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Materials Technology
Advanced Performance Materials
Volume 39, 2024 - Issue 1
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Research Article

Tinospora malabarica leaf extract fractions-derived silver nanoparticles and their spectral characterisation: evaluation of their toxicity properties against agricultural pests Spodoptera litura and Helicoverpa armigera

, , , , , , , & show all
Article: 2361221 | Received 11 Feb 2024, Accepted 23 May 2024, Published online: 11 Jun 2024

Figures & data

Figure 1. Floral collection and extract preparation.

Figure 1. Floral collection and extract preparation.

Figure 2. Collection of S. litura from around Mayiladuthurai district.

Figure 2. Collection of S. litura from around Mayiladuthurai district.

Figure 3. Collection of H. armigera from around Mayiladuthurai district.

Figure 3. Collection of H. armigera from around Mayiladuthurai district.

Figure 4. Bioassay experimental setup of Tm-LMF and AgNPs against S. litura.

Figure 4. Bioassay experimental setup of Tm-LMF and AgNPs against S. litura.

Figure 5. Bioassay experimental setup of Tm-LMF and AgNPs against H. armigera.

Figure 5. Bioassay experimental setup of Tm-LMF and AgNPs against H. armigera.

Table 1. Phytochemical screening of hexane, diethyl ether, dichloromethane, ethyl acetate and methanol extracts T. malabarica.

Figure 6. Various fractionation units (a) air shield TLC, (b) CC unit.

Figure 6. Various fractionation units (a) air shield TLC, (b) CC unit.

Figure 7. UV-vis spectroscopy analysis of Tm-LME of AgNPs.

Figure 7. UV-vis spectroscopy analysis of Tm-LME of AgNPs.

Figure 8. FTIR spectrum analysis of fraction V obtained from Tm-LME of AgNPs.

Figure 8. FTIR spectrum analysis of fraction V obtained from Tm-LME of AgNPs.

Table 2. FTIR spectra analysis of AgNPs obtained from Tm-LME.

Figure 9. SEM of synthesized AgNPs of Tm-LME.

Figure 9. SEM of synthesized AgNPs of Tm-LME.

Figure 10. SEM-EDX of synthesized AgNPs on the outer and inner surface of Tm-LME.

Figure 10. SEM-EDX of synthesized AgNPs on the outer and inner surface of Tm-LME.

Table 3. Larval toxicity induced by Tm-LMF on the larvae of selected polyphagous insect pests.

Table 4. Pupicidal toxicity induced by Tm-LMF on the larvae of selected polyphagous insect pests.

Table 5. Larval toxicity induced by Tm-AgNPs on the larvae of selected polyphagous insect pests.

Table 6. Pupicidal toxicity induced by Tm-AgNPs on the larvae of selected polyphagous insect pests.

Table 7. Enzyme activities (in µmol/mg/h−1) of fourth instar larvae of S. litura, H. armigera and A. janata fed on their respective host plant treated with different fractions.

Data availability statement

The authors confirm that the data supporting the findings of this study are available within the article.