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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 6
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Original Articles

MICROWAVE PROMOTED EFFICIENT SYNTHESIS OF SUBSTITUTED URACILS AND THIOURACILS UNDER SOLVENT-FREE CONDITIONS

Mohammad M. Mojtahedi Department of Chemistry, Sharif University of Technology, Tehran, Iran
,
Mohammad R. Saidi Department of Chemistry, Sharif University of Technology, Tehran, Iran
,
Jafar S. Shirzi Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran
&
Mohammad Bolourtchian Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran
Pages 851-855 | Received 05 Jan 2001, Published online: 16 Aug 2006

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Furgan Aslanoglu & Ahmet Yazıcı. (2023) 6-methylthiouracil and 6-methyluracil derivatives synthesized by reaction of acetylketene with thiourea and urea compounds in presence of Yb(TFA)3. Synthetic Communications 53:20, pages 1713-1721.
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Navjeet Kaur. (2015) Review on the Synthesis of Six-MemberedN,N-Heterocycles by Microwave Irradiation. Synthetic Communications 45:10, pages 1145-1182.
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Arpi Majumder, Ragini Gupta & Anshu Jain. (2013) Microwave-assisted synthesis of nitrogen-containing heterocycles. Green Chemistry Letters and Reviews 6:2, pages 151-182.
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Ji‐Tai Li, Zhi‐Ping Lin, Jun‐Fen Han & Tong‐Shuang Li. (2004) One‐Pot Synthesis of 4‐Oxo‐2‐thioxohexahydropyrimidines Catalyzed by Potassium Carbonate Under Ultrasound. Synthetic Communications 34:14, pages 2623-2631.
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Abdussalam K. Qaroush, Ahed W. Alsayyed, Ala'a F. Eftaiha, Feda'a M. Al‐Qaisi & Bader A. Salameh. (2022) Green Microwave‐Assisted Synthesis of Cyclic/Acyclic Ureas from Propylene Carbonate. ChemistrySelect 7:20.
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Mohammadesmaeil Moayyed & Dariush Saberi. (2020) Iodine-catalyzed synthesis of β-uramino crotonic esters as well as oxidative esterification of carboxylic acids in choline chloride/urea: a desirable alternative to organic solvents. Journal of the Iranian Chemical Society 18:2, pages 445-455.
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J S Aher, A V kardel, M R Gaware, D D Lokhande & A M Bhagare. (2019) One pot synthesis of pyrimidine-5-carbonitrile and pyrimidine-5-carboxamide using ammonium chloride under solvent free condition. Journal of Chemical Sciences 131:7.
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Chandrabhan Verma, L. O. Olasunkanmi, I. B. Obot, Eno E. Ebenso & M. A. Quraishi. (2016) 5-Arylpyrimido-[4,5-b]quinoline-diones as new and sustainable corrosion inhibitors for mild steel in 1 M HCl: a combined experimental and theoretical approach. RSC Advances 6:19, pages 15639-15654.
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Lütfiye Aydın, Emine Şahan, Zülbiye Önal & Talat Özpozan. (2014) Synthesis, experimental spectra (IR & Raman and NMR), vibrational analysis and theoretical DFT investigations of N-(5-(4-methylbenzoyl)-2-oxo-4-(4-methylphenyl)pyrimidine-1(2H)-yl)-4-methylbenzamide. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 129, pages 22-34.
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Jeffrey T. Kohrt, Ed Conn, Robert Maguire, Stephen W. Wright & Robert Singer. (2013) Expedient synthesis of novel β-ketoesters from the Mizoroki–Heck coupling of ethyl 3-ethoxyacrylate with aryl and pyridyl halides. Tetrahedron Letters 54:51, pages 7065-7068.
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Ersin İnkaya, Muharrem Dinçer, Emine Şahan & İsmail Yıldırım. (2013) Synthesis, spectroscopic and structural characterization of 5-benzoyl-4-phenyl-2-methylthio-1H-pyrimidine with theoretical calculations using density functional theory. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 114, pages 92-100.
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Sohail Saeed, Rizwan Hussain & Muhammad Ali. (2013) Synthesis and Antimicrobial Activity of N -[(2 Z )-3-(4,6-Substitutedpyrimidin-2-yl)-4-phenyl-1,3-thiazol-2(3 H )-ylidene]-3, 5-dinitrobenzamide Analogues . Journal of Heterocyclic Chemistry 50:2, pages 237-243.
