. Ragauskas & Jian-er Jiang. (1996) Chemical Structure of Residual Lignin from Kraft Pulp. Journal of Wood Chemistry and Technology 16:4, pages 347-365.
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Articles from other publishers (63)

Xiaojuan Chen, Huchen Yang, Lidan Zhang, Zhongli Li, Yunna Xue, Rongfeng Wang, Xiaolin Fan & Shaolong Sun. (2023) Green construction and release mechanism of lignin-based double-layer coated urea. Biotechnology for Biofuels and Bioproducts 16:1.
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Haonan Zhang, Qi Liu, Yanchen Zhu, Zhang Feng, Hao Ren & Huamin Zhai. (2023) Structural comparison of different isolated eucalyptus lignins and analysis of their interaction mechanism with bovine serum albumin solution under QCM-D. Holzforschung 0:0.
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Chaofeng Zhang & Feng Wang. 2022. Lignin Conversion Catalysis. Lignin Conversion Catalysis 39 78 .
Qi Liu, Yanru Xu, Fangong Kong, Hao Ren & Huamin Zhai. (2022) Synthesis of phenolic resins by substituting phenol with modified spruce kraft lignin. Wood Science and Technology 56:5, pages 1527-1549.
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Qi Liu, Haonan Zhang, Hao Ren & Huamin Zhai. (2022) Structural analysis of light-colored separated lignin (lignocresol) and its antioxidant properties. International Journal of Biological Macromolecules 197, pages 169-178.
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Iuliana Ribca, Marcus E. Jawerth, Calvin J. Brett, Martin Lawoko, Matthias Schwartzkopf, Andrei Chumakov, Stephan V. Roth & Mats Johansson. (2021) Exploring the Effects of Different Cross-Linkers on Lignin-Based Thermoset Properties and Morphologies. ACS Sustainable Chemistry & Engineering 9:4, pages 1692-1702.
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Anna V. Faleva, Artem V. Belesov, Aleksandr Yu. Kozhevnikov, Danil I. Falev, Dmitry G. Chukhchin & Evgeniy V. Novozhilov. (2021) Analysis of the functional group composition of the spruce and birch phloem lignin. International Journal of Biological Macromolecules 166, pages 913-922.
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Adam Ekielski & Pawan Kumar Mishra. (2020) Lignin for Bioeconomy: The Present and Future Role of Technical Lignin. International Journal of Molecular Sciences 22:1, pages 63.
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Bin Luo, Zhuan Jia, Hongrui Jiang, Shuangfei Wang & Douyong Min. (2020) Improving the Reactivity of Sugarcane Bagasse Kraft Lignin by a Combination of Fractionation and Phenolation for Phenol–Formaldehyde Adhesive Applications. Polymers 12:8, pages 1825.
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Esakkiammal Sudha Esakkimuthu, Nathalie Marlin, Marie-Christine Brochier-Salon & Gérard Mortha. (2020) Study of the Reactivity of Lignin Model Compounds to Fluorobenzylation Using 13C and 19F NMR: Application to Lignin Phenolic Hydroxyl Group Quantification by 19F NMR. Molecules 25:14, pages 3211.
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Anna V. Faleva, Aleksandr Yu. Kozhevnikov, Sergey A. Pokryshkin, Artem V. Belesov & Ilya I. Pikovskoi. (2020) Structural characterization of the lignin from Saxifraga (Saxifraga oppositifolia L.) stems. International Journal of Biological Macromolecules 155, pages 656-665.
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Xiaolin Luo & Li Shuai. 2020. Green Adhesives. Green Adhesives 25 56 .
Shichao Wang, Mugaanire Tendo Innocent, Qianqian Wang, Hengxue Xiang, Jianguo Tang & Meifang Zhu. (2020) Kraft lignin-based piezoresistive sensors: Effect of chemical structure on the microstructure of ultrathin carbon fibers. International Journal of Biological Macromolecules 151, pages 730-739.
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Yong-Chao Lu, Yao Lu & Xing Fan. 2020. Lignin. Lignin 17 75 .
Xianzhi Meng, Claudia Crestini, Haoxi Ben, Naijia Hao, Yunqiao Pu, Arthur J. Ragauskas & Dimitris S. Argyropoulos. (2019) Determination of hydroxyl groups in biorefinery resources via quantitative 31P NMR spectroscopy. Nature Protocols 14:9, pages 2627-2647.
