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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 5
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Original Articles

Improved Solvent‐Free Dakin Oxidation Protocol

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Pages 784-788 | Received 05 Sep 2007, Published online: 15 Feb 2008
 

Abstract

A solvent‐free Dakin reaction with mCPBA was accomplished with various aromatic aldehydes, resulting in an easy and improved methodology for the preparation of corresponding phenols. 3,4‐Methylenedioxyphenol, 3,4‐dimethoxyphenol, 4‐methoxyphenol, 4‐chlorophenol, and other functionalized phenols were obtained in high yields from the corresponding aromatic aldehydes in a few minutes. This new methodology represents an efficient alternative for this important synthetic conversion.

Acknowledgments

Thanks are due to Conselho Nacional de Desenrolvimento Científico e Tecnológico (CNPq, BR) and Fundação Carlos Chagas Filho de Amparo a Pesquisa do Estado do Rio de Janeiro (FAPERJ, BR) for financial support and fellowships.

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