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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 23
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Original Articles

KF‐Alumina Catalyzed One‐Pot Synthesis of Pyrido[2,3‐d]Pyrimidine Derivatives

Xiang‐shan Wang Department of Chemistry, Xuzhou Normal University, Xuzhou, Jiangsu, 221116, P.R. China; School of Chemical Engineering, China University of Mining and Technology, Xuzhou, Jiangsu, P.R. China; The Key Laboratory of Biotechnology on Medical Plant, Xuzhou, Jiangsu, P.R. ChinaCorrespondence[email protected]
,
Zhao‐sen Zeng Department of Chemistry, Xuzhou Normal University, Xuzhou, Jiangsu, 221116, P.R. China
,
Da‐qing Shi Department of Chemistry, Xuzhou Normal University, Xuzhou, Jiangsu, 221116, P.R. China; The Key Laboratory of Biotechnology on Medical Plant, Xuzhou, Jiangsu, P.R. China
,
Xian‐yong Wei School of Chemical Engineering, China University of Mining and Technology, Xuzhou, Jiangsu, P.R. China
&
Zhi‐min Zong School of Chemical Engineering, China University of Mining and Technology, Xuzhou, Jiangsu, P.R. China
Pages 4331-4338 | Received 24 May 2004, Published online: 10 Jan 2011

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Manisha R. Bhosle, Amruta Palke, Giribala M. Bondle, Aniket P. Sarkate, Rajaram Azad & Prasad V. L. S. Burra. (2023) Efficient Synthesis of Densely Functionalized Pyrido[2,3-d]Pyrimidines via Three-component One-pot Domino Knoevenagel aza-Diels Alder Reaction and Induces Apoptosis in Human Cancer Cell Lines via Inhibiting Aurora A and B Kinases. Polycyclic Aromatic Compounds 43:9, pages 7912-7929.
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Chetan K. Jadhav, Amol S. Nipate, Asha V. Chate & Charansingh H. Gill. (2022) An Organocatalytic Newer Synthetic Approach toward the Access of Dihydropyrido[2,3-d] Pyrimidine in Water: A Perfect Synergy for Eco-compatible Organic Synthesis. Polycyclic Aromatic Compounds 42:10, pages 7368-7384.
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Forough Ramezanzadeh, Manouchehr Mamaghani, Hossein Fallah-Bagher Shaidaei & Mehdi Sheykhan. (2021) Synthesis and Application of Imidazolium-Based Ionic Liquid Supported on Hydroxyapatite Encapsulated γ-Fe2O3 Nanocatalyst in Preparation of Pyrido[2,3-d]Pyrimidines. Polycyclic Aromatic Compounds 41:9, pages 1925-1943.
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Ajmal R. Bhat, Rajendra S. Dongre, Gowhar A. Naikoo, Israr U. Hassan & Tabassum Ara. (2017) Proficient synthesis of bioactive annulated pyrimidine derivatives: A review. Journal of Taibah University for Science 11:6, pages 1047-1069.
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Sibaji Nandi, Mullah Muhaiminul Islam, Mithu Saha, Sivaprasad Mitra, Snehadrinarayan Khatua & Amarta Kumar Pal. (2016) Regioselective synthesis of functionalized [1,6]-naphthyridines by KF/basic alumina as a recyclable catalyst and a brief study of their photophysical properties. Synthetic Communications 46:17, pages 1461-1476.
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M. Syamala. (2009) Recent Progress in Three-Component Reactions. An Update. Organic Preparations and Procedures International 41:1, pages 1-68.
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Xiang-Shan Wang, Mei-Mei Zhang, Qing Li, Chang-Sheng Yao & Shu-Jiang Tu. (2008) Simple Procedure for the Synthesis of 5,7-Diarylpyrido[2,3-d]pyrimidine Derivatives catalyzed by KF-Alumina. Synthetic Communications 38:12, pages 1896-1908.
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Xiang‐Shan Wang, Zhao‐Sen Zeng, Da‐Qing Shi, Shu‐Jiang Tu, Xian‐Yong Wei & Zhi‐Min Zong. (2005) Three‐Component, One‐Pot Synthesis of Pyrido[2,3‐d]pyrimidine Derivatives Catalyzed by KF‐alumina. Synthetic Communications 35:14, pages 1921-1927.
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Articles from other publishers (33)

Elshimaa Mohmed Eid. (2024) Sustainable Green Synthesis of Pyrimidine Derivatives: Review on Multicomponent Synthesis, Catalysts and Techniques. Current Organic Synthesis 21:2, pages 127-139.
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Luan A. Martinho & Carlos Kleber Z. Andrade. (2022) A greener approach for the synthesis of pyrido[2,3‐ d ]pyrimidine derivatives in glycerol under microwave heating . Journal of Heterocyclic Chemistry 59:8, pages 1417-1429.
