Structure and properties of solid state diffusion bonding of 17-4PH stainless steel and titanium

Abstract

Solid state diffusion bonded joint between titanium and 17-4 precipitation hardening stainless steel was carried out in the temperature range of 800–1050°C in steps of 50°C for 30 min and also at 950°C for 30–180 min in steps of 30 min under a uniaxial pressure of 3·5 MPa in vacuum. Bonded samples were characterised using light microscopy, field emission scanning electron microscopy and X-ray diffraction technique. Up to 850°C for 30 min, FeTi phase was formed at the diffusion interface; however, α-Fe+λ, χ, Fe₂Ti and FeTi phases and phase mixtures were formed above 850°C for 30 min and at 950°C for all bonding times. Maximum tensile strength of ∼326 MPa, shear strength of ∼254 MPa and impact toughness of ∼24 J were obtained for the diffusion couple processed at 1000°C for 30 min and 30–180 min time interval at 950°C, and maximum tensile strength ∼323 MPa, shear strength ∼243 MPa and impact toughness of ∼22 J were achieved when bonding was processed for 120 min. The residual stress of the bonded joints increases with the increase in bonding temperatures and times.

Keywords:

• Diffusion bonding
• Scanning electron microscopy
• Strength
• Impact toughness