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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 196, 2021 - Issue 4
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Original Articles

Ultrasound-promoted, rapid and green synthesis of phosphonamide derivatives under catalyst and solvent-free conditions

Fouzia Bouchareba Laboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Faculty of Sciences, Department of Chemistry, Badji-Mokhtar – Annaba University, Annaba, Algeria;b Department of Chemistry, Faculty of Sciences and Technology, Chadli Bendjedid – EL Tarf University, El Tarf, AlgeriaView further author information
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Malika Berredjema Laboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Faculty of Sciences, Department of Chemistry, Badji-Mokhtar – Annaba University, Annaba, AlgeriaCorrespondence[email protected] [email protected]
View further author information
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Abdeslem Bouzinaa Laboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Faculty of Sciences, Department of Chemistry, Badji-Mokhtar – Annaba University, Annaba, AlgeriaView further author information
&
Meriem Guerfia Laboratory of Applied Organic Chemistry, Synthesis of Biomolecules and Molecular Modelling Group, Faculty of Sciences, Department of Chemistry, Badji-Mokhtar – Annaba University, Annaba, AlgeriaView further author information
Pages 422-430 | Received 04 Aug 2020, Accepted 18 Nov 2020, Published online: 14 Dec 2020
 
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Abstract

We report a rapid, efficient, economic, environmentally benign, and easy to scale-up method for the synthesis of phosphonamide derivatives using ultrasound irradiation, under catalyst and solvent-free conditions starting from the corresponding amine and phenyl phosphonic dichloride. The reaction was achieved in excellent isolated yield in a short reaction time at room temperature. The structures of the synthesized compounds are confirmed by elemental analysis as well as by IR and 1H, 13C, 31P NMR spectroscopic data and mass spectrometry.

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Disclosure statement

No potential conflict of interest was reported by the author(s).

Additional information

Funding

This work was supported financially by The General Directorate for Scientific Research and Technological Development (DG-RSDT), Algerian Ministry of Scientific Research, Applied Organic Chemistry Laboratory (FNR 2000).

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