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Integrated Ferroelectrics
An International Journal
Volume 205, 2020 - Issue 1: Proceedings of the International Conference on Nano-Structured Materials and Devices (ICNSMD-2018): Part IV of IV
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Section F: Other Emerging Areas

Structural, Mechanical and Dielectric Properties of Microwave-Assisted High-Energy Ball Milling Synthesis of Hydroxyapatite

Sujata SwainDepartment of Physics and Astronomy, National Institute of Technology, Rourkela, India;
,
Sk. Muneer A.Department of Physics and Astronomy, National Institute of Technology, Rourkela, India;
,
R. SahuDepartment of Physics and Astronomy, National Institute of Technology, Rourkela, India;
,
A. MahapatraDepartment of Physics and Astronomy, National Institute of Technology, Rourkela, India;
,
R. R. NegiDepartment of Physics and Astronomy, National Institute of Technology, Rourkela, India;
,
B. SamantaDepartment of Physics and Astronomy, National Institute of Technology, Rourkela, India;
,
D. NandaDepartment of Physics and Astronomy, National Institute of Technology, Rourkela, India;
,
P. KumarDepartment of Physics and Astronomy, National Institute of Technology, Rourkela, India; Correspondence[email protected]
,
S. DasguptaDepartment of Ceramic Engineering, National Institute of Technology, Rourkela, India;
&
SoniaDepartment of Chemistry, Govt. (A) College, Rourkela, India
 show all
Pages 186-193 | Received 01 Oct 2018, Accepted 12 Aug 2019, Published online: 09 Feb 2020
 
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Abstract

In the present work, the effect of high-energy ball milling (HEBM) of starting precursors of hydroxyapatite (Ca10(PO4)6(OH)2)/HA system on the processing temperature, morphological, mechanical, and electrical properties are highlighted. Calcination and sintering of HA system were carried out in microwave furnace. XRD study confirmed the evolution of HA phase and EDX analysis confirmed Ca/P ratio ∼1.65. Grain size of HA samples, synthesized by using microwave-assisted HEBM technique was found to be in the order of 54–75 nm. Enhanced dielectric and mechanical properties were obtained in HA samples.

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