123
Views
7
CrossRef citations to date
0
Altmetric
Pharmaceutical Analysis

Simultaneous Determination of Dipyrone and Papaverine in Pharmaceutical Formulation using PLS Regression and UV Spectrophotometry

, , &
Pages 975-986 | Received 07 Apr 2006, Accepted 31 Jul 2006, Published online: 04 Apr 2007

References

  • Abdel‐Ghani , N. T. , Shoukry , A. F. , Issa , Y. M. and Wahdan , O. A. 2002 . Spectrophotometric determination of meclozine HCl and papaverine HCl in their pharmaceutical formulations . J. Pharm. Biomed. Anal. , 28 : 373 – 378 .
  • Albuquerque , J. S. , Silva , V. L. , Lima , F. , Araujo , A. N. and Montenegro , M.C. B.S.M. 2003 . Determination of dipyrone in pharmaceutical products by flow injection analysis with potentiometric detection . Anal. Sci. , 19 : 691 – 694 .
  • Altun , M. L. 2002 . HPLC method for the analysis of paracetamol, caffeine and dipyrone . Turk. J. Chem. , 26 : 521 – 528 .
  • Annual Book of ASTM Standards . 2000 . E1655‐00 Norm West Conshohocken, , USA : ASTM International .
  • Bella , A. J. and Brock , G. B. 2004 . Intracavernous pharmacotherapy for erectile dysfunction . Endocrine , 23 : 149 – 155 .
  • Blanco , M. , Coello , J. , Iturriaga , H. , Maspoch , S. and de la Pezuela , C. 1998 . Near‐infrared spectroscopy in the pharmaceutical industry . Analyst , 123 : 135R – 150R .
  • Braga , J. W. and Poppi , R. J. 2004a . Validation of models of multivariate calibration: an application in the determination of polymorphic purity of carbamazepine by near infrared spectroscopy . Quim. Nova , 27 : 1004 – 1011 .
  • Braga , J. W. and Poppi , R. J. 2004b . Figures of merit for the determination of the polymorphic purity of carbamazepone by infared spectroscopy and multivariate calibration . J. Pharm. Sci. , 93 : 2124 – 2134 .
  • Brereton , R. G. 2000 . Introduction to multivariate calibration in analytical chemistry . Analyst , 125 : 2125 – 2154 .
  • Compendium for Analytical Terminology . 2002 . ⟨http://www.iupac.org/publications/analytical_compendium/⟩ (5 June 2006)
  • Damiani , P. C. , Moschetti , A. C. , Rovetto , A. J. , Benavente , F. and Olivieri , A. C. 2005 . Design and optimization of a chemometrics‐assisted spectrophotometric method for the simultaneous determination of levodopa and carbidopa in pharmaceutical products . Anal. Chim. Acta , 543 : 192 – 198 .
  • de la Pena , A. M. , Mansilla , A. E. , Gomez , D. G. , Olivieri , A. C. and Goicoechea , H. C. 2003 . Interference‐free analysis using three‐way fluorescence data and the parallel factor model. Determination of fluoroquinolone antibiotics in human serum . Anal. Chem. , 75 : 2640 – 2646 .
  • Dinc , E. and Baleanu , D. 2002 . Spectrophotometric quantitative determination of cilazapril and hydrochlorothiazide in tablets by chemometric methods . J. Pharm. Biomed. Anal. , 30 : 715 – 723 .
  • Elad , D. and Ginsburg , D. 1952 . The synthesis of papaverine . Bull. Narcotics , 3 : 27 – 34 .
  • Eppelsheim , C. , Aubeck , R. , Hampp , N. and Brauchle , C. 1991 . Determination of ethaverine and papaverine using ion‐selective electrodes . Analyst , 116 : 1001 – 1003 .
  • Ergun , H. , Bagdatoglu , C. , Ugur , H. C. , Temiz , C. , Attar , A. , Egemen , N. and Tulunay , F. C. 2000 . The vasorelaxant effect of dipyrone on an experimental cerebral vasospasm model in rabbits . Neurol. Res. , 22 : 815 – 818 .
  • Ferre , J. , Brown , S. D. and Rius , F. X. 2001 . Improved calculation of the net analyte signal in inverse multivariate calibration . J. Chemom. , 15 : 537 – 553 .
  • Firlik , K. S. , Kaufmann , A. M. , Firlik , A. D. , Jungreis , C. A. and Yonas , H. 1999 . Intra‐arterial papaverine for the treatment of cerebral vasospasm following aneurysmal subarachnoid hemorrhage . Surg. Neurol. , 51 : 66 – 74 .
  • Gallego , J. M.L. and Arroyo , J. P. 2002 . Spectrophotometric determination of hydrocortisone, nystatin and oxytetracycline in synthetic and pharmaceutical preparations based on various univariate and multivariate methods . Anal. Chim. Acta , 460 : 85 – 97 .
  • Goicoechea , H. C. and Olivieri , A. C. 1999 . Enhanced synchronous spectrofluorometric determination of tetracycline in blood serum by chemometric analysis. Comparison of partial least‐squares and hybrid linear analysis calibrations . Anal. Chem. , 71 : 4361 – 4368 .
  • International Conference on Harmonization . 1997 . ICH Harmonised Tripartite Guideline‐Validation of analytical procedures: Methodology . Fed. Regist. , 62 : 11260
  • Izolani , A. O. , de Moraes , M. T. and Tellez , C. A. 2003 . Fourier transform Raman spectroscopy of drugs: quantitative analysis of 1‐phenyl‐2,3‐dimethyl‐5‐pyrazolone‐4‐methylaminomethane sodium sulfonate: (dipyrone) . J. Raman Spectrosc. , 34 : 837 – 843 .
