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Original Articles

β-lactam antibiotics residues analysis in bovine milk by LC-ESI-MS/MS: a simple and fast liquid–liquid extraction method

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Pages 497-507 | Received 24 Nov 2010, Accepted 28 Jun 2011, Published online: 11 Oct 2011

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Min Hu, Yujie Ben, Ming Hung Wong & Chunmiao Zheng. (2021) Trace Analysis of Multiclass Antibiotics in Food Products by Liquid Chromatography-Tandem Mass Spectrometry: Method Development. Journal of Agricultural and Food Chemistry 69:5, pages 1656-1666.
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Gjylai Alija, Zehra Hajrulai-Musliu & Risto Uzunov. (2020) Development and validation of confirmatory LC–MS/MS method for multi-residue analysis of antibiotic drugs in bovine milk. SN Applied Sciences 2:9.
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Yuanling Zhao, Xi’ai Hou, Dongmei Qin & Dan Liu. (2019) Dispersive Liquid-Liquid Microextraction Method for the Simultaneous Determination of Four Isomers of Hexachlorocyclohexane and Six Pyrethroid Pesticides in Milk by Gas Chromatography Electron Capture Detector. Food Analytical Methods 13:2, pages 370-381.
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Andréa Renata Bortolotte, Daniela Daniel, Patrícia Aparecida de Campos Braga & Felix Guillermo Reyes Reyes. (2019) A simple and high-throughput method for multiresidue and multiclass quantitation of antimicrobials in pangasius (Pangasionodon hypophthalmus) fillet by liquid chromatography coupled with tandem mass spectrometry. Journal of Chromatography B 1124, pages 17-25.
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Jun Chen, Guang-Guo Ying & Wen-Jing Deng. (2019) Antibiotic Residues in Food: Extraction, Analysis, and Human Health Concerns. Journal of Agricultural and Food Chemistry 67:27, pages 7569-7586.
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Fenfang Deng, Hong Yu, Xinhong Pan, Guoyuan Hu, Qiqin Wang, Rongfei Peng, Lei Tan & Zhicong Yang. (2018) Ultra-high performance liquid chromatography tandem mass spectrometry for the determination of five glycopeptide antibiotics in food and biological samples using solid-phase extraction. Journal of Chromatography A 1538, pages 54-59.
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Louise Jank, Magda Targa Martins, Juliana Bazzan Arsand, Tanara Magalhães Campos Motta, Tiago Corrêa Feijó, Tamara dos Santos Castilhos, Rodrigo Barcellos Hoff, Fabiano Barreto & Tânia Mara Pizzolato. (2017) Liquid Chromatography–Tandem Mass Spectrometry Multiclass Method for 46 Antibiotics Residues in Milk and Meat: Development and Validation. Food Analytical Methods 10:7, pages 2152-2164.
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Victoria Samanidou, Katia Michaelidou, Abuzar Kabir & Kenneth G. Furton. (2017) Fabric phase sorptive extraction of selected penicillin antibiotic residues from intact milk followed by high performance liquid chromatography with diode array detection. Food Chemistry 224, pages 131-138.
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Eun-Kee Park, Yong-Jae Ryu, Chun-Nam Cha, Chang-Yeul Yoo, Suk Kim & Hu-Jang Lee. (2016) Analysis of antibiotic residues in milk from healthy dairy cows treated with bovine mastitis ointment using ultra-performance liquid chromatography coupled with electrospray tandem mass spectrometry. Korean Journal of Veterinary Research 56:4, pages 233-239.
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Noorfatimah Yahaya, Mohd Marsin Sanagi, Takahito Mitome, Norikazu Nishiyama, Wan Aini Wan Ibrahim & Hadi Nur. (2014) Dispersive Micro-Solid Phase Extraction Combined with High-Performance Liquid Chromatography for the Determination of Three Penicillins in Milk Samples. Food Analytical Methods 8:5, pages 1079-1087.
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Paola Bottoni & Sergio Caroli. (2015) Detection and quantification of residues and metabolites of medicinal products in environmental compartments, food commodities and workplaces. A review. Journal of Pharmaceutical and Biomedical Analysis 106, pages 3-24.
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Mónica Díaz-Bao, Rocío Barreiro, José Manuel Miranda, Alberto Cepeda & Patricia Regal. (2015) Fast HPLC-MS/MS Method for Determining Penicillin Antibiotics in Infant Formulas Using Molecularly Imprinted Solid-Phase Extraction. Journal of Analytical Methods in Chemistry 2015, pages 1-8.
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MingHui Li, WenShen He, LiJun Zhang & ChengLi Duan. (2015) Analysis of penicillin and its β-lactamase hydrolysis products in milk using capillary zone electrophoresis. Analytical Methods 7:11, pages 4602-4607.
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Magda Targa Martins, Jéssica Melo, Fabiano Barreto, Rodrigo Barcellos Hoff, Louise Jank, Michele Soares Bittencourt, Juliana Bazzan Arsand & Elfrides Eva Scherman Schapoval. (2014) A simple, fast and cheap non-SPE screening method for antibacterial residue analysis in milk and liver using liquid chromatography–tandem mass spectrometry. Talanta 129, pages 374-383.
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Alexandra Junza, Noemí Dorival-García, Alberto Zafra-Gómez, Dolores Barrón, Oscar Ballesteros, José Barbosa & Alberto Navalón. (2014) Multiclass method for the determination of quinolones and β-lactams, in raw cow milk using dispersive liquid–liquid microextraction and ultra high performance liquid chromatography–tandem mass spectrometry. Journal of Chromatography A 1356, pages 10-22.
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T.M. Campos Motta, R.B. Hoff, F. Barreto, R.B.S. Andrade, D.M. Lorenzini, L.Z. Meneghini & T.M. Pizzolato. (2014) Detection and confirmation of milk adulteration with cheese whey using proteomic-like sample preparation and liquid chromatography–electrospray–tandem mass spectrometry analysis. Talanta 120, pages 498-505.
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Xiao-Lin Hou, Yin-Liang Wu, Yan Lv, Xiu-Qin Xu, Jian Zhao & Ting Yang. (2013) Development and validation of an ultra high performance liquid chromatography tandem mass spectrometry method for determination of 10 cephalosporins and desacetylcefapirin in milk. Journal of Chromatography B 931, pages 6-11.
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Xiaojia Huang, Linli Chen, Meng Chen, Dongxing Yuan & Shuyu Nong. (2013) Sensitive monitoring of penicillin antibiotics in milk and honey treated by stir bar sorptive extraction based on monolith and LC-electrospray MS detection. Journal of Separation Science 36:5, pages 907-915.
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