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Pandaram Palanisamy, Samson Jegan Jenniefer, Packianathan Thomas Muthiah & Sudalaiandi Kumaresan. (2013) Synthesis, characterization, antimicrobial, anticancer, and antituberculosis activity of some new pyrazole, isoxazole, pyrimidine and benzodiazepine derivatives containing thiochromeno and benzothiepino moieties. RSC Advances 3:42, pages 19300.
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S. Maddila, G.L.V. Damu, E.O. Oseghe, O.A. Abafe, C. Venakata Rao & P. Lavanya. (2012) Synthesis and Biological Studies of Novel Biphenyl-3,5-dihydro-2H-thiazolopyrimidines Derivatives. Journal of the Korean Chemical Society 56:3, pages 334-340.
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Y. Kotaiah, N. Hari Krishna, K. Naga Raju, C.V. Rao, S.B. Jonnalagadda & Suresh Maddila. (2012) Synthesis and Biological Evaluation of Novel Isopropyl 2-thiazolopyrimidine-6-carboxylate Derivatives. Journal of the Korean Chemical Society 56:1, pages 68-73.
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Suresh Maddila & Sreekantha B. Jonnalagadda. (2012) Synthesis and Biological Activity of Ethyl 2-(substituted benzylthio)-4-(3′-(ethoxycarbonyl)biphenyl-4-yl)-6-methyl-1,4-dihydropyrimidine-5-carboxylate Derivatives. Archiv der Pharmazie 345:2, pages 163-168.
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Toshiaki Sasada, Youichi Aoki, Reiko Ikeda, Norio Sakai & Takeo Konakahara. (2011) Synthesis of Tri‐ or Tetrasubstituted Pyrimidine Derivatives through the [5+1] Annulation of Enamidines with either N , N ‐Dimethylformamide Dialkyl Acetals or Orthoesters and Their Application in a Ring Transformation of Pyrimidines to Pyrido[2,3‐ d ]pyrimidin‐5‐one Derivatives . Chemistry – A European Journal 17:34, pages 9385-9394.
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Sohail Saeed, Naghmana Rashid, Peter G. Jones & Arifa Tahir. (2010) Synthesis and pharmacological properties of N‐substituted‐ N ′‐(4,6‐dimethylpyrimidin‐2‐yl)‐thiourea derivatives and related fused heterocyclic compounds . Journal of Heterocyclic Chemistry 48:1, pages 74-82.
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Larry T. Pierce, Michael M. Cahill & Florence O. McCarthy. (2010) Design and synthesis of novel 5,6-bisindolylpyrimidin-4-ones structurally related to ruboxistaurin (LY333531). Tetrahedron 66:51, pages 9754-9761.
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Sohail Saeed, Naghmana Rashid, Peter Jones, Rizwan Hussain & Moazzam Bhatti. (2010) Synthesis, spectroscopic characterization, crystal structure and antifungal activity of thiourea derivatives containing a thiazole moiety. Open Chemistry 8:3, pages 550-558.
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M. Jain. 2010. Chemical Shifts and Coupling Constants for Hydrogen-1, Heterocycles. Chemical Shifts and Coupling Constants for Hydrogen-1, Heterocycles 468 468 .
M. Jain. 2010. Chemical Shifts and Coupling Constants for Hydrogen-1, Heterocycles. Chemical Shifts and Coupling Constants for Hydrogen-1, Heterocycles 65 65 .
M. Jain. 2010. Chemical Shifts and Coupling Constants for Hydrogen-1, Heterocycles. Chemical Shifts and Coupling Constants for Hydrogen-1, Heterocycles 160 160 .
Marcos A. P. Martins, Clarissa P. Frizzo, Dayse N. Moreira, Lilian Buriol & Pablo Machado. (2009) Solvent-Free Heterocyclic Synthesis. Chemical Reviews 109:9, pages 4140-4182.
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Swapnil S. Sonar, Sandip A. Sadaphal, Shivaji S. Pawar, Bapurao B. Shingate & Murlidhar S. Shingare. (2009) Microwave assisted convenient synthesis of quino[2,3-b][1,5]benzoxazepines. Chinese Chemical Letters 20:5, pages 557-561.
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Mohammad M. Mojtahedi, Mohammad R. Saidi, Jafar S. Shirzi & Mohammad Bolourtchian. (2010) ChemInform Abstract: Microwave Promoted Efficient Synthesis of Substituted Uracils and Thiouracils under Solvent‐Free Conditions.. ChemInform 33:33.
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