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Original Articles

Determination of PDE-5 inhibitors and appetite suppressants in adulterated dietary supplements using LC/PDA and LC/MS

, , , , , , , & show all
Pages 29-32 | Received 19 Jul 2011, Accepted 09 Jan 2012, Published online: 01 Mar 2012

References

  • Choi , D , Im , M , Lee , K , Kwon , K , Jeong , J , Park , G , Hong , M and Lee , C . 2004 . Determining anti-impotence drug-like compounds in food . Anal Sci Technol , 17 : 520 – 526 .
  • De Orsi , D , Pellegrini , M , Marchei , E , Nebuloni , P , Gallinella , B , Scaravelli , B , Martufi , A , Gagliardi , L and Pichini , S . 2009 . High performance liquid chromatography-diode array and electrospray-mass spectrometry analysis of vardenafil, sildenafil, tadalafil, testosterone and local anesthetics in cosmetic creams sold on the Internet web sites . J Pharm Biomed Anal , 50 ( 3 ) : 362 – 369 .
  • Ding , L , Hao , XY , Huang , X and Zhang , SQ . 2003 . Simultaneous determination of sibutramine and its N-desmethyl metabolites in human plasma by liquid chromatography-electrospray ionization-mass spectrometry—method and clinical applications . Anal Chim Acta , 492 ( 1–2 ) : 241 – 248 .
  • Gratz , SR , Flurer , CL and Wolnik , KA . 2004 . Analysis of undeclared synthetic phosphodiesterase-5 inhibitors in dietary supplements and herbal matrices by LC-ESI-MS and LC-UV . J Pharm Biomed Anal , 36 ( 3 ) : 525 – 533 .
  • Hernando , MD , Suarez-Barcena , JM , Bueno , MJM , Garcia-Reyes , JF and Fernandez-Alba , AR . 2007 . Fast separation liquid chromatography-tandem mass spectrometry for the confirmation and quantitative analysis of avermectin residues in food . J Chromatogr A , 1155 ( 1 ) : 62 – 73 .
  • Jung , J , Hermanns-Clausen , M and Weinmann , W . 2006 . Anorectic sibutramine detected in a Chinese herbal drug for weight loss . Forensic Sci Int , 161 ( 2–3 ) : 221 – 222 .
  • Kim , SH , Lee , J , Yoon , T , Choi , J , Choi , D , Kim , D and Kwon , SW . 2009 . Simultaneous determination of anti-diabetes/anti-obesity drugs by LC/PDA, and targeted analysis of sibutramine analog in dietary supplements by LC/MS/MS . Biomed Chromatogr , 23 ( 12 ) : 1259 – 1265 .
  • Lee , HM and Lee , BJ . 2011 . A novel approach to simultaneous screening and confirmation of regulated pharmaceutical compounds in dietary supplements by LC/MS/MS with an information-dependent acquisition method . Food Addit Contam A , 28 ( 4 ) : 396 – 407 .
  • Wang , J , Chen , B and Yao , S . 2008 . Analysis of six synthetic adulterants in herbal weight-reducing dietary supplements by LC electrospray ionization-MS . Food Addit Contam A , 25 ( 7 ) : 822 – 830 .
  • Wang , J , Jiang , Y , Wang , Y , Zhao , X , Cui , Y and Gu , J . 2007 . Liquid chromatography tandem mass spectrometry assay to determine the pharmacokinetics of aildenafil in human plasma . J Pharm Biomed Anal , 44 ( 1 ) : 231 – 235 .
  • Zhu , X , Xiao , S , Chen , B , Zhang , F , Yao , S , Wan , Z , Yang , D and Han , H . 2005 . Simultaneous determination of sildenafil, vardenafil and tadalafil as forbidden components in natural dietary supplements for male sexual potency by high-performance liquid chromatography-electrospray ionization mass spectrometry . J Chromatogr A , 1066 ( 1–2 ) : 89 – 95 .
  • Zou , P , Oh , SS , Hou , P , Low , MY and Koh , HL . 2006 . Simultaneous determination of synthetic phosphodiesterase-5 inhibitors found in a dietary supplement and pre-mixed bulk powders for dietary supplements using high-performance liquid chromatography with diode array detection and liquid chromatography-electrospray ionization tandem mass spectrometry . J Chromatogr A , 1104 ( 1–2 ) : 113 – 122 .

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