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Articles

Method development and evaluation for the determination of perfluoroalkyl and polyfluoroalkyl substances in multiple food matrices

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Pages 752-776 | Received 19 Oct 2021, Accepted 06 Dec 2021, Published online: 04 Feb 2022

Figures & data

Figure 1. Chromatograms of individual PFASs, note Br-PFOS and L-PFOS appear in the same trace. A and B – carboxylic acids and sulfonate traces, while C shows PAP traces.

Figure 1. Chromatograms of individual PFASs, note Br-PFOS and L-PFOS appear in the same trace. A and B – carboxylic acids and sulfonate traces, while C shows PAP traces.

Figure 1. (Continued).

Figure 1. (Continued).

Figure 1. (Continued).

Figure 1. (Continued).

Table 1. Analyte information including transitions monitored, surrogate standard selection and linearity of response established using LC-MS/MS

Table 2. List of surrogates and performance standards

Figure 2. Proficiency test z-scores for PFASs in fish and prawns; note PFOA and ΣPFOS data provided in graphical abstract.

Figure 2. Proficiency test z-scores for PFASs in fish and prawns; note PFOA and ΣPFOS data provided in graphical abstract.

Figure 3. Proficiency test z-scores for PFASs in proficiency test materials; note PFOA and ΣPFOS data provided in graphical abstract.

Figure 3. Proficiency test z-scores for PFASs in proficiency test materials; note PFOA and ΣPFOS data provided in graphical abstract.

Table 3. Instrumental limits of detection (LOD) and limits of quantification (LOQ) determined for method analytes

Table 4. Summary of recovery information for analytes in canned fish samples

Table 5. Summary of recovery information for analytes in pizza

Table 6. Summary of recovery information for analytes in chicken nuggets

Table 7. Summary of recovery information for analytes in spinach

Supplemental material

Supplemental Material

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