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Research article

Tribological study of magnesium-based AZ91/TiC/rGO hybrid composite prepared by powder metallurgy route: an experimental and analytical approach

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Accepted 23 Jun 2024, Published online: 01 Jul 2024
 

ABSTRACT

In this research, hybrid composites of magnesium alloy (AZ91) reinforced with titanium carbide (TiC) and reduced graphene oxide (rGO) were studied. The powder metallurgy method was used to synthesise magnesium alloy-based hybrid composites. The tribological behaviour of fabricated composite samples was examined using a pin-on-disc tribotester per the ASTM G99 standard. Using the Taguchi method, the design of the experiment (DOE) was constructed. The L9 orthogonal array opted for tribo-performance evaluation. Also, an ANOVA and regression analysis were carried out to ascertain the relative impact of the tribological factors on the responses. In the present investigation, three variable factors were considered, i.e. reinforcement percentage of TiC (0–10%) keeping constant 0.5 wt.% rGO, disc sliding velocity (0.5 to 1.5 m/s), and applied load varies between 10 and 30 N. It was found that the load parameter had a considerable impact on both the wear rate (WR) and the coefficient of friction (COF). Sliding velocity, on the other hand, had a minimal effect on WR. The concentration of reinforcement exhibits a moderate effect. Taguchi’s predictive results were also compared with experimental results. The worn surfaces were analysed using scanning electron microscopy (SEM), and surface roughness was used for wear mechanics analysis.

Nomenclature

MMCs=

Metal matrix composites

HMMMCs=

Hybrid magnesium metal matrix composites

TiC=

Titanium carbide

rGO=

Reduced graphene oxide

Mg=

Magnesium

Al=

Aluminium

PM=

Powder metallurgy

LVDT=

Linear Variable Differential Transformer

wt.%=

Weight percentage

N=

Newton

m/s=

Meter per second

Ts=

Sintering temperature

DOE=

Design of the experiment

ASTM=

American Society for Testing and Materials

μm=

Microns meter

nm=

Nano meter

WR=

Wear rate

COF=

Coefficient of friction

SEM=

Scanning Electron Microscopy

FESEM=

Field emission scanning electron microscopy

EDX=

Energy dispersive X-ray

S/N=

Signal-to-noise

ANOVA=

Analysis of variance

Tm=

Melting temperature

Disclosure statement

No potential conflict of interest was reported by the author(s).

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