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Original Articles

Determination of PDE-5 inhibitors and appetite suppressants in adulterated dietary supplements using LC/PDA and LC/MS

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Pages 29-32 | Received 19 Jul 2011, Accepted 09 Jan 2012, Published online: 01 Mar 2012

Keep up to date with the latest research on this topic with citation updates for this article.

Read on this site (8)

Samin Hamidi. (2023) Assessment of Undeclared Synthetic Drugs in Dietary Supplements in an Analytical View: A Comprehensive Review. Critical Reviews in Analytical Chemistry 53:5, pages 986-996.
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Luigi Giannetti, Valentina Gallo, Francesco Necci, Francesca Marini, Andrea Giorgi, Elisa Sonego, Francesca D’Onofrio & Bruno Neri. (2023) LC-HRMS analysis of 13 classes of pharmaceutical substances in food supplements. Food Additives & Contaminants: Part B 16:3, pages 253-265.
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Bo Ding, Zhiyuan Wang, Jianjun Xie, Guangfeng Zeng & Wenrui Chen. (2018) Phosphodiesterase-5 inhibitors in Chinese tonic liquors by liquid chromatography coupled with quadrupole time of flight mass spectrometry. Food Additives & Contaminants: Part B 11:3, pages 214-222.
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Ji Hye Jeong, Ji Hyun Lee, Hyung Joo Kim, Hyoung Joon Park, In Sun Hwang, Kyoung Moon Han, Chang-Yong Yoon, Sooyeul Cho & Woo Seong Kim. (2016) LC-ESI-MS/MS analysis of phosphodiesterase-5 inhibitors and their analogues in foods and dietary supplements in Korea. Food Additives & Contaminants: Part B 9:1, pages 1-8.
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Hyung Joo Kim, Ji Hyun Lee, Hyoung Joon Park, Jung-Yeon Kim, Sooyeul Cho & Woo Seong Kim. (2014) Determination of non-opioid analgesics in adulterated food and dietary supplements by LC-MS/MS. Food Additives & Contaminants: Part A 31:6, pages 973-978.
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Caroline Mathon, Anita Ankli, Eike Reich, Stefan Bieri & Philippe Christen. (2014) Screening and determination of sibutramine in adulterated herbal slimming supplements by HPTLC-UV densitometry. Food Additives & Contaminants: Part A 31:1, pages 15-20.
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Ji Hyune Lee, Nam Sook Kim, Kyoung Moon Han, Sung Hun Kim, Sooyeul Cho & Woo Seong Kim. (2013) Monitoring by LC-MS/MS of 48 compounds of sildenafil, tadalafil, vardenafil and their analogues in illicit health food products in the Korean market advertised as enhancing male sexual performance. Food Additives & Contaminants: Part A 30:11, pages 1849-1857.
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Ji Won Kim, Soon Jae Kweon, Seon Kyung Park, Jung Yeon Kim, Ji Hyun Lee, Kyoung Moon Han, Sooyeul Cho, Jinho Kim, Soon Young Han, Hyoung Ja Kim & Woo Seong Kim. (2013) Isolation and identification of a sibutramine analogue adulterated in slimming dietary supplements. Food Additives & Contaminants: Part A 30:7, pages 1221-1229.
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Articles from other publishers (14)