  • Jin , Y. , Mi , J. Q. , He , H. T. , Guo , Z. Q. , Zhao , M. P. and Chang , W. B. 2005 . Development of an indirect competitive ELISA for the determination of papaverine . Talanta , 66 : 1005 – 1011 .
  • Lima , J. L.F.C. , Sa , S. M.O. , Santos , J. L.M. and Zagatto , E. A.G. 2003 . Multi‐pumping flow system for the spectrophotometric determination of dipyrone in pharmaceutical preparations . J. Pharm. Biomed. Anal. , 32 : 1011 – 1017 .
  • Magnuszewska , B. , Ostrowska , J. and Figaszewski , Z. 2000 . Determination of papaverine hydrochloride in injections with an ion‐selective electrode . Chem. Anal.‐Warsaw , 45 : 105 – 115 .
  • Majlat , P. , Helboe , P. and Kristensen , A. K. 1981 . Separation and quantitative‐determination of homatropine methylbromide and opium‐alkaloids in admixture in pharmacutical preparation by gas‐liquid and high‐performance liquid‐chromatography . Int. J. Pharm. , 9 : 245 – 255 .
  • Martens , H. and Naes , T. 1989 . Multivariate Calibration Chichester, , USA : Wiley .
  • Medeiros , E. P. , Castro , S. L. , Formiga , F. M. , Santos , S. R.B. , Araujo , M. C.U. and Nascimento , V. B. 2004 . A flow injection method for biamperometric determination of dipyrone in pharmaceuticals . Microchem. J. , 78 : 91 – 96 .
  • Miller , J. N. and Miller , J. C. 2000 . Statistics for Analytical Chemistry , 4th ed. Harlow, , USA : Prentice Hall .
  • MillerIhli , N. J. , Ohaver , T. C. and Harnly , J. M. 1984 . Calibration and curve fitting for extended range AAS . Spectrochim. Acta B , 39 : 1603 – 1614 .
  • Mirzaeva , K. A. , Akhmedova , M. S. , Ramazanov , A. S. and Akhmedov , S. A. 2004 . Extraction‐photometric determination of dimedrol and papaverine in pharmaceutical dosage forms . J. Anal. Chem. , 59 : 215 – 218 .
  • Moreira , A. B. , Dias , I. L.T. , Neto , G. O. , Zagatto , E. A.G. , Ferreira , M. M.C. and Kubota , L. T. 2005 . Solid‐phase spectrofluorimetric determination of acetylsalicylic acid and caffeine in pharmaceutical preparations using partial least‐squares multivariate calibration . Talanta , 67 : 65 – 69 .
  • Moussa , A. F.A. 1978 . Spectrophotometric determination of PAS in presence of its degradation product M‐aminophenol . Pharmazie , 33 : 460 – 461 .
  • Sena , M. M. and Poppi , R. J. 2004a . N‐way PLS applied to simultaneous spectrophotometric determination of acetylsalicylic acid, paracetamol and caffeine . J. Pharm. Biomed. Anal. , 34 : 27 – 34 .
  • Sena , M. M. , Chaudhry , Z. F. , Collins , C. H. and Poppi , R. J. 2004b . Direct determination of diclofenac in pharmaceutical formulations containing B vitamins by using UV spectrophotometry and partial least square regression . J. Pharm. Biomed. Anal. , 36 : 743 – 749 .
  • Sena , M. M. , Trevisan , M. G. and Poppi , R. J. 2006 . Combining standard addition method and second‐order advantage for direct determination of salicylate in undiluted human plasma by spectrofluorimetry . Talanta , 68 : 1707 – 1712 .
  • Senyuva , H. Z. , Aksahin , I. , Ozcan , S. and Kabasakal , B. V. 2005 . Rapid, simple and accurate liquid chromatography‐diode array detection validated method for the determination of dipyrone in solid and liquid dosage forms . Anal. Chim. Acta , 547 : 73 – 77 .
  • Shamloul , R. , Atteya , A. , Elnashaar , A. , Gadallah , A. , Zohdy , W. and Abdelsalam , W. 2005 . Intracavernous sodium nitroprusside (SNP) versus papaverine/phentolamine in erectile dysfunction: a comparative study of short‐term efficacy and side‐effects . J. Sex. Med. , 2 : 117 – 120 .
  • Smith , W. S. , Dowd , C. F. , Johnston , C. , Ko , N. U. , DeArmond , S. J. , Dillon , W. P. , Setty , D. , Lawton , M. T. , Young , W. L. , Higashida , R. T. and Halbach , V. V. 2004 . Neurotoxicity of intra‐arterial papaverine preserved with chlorobutanol used for the treatment of cerebral vasospasm after aneurysmal subarachnoid hemorrhage . Stroke , 35 : 2518 – 2522 .
  • Teixeira , M. F.S. , Marcolino‐Junior , L. H. , Fatibello , O. , Dockal , E. R. and Cavalheiro , E. T.G. 2004 . Voltammetric determination of dipyrone using a N,N‐ethylenebis(salicylideneaminato)oxovanadium(IV) modified carbon‐paste electrode . J. Braz. Chem. Soc. , 15 : 803 – 808 .
  • The British Pharmacopoeia . 2002 . Vol. II , London, , UK : Stationery Office .
  • Trevisan , M. G. and Poppi , R. J. 2003 . Determination of doxorubicin in human plasma by excitation‐emission matrix fluorescence and multi‐way analysis . Anal. Chim. Acta , 493 : 69 – 81 .
  • United States Pharmacopoeia . 2005 . Rockville, , USA : United States Pharmacopoeial Convention .
  • Zhang , S. , Zhuang , Y. F. and Ju , H. X. 2004 . Flow‐injection chemiluminescence determination of papaverine using cerium (IV)‐sulfite system . Anal. Lett. , 37 : 143 – 155 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.