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Mona Alinejad, Christián Henry, Saeid Nikafshar, Akash Gondaliya, Sajad Bagheri, Nusheng Chen, Sandip Singh, David Hodge & Mojgan Nejad. (2019) Lignin-Based Polyurethanes: Opportunities for Bio-Based Foams, Elastomers, Coatings and Adhesives. Polymers 11:7, pages 1202.
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Tor Sewring, Weizhen Zhu, Maria Sedin & Hans Theliander. (2019) Predictions of Pair Interaction Potentials between Kraft Lignin Macromolecules in Black Liquors by Utilization of a Modified Poisson–Boltzmann Approach. Industrial & Engineering Chemistry Research 58:8, pages 3427-3439.
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Emmanuel Isaac Akpan. 2019. Sustainable Lignin for Carbon Fibers: Principles, Techniques, and Applications. Sustainable Lignin for Carbon Fibers: Principles, Techniques, and Applications 65 150 .
Yanqin Huang, Huacai Liu, Hongyou Yuan, Xiuzheng Zhuang, Song Yuan, Xiuli Yin & Chuangzhi Wu. (2018) Association of chemical structure and thermal degradation of lignins from crop straw and softwood. Journal of Analytical and Applied Pyrolysis 134, pages 25-34.
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Hélène Curmi, Christine Chirat, Marie-Christine Brochier Salon & Dominique Lachenal. (2018) Effect of autohydrolysis on alkaline delignification of mixed hardwood chips and on lignin structure. Holzforschung 72:8, pages 631-636.
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Christopher S. Lancefield, Hans L. J. Wienk, Rolf Boelens, Bert M. Weckhuysen & Pieter C. A. Bruijnincx. (2018) Identification of a diagnostic structural motif reveals a new reaction intermediate and condensation pathway in kraft lignin formation. Chemical Science 9:30, pages 6348-6360.
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Lars Passauer, Katrin Salzwedel, Marlene Struch, Nadine Herold & Jörn Appelt. (2016) Quantitative Analysis of the Etherification Degree of Phenolic Hydroxyl Groups in Oxyethylated Lignins: Correlation of Selective Aminolysis with FTIR Spectroscopy. ACS Sustainable Chemistry & Engineering 4:12, pages 6629-6637.
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Omid Hosseinaei, David P. Harper, Joseph J. Bozell & Timothy G. Rials. (2016) Role of Physicochemical Structure of Organosolv Hardwood and Herbaceous Lignins on Carbon Fiber Performance. ACS Sustainable Chemistry & Engineering 4:10, pages 5785-5798.
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Simone Strasser, Katrin Niegelhell, Manuel Kaschowitz, Sabina Markus, Rupert Kargl, Karin Stana-Kleinschek, Christian Slugovc, Tamilselvan Mohan & Stefan Spirk. (2016) Exploring Nonspecific Protein Adsorption on Lignocellulosic Amphiphilic Bicomponent Films. Biomacromolecules 17:3, pages 1083-1092.
Crossref
Stephanie Laurichesse & Luc Avérous. 2016. Biodegradable and Biobased Polymers for Environmental and Biomedical Applications. Biodegradable and Biobased Polymers for Environmental and Biomedical Applications 385 436 .
Wei Zhang, Noppadon Sathitsuksanoh, Blake A. Simmons, Charles E. Frazier, Justin R. Barone & Scott Renneckar. (2016) Revealing the thermal sensitivity of lignin during glycerol thermal processing through structural analysis. RSC Advances 6:36, pages 30234-30246.
Crossref
Tazien Rashid, Chong Fai Kait & Thanabalan Murugesan. (2016) Effect of Temperature on Molecular Weight Distribution of Pyridinium Acetate Treated Kraft Lignin. Procedia Engineering 148, pages 1363-1368.
Crossref
Nikhil D. Patil, Nicolas R. Tanguy & Ning Yan. 2016. Lignin in Polymer Composites. Lignin in Polymer Composites 27 47 .
Hendrik Mainka, Liane Hilfert, Sabine Busse, Frank Edelmann, Edgar Haak & Axel S. Herrmann. (2015) Characterization of the major reactions during conversion of lignin to carbon fiber. Journal of Materials Research and Technology 4:4, pages 377-391.
Crossref
Francisco G. Calvo‐Flores, José A. Dobado, Joaquín Isac‐García & Francisco J. Martín‐MartíNez. 2015. Lignin and Lignans as Renewable Raw Materials. Lignin and Lignans as Renewable Raw Materials 145 188 .