Ahmad Yusri Mohd Yusop, Linda Xiao & Shanlin Fu. (2021) Liquid chromatography-high-resolution mass spectrometry analysis of erectile dysfunction drugs and their analogues in food products. Forensic Science International 322, pages 110748.
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Nam Sook Kim, Sun Hee Moon, Hwan Seong Choi, Ji Hyun Lee, Seongsoo Park & Hoil Kang. (2020) Simultaneous separation and determination of 20 potential adulterant antigout and antiosteoporosis pharmaceutical compounds in herbal food products using LC with electrospray ionization MS/MS and LC with quadrupole‐time‐of‐flight MS. Journal of Separation Science 43:14, pages 2750-2765.
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Yogini S. Jaiswal & Leonard L. Williams. 2020. Herbal Medicine in India. Herbal Medicine in India 249 261 .
Ahmad Yusri Mohd Yusop, Linda Xiao & Shanlin Fu. (2019) Determination of phosphodiesterase 5 (PDE5) inhibitors in instant coffee premixes using liquid chromatography-high-resolution mass spectrometry (LC-HRMS). Talanta 204, pages 36-43.
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Thaís Ramos Dal Molin, Géssica Domingos Silveira, Gabriela Camera Leal, Larissa Sabo Müller, Diana Tomazi Muratt, Leandro Machado Carvalho & Carine Viana. (2019) A new approach to ion exchange chromatography with conductivity detection for adulterants investigation in dietary supplements. Biomedical Chromatography.
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Ji Hyun Lee, Han Na Park, Ok Rim Park, Nam Sook Kim, Sung-Kwan Park & Hoil Kang. (2019) Screening of illegal sexual enhancement supplements and counterfeit drugs sold in the online and offline markets between 2014 and 2017. Forensic Science International 298, pages 10-19.
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Amanda B. Lima, Wallans T. P. dos Santos & Richard G. Compton. (2019) Simple and Sensitive Determination of Sibutramine in Slimming Tea Beverages Using a Carbon Screen‐printed Electrode with Adsorptive Stripping Voltammetry. Electroanalysis 31:5, pages 975-980.
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Jhonys M. Freitas, Thiago C. Oliveira, Mario H.P. Santana, Craig E. Banks, Rodrigo A.A. Munoz & Eduardo M. Richter. (2019) A simple and fast-portable method for the screening of the appetite-suppressant drug sibutramine in natural products and multivitamins supplements. Sensors and Actuators B: Chemical 282, pages 449-456.
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Francesco Saverio Romolo, Andrea Salvini, Fabio Zelaschi, Massimo Oddone, Sara Odoardi, Serena Mestria & Sabina Strano Rossi. (2019) Instrumental neutron activation analysis (INAA) and liquid chromatography (LC) coupled to high resolution mass spectrometry (HRMS) characterisation of sildenafil based products seized on the Italian illegal market. Forensic Science International: Synergy 1, pages 126-136.
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Alicia G. Lydecker, Abhisheak Sharma, Christopher R. McCurdy, Bonnie A. Avery, Kavita M. Babu & Edward W. Boyer. (2016) Suspected Adulteration of Commercial Kratom Products with 7-Hydroxymitragynine. Journal of Medical Toxicology 12:4, pages 341-349.
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Tiago Rocha, Joana S. Amaral & Maria Beatriz P.P. Oliveira. (2016) Adulteration of Dietary Supplements by the Illegal Addition of Synthetic Drugs: A Review. Comprehensive Reviews in Food Science and Food Safety 15:1, pages 43-62.
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N. Satheeshkumar, David Paul & A. Lingesh. 2016. Medicinal Plants - Recent Advances in Research and Development. Medicinal Plants - Recent Advances in Research and Development 73 95 .
Lukas Vaclavik, Alexander J. Krynitsky & Jeanne I. Rader. (2014) Mass spectrometric analysis of pharmaceutical adulterants in products labeled as botanical dietary supplements or herbal remedies: a review. Analytical and Bioanalytical Chemistry 406:27, pages 6767-6790.
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Payam Aqai, Natalia Gómez Blesa, Hilary Major, Mattia Pedotti, Luca Varani, Valentina E. V. Ferrero, Willem Haasnoot & Michel W. F. Nielen. (2013) Receptor-based high-throughput screening and identification of estrogens in dietary supplements using bioaffinity liquid-chromatography ion mobility mass spectrometry. Analytical and Bioanalytical Chemistry 405:29, pages 9427-9436.
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