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Solvent Extraction and Ion Exchange Volume 13, 1995 - Issue 2
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Original Articles

EXTRACTION OF LANTHANIDE(III) AND URANYL(VI) FROM NITRIC ACID SOLUTION BY N,N'-DIMETHYL-N,N'-DIBUTYLMALONAMIDE

Takashi NAKAMURA Department of Nuclear Engineering, Faculty of Engineering, Osaka University, Yamadaoka, Suita-shi, Osaka, 565, Japan
&
Chie MIYAKE Department of Nuclear Engineering, Faculty of Engineering, Osaka University, Yamadaoka, Suita-shi, Osaka, 565, Japan
Pages 253-273 | Published online: 27 Apr 2007

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Cyril Micheau, Yuki Ueda, Kazuhiro Akutsu-Suyama, Damien Bourgeois & Ryuhei Motokawa. (2023) Deuterated Malonamide Synthesis for Fundamental Research on Solvent Extraction Systems. Solvent Extraction and Ion Exchange 41:2, pages 221-240.
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E. A. Mowafy, D. Mohamed & A. Alshammari. (2015) Extraction and Separation of Selected Platinum-Group and Base Metal Ions from Nitric Acid Solutions Using Thiodiglycolamides (TDGA) as Novel Extractants. Separation Science and Technology 50:15, pages 2352-2359.
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Peizhuo Hu, Lijuan Qian, Hailong Wang, Huimin Zhu & Wangsuo Wu. (2014) Extraction of Uranium(VI) and Thorium(IV) from Nitric Acid Solution by N,N,N′,N′ – Tetraoctylglutaricamide. Separation Science and Technology 49:10, pages 1521-1526.
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Yuji Sasaki, Yasuhiro Tsubata, Yoshihiro Kitatsuji, Yumi Sugo, Noriko Shirasu & Yasuji Morita. (2014) Novel Extractant, NTAamide, and its Combination with TEDGA for Mutual Separation of Am/Cm/Ln. Solvent Extraction and Ion Exchange 32:2, pages 179-188.
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Mohsen M. Aly & Mohammed F. Hamza. (2013) A Review: Studies on Uranium Removal Using Different Techniques. Overview. Journal of Dispersion Science and Technology 34:2, pages 182-213.
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M. C. Costa, I. Pêczek, Z. Sadowski, S. Natu & A. P. Paiva. (2007) The Solvent Extraction of Iron(III) from Chloride Solutions by N,N′‐Tetrasubstituted Malonamides: Structure‐Activity Relationships. Solvent Extraction and Ion Exchange 25:4, pages 463-484.
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E. A. Mowafy & H. F. Aly. (2007) Synthesis of some N,N,N′,N′‐Tetraalkyl‐3‐Oxa‐Pentane‐1,5‐Diamide and their Applications in Solvent Extraction. Solvent Extraction and Ion Exchange 25:2, pages 205-224.
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E. A. Mowafy & H. F. Aly. (2006) Extraction Behaviors of Trivalent Lanthanides from Nitrate Medium by Selected Substituted Malonamides. Solvent Extraction and Ion Exchange 24:5, pages 677-692.
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Kornelia Matloka, Artem Gelis, Monica Regalbuto, George Vandegrift & Michael J. Scott. (2006) C 3‐Symmetric Tripodal Thio/Diglycolamide‐Based Ligands for Trivalent f‐Element Separations. Separation Science and Technology 41:10, pages 2129-2146.
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M. C. Costa, M. Martins & A. P. Paiva. (2005) Solvent Extraction of Iron(III) from Acidic Chloride Media Using N,N′‐Dimethyl‐N,N′‐dibutylmalonamide. Separation Science and Technology 39:15, pages 3573-3599.
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M. C. Costa, A. Carvalho, A. Uryga & A. P. Paiva. (2003) Solvent Extraction of Iron(III) from Hydrochloric Acid Solutions Using N,N′‐Dimethyl‐N,N′‐diphenylmalonamide and N,N′‐Dimethyl‐N,N′‐diphenyltetradecylmalonamide. Solvent Extraction and Ion Exchange 21:5, pages 653-686.
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Gregg J. Lumetta, Brian M. Rapko, Benjamin P. Hay, Priscilla A. Garza, James E. Hutchison & Robert D. Gilbertson. (2003) A Novel Bicyclic Diamide with High Binding Affinity for Trivalent f‐Block Elements. Solvent Extraction and Ion Exchange 21:1, pages 29-39.
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E. A. Mowafy & H. F. Aly. (2002) EXTRACTION BEHAVIOURS OF Nd(III), Eu(III), La(III), Am(III), AND U(VI) WITH SOME SUBSTITUTED MALONAMIDES FROM NITRATE MEDIUM. Solvent Extraction and Ion Exchange 20:2, pages 177-194.
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Gregg Lumetta, Richard Sell & Bruce McNamara. (2002) Thermal Decomposition of Neodymium Amide Complexes. Journal of Coordination Chemistry 55:6, pages 651-658.
