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International Journal of Polymer Analysis and Characterization Volume 21, 2016 - Issue 1
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Original Articles

Sequence distribution of PMMA/iBuA copolymer by incremental calculation of 13C NMR spectra

Maria SiołekInstitute of Chemistry, Department of Materials Chemistry and Technology, Silesian University, Katowice, Poland;Research and Development Center, Synthos S.A., Oświęcim, Poland
,
Norbert HenzelInstitute of Electronics, Silesian Technical University, Gliwice, Poland
&
Marek MatlengiewiczInstitute of Chemistry, Department of Materials Chemistry and Technology, Silesian University, Katowice, PolandCorrespondence[email protected]
Pages 69-76 | Received 11 Aug 2015, Accepted 05 Sep 2015, Published online: 30 Nov 2015

References

  • Matlengiewicz, M. 2011. Microstructure analysis of acrylate-methacrylate copolymers by 13C NMR spectroscopy. In Encyclopedia of Analytical Chemistry, Suppl. Vols. S1–S3, ed. R. A. Meyers pp. 725–738. Chichester, UK: John Wiley.
  • Matlengiewicz, M., G. Nguyen, D. Nicole, and N. Henzel. 2000. Analysis of β-CH2 signals in the 13C NMR spectra of the methyl methacrylate-ethyl acrylate copolymer as a tool for microstructure determination. J. Polym. Sci. Part A Polym. Chem. 38:2147–2155.
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  • Aerdts, A. M., A. L. German, and G. P. M. van der Velden. 1994. Determination of the reactivity ratios, sequence distribution and stereoregularity of butyl acrylate-methyl methacrylate copolymers by means of proton and carbon-13 NMR. Magn. Reson. Chem. 32(Suppl 1):S80–S88.
  • San Roman J., and M. Valero. 1990. Quantitative evaluation of sequence distribution and stereoregularity in ethyl acrylate-methyl methacrylate copolymers by 13C n.m.r. spectroscopy. Polymer 31:1216–1221.
  • Nguyen, G., D. Nicole, M. Swistek, M. Matlengiewicz, and B. Wiegert. 1997. Sequence distribution of the methyl methacrylate–ethyl acrylate copolymer by 13C NMR spectroscopy. Polymer 38:3455–3461.
  • Nguyen, G., M. Matlengiewicz, and D. Nicole. 1999. Incremental method for determination of sequence distribution of poly(methyl methacrylate) by 13C NMR spectroscopy. Analusis 27:847–853.
  • Bujak, P., M. Matlengiewicz, and N. Henzel. 2007. Incremental calculation of sequence distribution of poly(butyl acrylate). Int. J. Polym. Anal. Charact. 12:95–104.

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