Stéphanie Laurichesse & Luc Avérous. (2014) Chemical modification of lignins: Towards biobased polymers. Progress in Polymer Science 39:7, pages 1266-1290.
Crossref
Iulian Andrei Gilca, Roxana Elena Ghitescu, Adrian Catalin Puitel & Valentin I. Popa. (2014) Preparation of lignin nanoparticles by chemical modification. Iranian Polymer Journal 23:5, pages 355-363.
Crossref
Alex Berlin & Mikhail Balakshin. 2014. Bioenergy Research: Advances and Applications. Bioenergy Research: Advances and Applications 315 336 .
Sanghamitra Sen, Hasan Sadeghifar & Dimitris S. Argyropoulos. (2013) Kraft Lignin Chain Extension Chemistry via Propargylation, Oxidative Coupling, and Claisen Rearrangement. Biomacromolecules 14:10, pages 3399-3408.
Crossref
Hoyong Chung & Newell R. Washburn. (2013) Chemistry of lignin-based materials. Green Materials 1:3, pages 137-160.
Crossref
Jae-Young Kim, Shinyoung Oh, Hyewon Hwang, Ung-Jin Kim & Joon Weon Choi. (2013) Structural features and thermal degradation properties of various lignin macromolecules obtained from poplar wood (Populus albaglandulosa). Polymer Degradation and Stability 98:9, pages 1671-1678.
Crossref
Christian J. Richard, Bhavish Patel, David Chadwick & Klaus Hellgardt. (2013) Hydrothermal deoxygenation of pyrolysis oil from Norwegian spruce: Picea abies. Biomass and Bioenergy 56, pages 446-455.
Crossref
C.G. da Silva, S. Grelier, F. Pichavant, E. Frollini & A. Castellan. (2013) Adding value to lignins isolated from sugarcane bagasse and Miscanthus. Industrial Crops and Products 42, pages 87-95.
Crossref
Geoffrey Moxley, Armindo Ribeiro Gaspar, Don Higgins & Hui Xu. (2012) Structural changes of corn stover lignin during acid pretreatment. Journal of Industrial Microbiology and Biotechnology 39:9, pages 1289-1299.
Crossref
Jackson D. MegiattoJrJr, Emmanuel Cazeils, Frédérique Ham-Pichavant, Stéphane Grelier, Christian Gardrat & Alain Castellan. (2012) Styrene-Spaced Copolymers Including Anthraquinone and β-O-4 Lignin Model Units: Synthesis, Characterization and Reactivity Under Alkaline Pulping Conditions. Biomacromolecules 13:5, pages 1652-1662.
Crossref
Lars Passauer, Klaus Fischer & Falk Liebner. (2011) Activation of pine kraft lignin by Fenton-type oxidation for cross-linking with oligo(oxyethylene) diglycidyl ether. Holzforschung 65:3.
Crossref
Yunqiao Pu, Shilin Cao & Arthur J. Ragauskas. (2011) Application of quantitative 31P NMR in biomass lignin and biofuel precursors characterization. Energy & Environmental Science 4:9, pages 3154.
Crossref
Elaine C. Ramires, Jackson D. MegiattoJr.Jr., Christian Gardrat, Alain Castellan & Elisabete Frollini. (2010) Valorization of an industrial organosolv-sugarcane bagasse lignin: Characterization and use as a matrix in biobased composites reinforced with sisal fibers. Biotechnology and Bioengineering 107:4, pages 612-621.
Crossref
Gösta Brunow & Knut Lundquist. 2010. Lignin and Lignans. Lignin and Lignans 267 299 .
Dimitris Argyropoulos. 2010. Lignin and Lignans. Lignin and Lignans 245 265 .
Shannon M. Notley & Magnus Norgren. (2010) Surface Energy and Wettability of Spin-Coated Thin Films of Lignin Isolated from Wood. Langmuir 26:8, pages 5484-5490.
Crossref
Elaine C. Ramires, Jackson D. MegiattoJr.Jr., Christian Gardrat, Alain Castellan & Elisabete Frollini. (2010) Biobased composites from glyoxal–phenolic resins and sisal fibers. Bioresource Technology 101:6, pages 1998-2006.