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Mr. Towseef Ahmad Padder, Dr. Rekha Israni & Mohd Waseem Wani. (2022) Synthesis, Charaterization and Bioactivities of Fused Pyrimidobenzothiazol-4-one. International Journal of Advanced Research in Science, Communication and Technology, pages 210-214.
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Kiran R. Khillare, Dipak S. Aher, Laxmikant D. Chavan & Sunil G. Shankarwar. (2021) Cesium salt of 2-molybdo-10-tungstophosphoric acid as an efficient and reusable catalyst for the synthesis of uracil derivatives via a green route . RSC Advances 11:54, pages 33980-33989.
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Mohammad Nikpassand & Elaheh hoseinnezhad. (2020) Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2Pr@glucose amine as a mild nano catalyst. Arabian Journal of Chemistry 13:12, pages 8995-9004.
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Tayebeh Farahmand, Saeedeh Hashemian & Ali Sheibani. (2020) Efficient one-pot synthesis of pyrano[2,3-d]pyrimidinone and pyrido [2,3-d] pyrimidine derivatives by using of Mn-ZIF-8@ZnTiO3 nanocatalyst. Journal of Molecular Structure 1206, pages 127667.
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Dattatraya K. Jamale, Vashishtha M. Gurame, Navanath J. Valekar, Shankar P. Hangirgekar, Govind B. Kolekar & Prashant V. Anbhule. (2019) An Efficient Protocol for the Synthesis of Pyrido[2,3‐ d ]pyrimidines in Glycerol–Water Medium: Assessment by Green Chemistry Metrics . Macromolecular Symposia 387:1.
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Boshra Mirhosseini-Eshkevari, Manzarbanoo Esnaashari & Mohammad Ali Ghasemzadeh. (2019) Novel Brönsted Acidic Ionic Liquids Confined in UiO-66 Nanocages for the Synthesis of Dihydropyrido[2,3- d ]Pyrimidine Derivatives under Solvent-Free Conditions . ACS Omega 4:6, pages 10548-10557.
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Fatemeh Rigi & Hamid Reza Shaterian. (2018) One‐pot synthesis of 2‐amino‐4,8‐dihydropyrano[3,2‐b]pyranes and pyridopyrimidines under mild conditions. Journal of the Chinese Chemical Society 66:4, pages 434-437.
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Pegah Farokhian, Manouchehr Mamaghani, Nosrat Ollah Mahmoodi, Khalil Tabatabaeian & Abdollah Fallah Shojaie. (2019) An expeditious one-pot synthesis of pyrido[2,3- d ]pyrimidines using Fe 3 O 4 –ZnO–NH 2 –PW 12 O 40 nanocatalyst . Journal of Chemical Research 43:3-4, pages 135-139.
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Toktam Afrough, Mehdi Bakavoli & Hossein Eshghi. (2019) A New Multicomponent Synthetic Route to Hexahydropyrido[2,3- d ]pyrimidine Derivatives . Journal of Heterocyclic Chemistry 56:2, pages 636-641.
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Majid M. Heravi, Vahideh Zadsirjan, Mahzad Dehghani & Tahereh Ahmadi. (2018) Towards click chemistry: Multicomponent reactions via combinations of name reactions. Tetrahedron 74:27, pages 3391-3457.
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Farhad Shirini, Mohaddeseh Safarpoor Nikoo Langarudi, Nader Daneshvar, Negar Jamasbi & Mahsa Irankhah-Khanghah. (2018) Preparation and characterization of [H2-DABCO][ClO4]2 as a new member of DABCO-based ionic liquids for the synthesis of pyrimido[4,5-b]-quinoline and pyrimido[4,5-d]pyrimidine derivatives. Journal of Molecular Structure 1161, pages 366-382.
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Mohammad Bayat & Shima Nasri. (2018) Modified Kappa-Carrageenan as a Heterogeneous Green Catalyst for the Synthesis of Nitrogen and Sulfur-Containing Indenone-Fused Heterocyclic Compounds. Journal of Heterocyclic Chemistry 55:3, pages 650-659.
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Rajendra Sukhdeorao Dongre, Jyostna S. Meshram, Rupali Sudhakarrao Selokar, Faisal A. Almalki & Taibi Ben Hadda. (2018) Antibacterial activity of synthetic pyrido[2,3- d ]pyrimidines armed with nitrile groups: POM analysis and identification of pharmacophore sites of nitriles as important pro-drugs . New Journal of Chemistry 42:19, pages 15610-15617.
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Prasanna Nithiya Sudhan, Majid Ghashang & Syed Sheik Mansoor. (2016) Efficient synthesis of a novel series of indeno fused pyrido[2,3-d]pyrimidines using β-cyclodextrin-propyl sulfonic acid as an eco-friendly catalyst. Beni-Suef University Journal of Basic and Applied Sciences 5:4, pages 340-349.