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Yuji Sasaki, Yumi Sugo, Shinichi Suzuki & Shoichi Tachimori. (2001) THE NOVEL EXTRACTANTS, DIGLYCOLAMIDES, FOR THE EXTRACTION OF LANTHANIDES AND ACTINIDES IN HNO3–n-DODECANE SYSTEM. Solvent Extraction and Ion Exchange 19:1, pages 91-103.
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MARTIN ONWU CHIDOZIE OGWUEGBU & FRED CHILESHE. (2000) Coordination Chemistry in Mineral Processing. Mineral Processing and Extractive Metallurgy Review 21:6, pages 497-525.
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J. N. Mathur & K. L. Nash. (1998) THERMODYNAMICS OF EXTRACTION OF Am(III) AND Eu(III) FROM NITRATE AND THIOCYANATE MEDIA WITH OCTYL(PHENYL)-N,N-DIISOBUTYLCARBAMOYLMETHYLPHOSPHINE OXIDE. Solvent Extraction and Ion Exchange 16:6, pages 1341-1356.
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Articles from other publishers (31)

Ziwen Ying, Shuang Liu, Guannan Li, Qifeng Wei & Xiulian Ren. (2023) The effect of diluent on the extraction: Amide extracting chromium (VI) as an example. Journal of Molecular Liquids 384, pages 122205.
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E. Makombe, D. Bourgeois, L. Berthon & D. Meyer. (2022) Uranium(VI) and thorium(IV) extraction by malonamides: Impact of ligand molecular topology on selectivity. Journal of Molecular Liquids 368, pages 120701.
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Jong-Hyuk Jeon, Jin-Young Lee, Joon Soo Kim, Ho-Sung Yoon & Kumar Jyothi Rajesh. (2021) Separation of Uranium(VI) and Vanadium(V) from Sulfuric Acid Media by Amine Based Extractants through Liquid-liquid Extraction Technique#. Resources Recycling 30:4, pages 64-74.
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Ziwen Ying, Xiulian Ren, Jie Li, Guixuan Wu & Qifeng Wei. (2020) Recovery of chromium(VI) in wastewater using solvent extraction with amide. Hydrometallurgy 196, pages 105440.
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E. A. Mowafy, A. M. Al Shammari & D. Mohamed. (2019) Extraction of Uranium, Thorium, and Certain Lanthanides from Nitric Acid Medium with a Series of Substituted Glutaramides as Novel Extractants. Radiochemistry 61:6, pages 681-688.
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M. I. Kadyko, I. V. Skvortsov, A. V. Ivanov, E. V. Belova & B. F. Myasoedov. (2019) Effect of Irradiation on Hydrodynamic Properties of Extraction Mixtures Based on Carboxylic Acid Diamides in FS-13 Diluent. Radiochemistry 61:5, pages 579-584.
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D. Mohamed. (2017) Extraction of U(VI) and Th(IV) ions from nitric acid solutions with N,N,N′,N′-tetra-2-ethylhexylglutaramide. Radiochemistry 59:4, pages 354-359.
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Peng Ren, Ze-Yi Yan, Yang Li, Zuo-Miao Wu, Lei Wang, Lian-Biao Zhao, Yi-Quan Gao & Wang-Suo Wu. (2017) Synthesis and characterization of bisdiglycolamides for comparable extraction of Th4+, UO2 2+ and Eu3+ from nitric acid solution. Journal of Radioanalytical and Nuclear Chemistry 312:3, pages 487-494.
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Clotilde Gaillard, Maria Boltoeva, Isabelle Billard, Sylvia Georg, Valérie Mazan & Ali Ouadi. (2016) Ionic liquid-based uranium( vi ) extraction with malonamide extractant: cation exchange vs. neutral extraction . RSC Advances 6:74, pages 70141-70151.
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Xueming Zhong, Maosheng Fu, Yuancheng Qin, Dan Zhou & Tongcai Chen. (2015) Study on uranium recovery from tungsten residue: separation of U from Fe, Mn, Zr, Ti, Th, and Sc with mixture of N235 and TBP. Journal of Radioanalytical and Nuclear Chemistry 304:3, pages 1099-1108.
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Peizhuo Hu, Lijuan Qian, Xu Zhou, Dengfang Pan & Wangsuo Wu. (2012) Solvent extraction of uranyl by N,N,N′,N′-tetraoctylsuccinylamide from nitric acid solution. Journal of Radioanalytical and Nuclear Chemistry 295:2, pages 1209-1213.
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Yijia Yang & Spiro D. Alexandratos. (2012) Polymer-supported urea: The effect of hydrogen bonding on lanthanide ion affinities. Inorganica Chimica Acta 391, pages 130-134.
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Yu Cui, Yufen Hu, Yanju Zhang, Shaohong Yin & Guoxin Sun. (2010) Extraction of U(VI) with N,N′-dimethyl-N,N′-dioctylmalonamide from nitrate media. Russian Journal of Inorganic Chemistry 55:3, pages 468-471.
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Yijia Yang & Spiro D. Alexandratos. (2010) Mechanism of Ionic Recognition by Polymer-Supported Reagents: Immobilized Tetramethylmalonamide and the Complexation of Lanthanide Ions. Inorganic Chemistry 49:3, pages 1008-1016.