Crossref
Delphine Delmas, Dominique Lachenal, Gérard Mortha, Nathalie Marlin & Christophe Calais. (2009) Titration of free phenolic groups in pulps 10th EWLP, Stockholm, Sweden, August 25–28, 2008. Holzforschung 63:6.
Crossref
Jackson D. Megiatto, Jr., William Hoareau, Christian Gardrat, Elisabete Frollini & Alain Castellan. (2007) Sisal Fibers: Surface Chemical Modification Using Reagent Obtained from a Renewable Source; Characterization of Hemicellulose and Lignin as Model Study. Journal of Agricultural and Food Chemistry 55:21, pages 8576-8584.
Crossref
Qirong Fu, Dimitris S. Argyropoulos, David C. Tilotta & Lucian A. Lucia. (2007) Products and Functional Group Distributions in Pyrolysis Oil of Chromated Copper Arsenate (CCA)-Treated Wood, as Elucidated by Gas Chromatography and a Novel 31 P NMR-Based Method . Industrial & Engineering Chemistry Research 46:16, pages 5258-5264.
Crossref
R. P. Chandra, R. Bura, W. E. Mabee, A. Berlin, X. Pan & J. N. Saddler. 2007. Biofuels. Biofuels 67 93 .
Gösta Brunow. 2005. Biorefineries‐Industrial Processes and Products. Biorefineries‐Industrial Processes and Products 151 163 .
Reinaldo Ruggiero, Antonio E.H. Machado, Christian Gardrat, William Hoareau, Stéphane Grelier, B. Siegmund & Alain Castellan. (2005) Photodegradation of sugar cane bagasse acidolysis lignins. Journal of Photochemistry and Photobiology A: Chemistry 173:2, pages 150-155.
Crossref
William Hoareau, Wanderson G. Trindade, Bernard Siegmund, Alain Castellan & Elisabete Frollini. (2004) Sugar cane bagasse and curaua lignins oxidized by chlorine dioxide and reacted with furfuryl alcohol: characterization and stability. Polymer Degradation and Stability 86:3, pages 567-576.
Crossref
Christian Gardrat, Reinaldo Ruggiero, William Hoareau, Aziz Nourmamode, Stéphane Grelier, Bernard Siegmund & Alain Castellan. (2004) Photochemical study of an o-ethyl dibenzodioxocin molecule as a model for the photodegradation of non-phenolic lignin units of lignocellulosics. Journal of Photochemistry and Photobiology A: Chemistry 167:2-3, pages 111-120.
Crossref
Fadi S. Chakar & Arthur J. Ragauskas. (2004) Review of current and future softwood kraft lignin process chemistry. Industrial Crops and Products 20:2, pages 131-141.
Crossref
Tareq Saed Al Deen, D Brynn Hibbert, James M Hook & Robert J Wells. (2002) Quantitative nuclear magnetic resonance spectrometry. Analytica Chimica Acta 474:1-2, pages 125-135.
Crossref
Samir Hattalli, Ahmed Benaboura, Fr?d?rique Ham-Pichavant, Aziz Nourmamode & Alain Castellan. (2002) Adding value to Alfa grass (Stipa tenacissima L.) soda lignin as phenolic resins 1. Lignin characterization. Polymer Degradation and Stability 76:2, pages 259-264.
Crossref
C. Ingemar Johansson, John N. Saddler & Rodger P. Beatson. (2000) Characterization of the Polyphenolics Related to the Colour of Western Red Cedar (Thuja plicata Donn) Heartwood. Holzforschung 54:3.
Crossref
D. S. Argyropoulos & S. B. Menachem. 1998. Biopolymers from Renewable Resources. Biopolymers from Renewable Resources 292 322 .
Zhi‐Hua Jiang, Dimitris S. Argyropoulos & Alessandro Granata. (2005) Correlation analysis of 31 P NMR chemical shifts with substituent effects of phenols . Magnetic Resonance in Chemistry 33:5, pages 375-382.
Crossref
D. S. Argyropoulos. (1995) 31P NMR in wood chemistry: A review of recent progress. Research on Chemical Intermediates 21:3-5, pages 373-395.
Crossref
Oskar Faix, Dimitris S. Argyropoulos, Danielle Robert & Vincent Neirinck. (1994) Determination of Hydroxyl Groups in Lignins Evaluation of 1 H-, 13 C-, 31 P-NMR, FTIR and Wet Chemical Methods . hfsg 48:5, pages 387-394.
Crossref

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