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Swastika Singh, Mohammad Saquib, Mandavi Singh, Jyoti Tiwari, Fatima Tufail, Jaya Singh & Jagdamba Singh. (2016) A catalyst free, multicomponent-tandem, facile synthesis of pyrido[2,3-d]pyrimidines using glycerol as a recyclable promoting medium. New Journal of Chemistry 40:1, pages 63-67.
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Amaneh Mossafaii Rad & Masoud Mokhtary. (2015) Efficient one-pot synthesis of pyrido[2,3-d]pyrimidines catalyzed by nanocrystalline MgO in water. International Nano Letters 5:2, pages 109-123.
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Firouzeh Nemati & Raheleh Saeedirad. (2013) Nano-Fe3O4 encapsulated-silica particles bearing sulfonic acid groups as a magnetically separable catalyst for green and efficient synthesis of functionalized pyrimido[4,5-b]quinolines and indeno fused pyrido[2,3-d]pyrimidines in water. Chinese Chemical Letters 24:5, pages 370-372.
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Bai-Xiang Du, Yu-Ling Li, Xiang-Shan Wang & Da-Qing Shi. (2013) Ionic Liquid as an Efficient and Recyclable Reaction Medium for the Synthesis of Pyrido[2,3- d ]pyrimidines . Journal of Heterocyclic Chemistry 50:3, pages 534-538.
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Pratibha Rai, Madhulika Srivastava, Jaya Singh & Jagdamba Singh. (2013) An eco-efficient, domino synthesis of highly functionalized spiro-oxindole derivatives catalyzed by an organocatalyst in an aqueous medium. RSC Advances 3:41, pages 18775.
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Pranabes Bhattacharyya, Sanjay Paul & Asish R. Das. (2013) Facile synthesis of pyridopyrimidine and coumarin fused pyridine libraries over a Lewis base-surfactant-combined catalyst TEOA in aqueous medium. RSC Advances 3:10, pages 3203.
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Sanny Verma & Suman L. Jain. (2012) Thiourea dioxide in water as a recyclable catalyst for the synthesis of structurally diverse dihydropyrido[2,3-d]pyrimidine-2,4-diones. Tetrahedron Letters 53:21, pages 2595-2600.
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Shahrzad Abdolmohammadi & Saeed Balalaie. (2012) An Efficient Synthesis of Pyrido[2,3-<i>d</i>]pyrimidine Derivatives via One-Pot Three-Component Reaction in Aqueous Media. International Journal of Organic Chemistry 02:01, pages 7-14.
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Qi Han, Hui-Yin Li, Yossi Zafrani, Eytan Gershonov & Ishay Columbus. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
Subhasis Samai, Ganesh Chandra Nandi, Sushobhan Chowdhury & Maya Shankar Singh. (2011) l-Proline catalyzed synthesis of densely functionalized pyrido[2,3-d]pyrimidines via three-component one-pot domino Knoevenagel aza-Diels–Alder reaction. Tetrahedron 67:33, pages 5935-5941.
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Jairo Quiroga, Jorge Trilleras, Jaime Gálvez, Braulio Insuasty, Rodrigo Abonía, Manuel Nogueras & Justo Cobo. (2009) 5-Cyanoacetylpyrimidines as intermediates for 7-aryl-6-cyanopyrido[2,3-d]pyrimidin-5-ones. Tetrahedron Letters 50:46, pages 6404-6406.
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Saeed Balalaie, Shahrzad Abdolmohammadi & Bita Soleimanifard. (2009) An Efficient Synthesis of Novel Hexahydropyrido[2,3‐ d ]pyrimidine Derivatives from (Arylmethylidene)pyruvic Acids (=(3 E )‐4‐Aryl‐2‐oxobut‐3‐enoic Acids) in Aqueous Media . Helvetica Chimica Acta 92:5, pages 932-936.
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K.C. Majumdar, B. Sinha, P.K. Maji & S.K. Chattopadhyay. (2009) Palladium-catalyzed intramolecular arylation of pyrimidines: a novel and expedient avenue to benzannulated pyridopyrimidines. Tetrahedron 65:14, pages 2751-2756.
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Xiang-Shan Wang, Zhao-Sen Zeng, Da-Qing Shi, Shu-Jiang Tu, Xian-Yong Wei & Zhi-Min Zong. (2019) Synthesis of 5,7-Diarylpyrido[2,3- d ]Pyrimidine Derivatives catalysed by Kf-Alumina . Journal of Chemical Research 2006:7, pages 440-442.
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Xiang‐shan Wang, Zhao‐sen Zeng, Da‐qing Shi, Xian‐yong Wei & Zhi‐min Zong. (2005) KF‐Alumina Catalyzed One‐Pot Synthesis of Pyrido[2,3‐d]pyrimidine Derivatives.. ChemInform 36:19.
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