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International Journal of Polymer Analysis and Characterization Volume 21, 2016 - Issue 1
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Original Articles

Sequence distribution of PMMA/iBuA copolymer by incremental calculation of 13C NMR spectra

Maria SiołekInstitute of Chemistry, Department of Materials Chemistry and Technology, Silesian University, Katowice, Poland;Research and Development Center, Synthos S.A., Oświęcim, Poland
,
Norbert HenzelInstitute of Electronics, Silesian Technical University, Gliwice, Poland
&
Marek MatlengiewiczInstitute of Chemistry, Department of Materials Chemistry and Technology, Silesian University, Katowice, PolandCorrespondence[email protected]
Pages 69-76 | Received 11 Aug 2015, Accepted 05 Sep 2015, Published online: 30 Nov 2015
 
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ABSTRACT

An incremental method for characterizing triad and pentad distribution by 13C NMR spectroscopy was applied to the poly(methyl methacrylate-co-isobutyl acrylate) copolymer. Calculation of the intensity of individual lines was performed applying Bernoulli statistics, while the chemical shifts for each sequence were calculated by an incremental method. Based on these data, the carbonyl signal was simulated yielding good agreement at the triad and pentad level.

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