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Cui Yu, Sun Guoxin, Zhang Zhenwei, Hu Yufen & Sun Sixiu. (2007) Extraction of U(VI) with N,N’-dimethyl-N,N’-dioctylsuccinylamide in toluene. Journal of Radioanalytical and Nuclear Chemistry 272:1, pages 199-201.
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Moonsung Koh, Jaeryong Yoo, Yong Park, Daeil Bae, Kwangheon Park, Hakwon Kim & Hongdoo Kim. (2006) Supercritical CO 2 Extraction of Uranium(VI) from HNO 3 Solution Using N , N , N ‘, N ‘-Tetrabutyl-3-oxapentanediamide . Industrial & Engineering Chemistry Research 45:15, pages 5308-5313.
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Yu Cui, Guoxin Sun, Zhenwei Zhang, Yexin Li & Sixiu Sun. (2005) Extraction of U(VI) with unsymmetrical N-methyl-N-decylalkylamide in toluene. Radiochimica Acta 93:5, pages 287-290.
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Romain Diss & Georges Wipff. (2005) Lanthanide cationextraction by malonamideligands: from liquid–liquid interfaces to microemulsions. A molecular dynamics study. Phys. Chem. Chem. Phys. 7:2, pages 264-272.
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D. Max RoundhillD. Max Roundhill. 2001. Extraction of Metals from Soils and Waters. Extraction of Metals from Soils and Waters 193 230 .
Gregg J Lumetta, Bruce K McNamara, Brian M Rapko, Richard L Sell, Robin D Rogers, Grant Broker & James E Hutchison. (2000) Synthesis and characterization of mono- and bis-(tetraalkylmalonamide)uranium(VI) complexes. Inorganica Chimica Acta 309:1-2, pages 103-108.
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Linfeng Rao, PierLuigi Zanonato, Plinio Di Bernardo & Arturo Bismondo. (2000) Calorimetric and spectroscopic studies of Eu(III) complexation with tetramethylmalonamide and tetramethylsuccinamide in acetonitrile and dimethylsulfoxide. Inorganica Chimica Acta 306:1, pages 49-64.
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Brian M. Rapko, Bruce K. McNamara, Robin D. Rogers, Gregg J. Lumetta & Benjamin P. Hay. (1999) Coordination of Lanthanide Nitrates with N , N , N ‘, N ‘-Tetramethylsuccinamide . Inorganic Chemistry 38:20, pages 4585-4592.
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Gregg J. Lumetta, Bruce K. McNamara, Brian M. Rapko & James E. Hutchison. (1999) Complexation of uranyl ion by tetrahexylmalonamides: an equilibrium modeling and infrared spectroscopic study. Inorganica Chimica Acta 293:2, pages 195-205.
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Giovanni Sandrone, David A. Dixon & Benjamin P. Hay. (1999) C(sp 2 )−C(sp 3 ) Rotational Barriers in Simple Amides:  H 2 N−C(O)R (R = Methyl, Ethyl, i-Propyl, tert -Butyl) . The Journal of Physical Chemistry A 103:7, pages 893-902.
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Benjamin P. Hay, Omoshile Clement, Giovanni Sandrone & David A. Dixon. (1998) A Molecular Mechanics (MM3(96)) Force Field for Metal−Amide Complexes. Inorganic Chemistry 37:22, pages 5887-5894.
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G Ionova, R Guillaumont, S Ionov, C Madic & M.J Hudson. (1998) Structural investigations of N,N′-substituted malonamide crystal compounds as a basis to support trivalent lanthanide extraction mechanisms. Journal of Alloys and Compounds 275-277, pages 785-791.
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Yuji Sasaki, Takeo Adachi & Gregory R. Choppin. (1998) Solvent extraction study of actinide elements by N,N′-dimethyl-N,N′-dihexyl-3-oxapentanediamide and thenoyltrifluoroacetone. Journal of Alloys and Compounds 271-273, pages 799-802.
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O Clement, B.M Rapko & B.P Hay. (1998) Structural aspects of metal–amide complexes. Coordination Chemistry Reviews 170:1, pages 203-243.
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Y. Sasaki & G. R. Choppin. (1997) Solvent extraction of Eu, Th, U and am by N,N′-dimethyl-N,N′-dihexyl-3-thiopentanediamide and thenoyltrifluoroacetone. Journal of Radioanalytical and Nuclear Chemistry 222:1-2, pages 271-274.
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Y. Sasaki & G. R. Choppin. (1996) Extraction behaviors of Eu, Th, U and Am with diamides+thenoyltrifluoroacetone. Journal of Radioanalytical and Nuclear Chemistry Articles 207:2, pages 383-394.
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Yuji Sasaki & Gregory R. Choppin. (1996) Solvent Extraction of Eu, Th, U, Np and Am with N,N’-Dimethyl-N,N’-dihexyl-3-oxapentanediamide and Its Analogous Compounds. Analytical Sciences 12:2, pages 225-230.
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