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Agricultural and Biological Chemistry Volume 52, 1988 - Issue 9
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Organic Chemistry

Optical Resolution of (±)-Metyrosine

Hiroyuki SaitoCentral Research Laboratory, Nisshin Flour Milling Co., Ltd., Tsurugaoka, Oimachi, Iruma-gun, Saitama 354, Japan
,
Tahara YoshiyukiCentral Research Laboratory, Nisshin Flour Milling Co., Ltd., Tsurugaoka, Oimachi, Iruma-gun, Saitama 354, Japan
&
Masashi ToyodaCentral Research Laboratory, Nisshin Flour Milling Co., Ltd., Tsurugaoka, Oimachi, Iruma-gun, Saitama 354, Japan
Pages 2349-2350 | Received 04 Mar 1988, Published online: 06 Jun 2016

References

  • H. R. Almond, Jr., D. T. Manning and C. Niemann, Biochemistry, 1, 243 (1962).
  • J. S. Amato, W. M. Leonard and S. Karady, U. S. Patent 4,508,921 (Apr. 2, 1985).
  • Merck & Co., Inc., Neth. Appl. 6,607,757 (Dec. 5, 1966).
  • D. F. Hinkeley, Fr. Patent 1,502,949 (Nov. 24, 1967).
  • F. Bjorkling, J. Boutelje, S. Gatenbeck, K. Hult and T. Norin, Tetrahedron Lett., 26, 4957 (1985).
  • K. T. Potts, J. Chem. Soc., 1955, 1632.
  • K. Weinges, G. Grabb, D. Nagel and B. Stemmle, Chem. Ber., 104, 3594 (1971).
  • We used the specific rotation to determine the optical purity of (−)-metyrosine, because our attempt to separate the enantiomers by liquid chromatographic and NMR methods were fruitless.
  • The United States Pharmacopeia, XXI, 693 (1985).

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