180
Views
26
CrossRef citations to date
0
Altmetric
ENVIRONMENTAL ANALYSIS

Solid Phase Extraction and Determination of Lead in Water Samples Using Silica Gel Homogeneously Modified by Thiosalicylic Acid

&
Pages 2524-2543 | Received 23 Apr 2007, Accepted 01 Jun 2007, Published online: 29 Oct 2007

References

  • Akman , S. , Ince , H. and Koklu , U. 1992 . Determination some trace metals in sea‐water by atomic absorption spectrometry after concentration with modified silicas . J. Anal. Atomic Spectrom. , 7 : 187 – 189 .
  • Camel , V. 2003 . Review solid phase extraction of trace elements . Spectrochimica Acta Part B. , 58 : 1177 – 1233 .
  • Cornelis , R. 2005 . Handbook of Elemental Speciation II‐Species in Environment Food, Medicine and Occupational Health West Sussex, , England : John Wiley and Sons .
  • Dogan , C. E. and Koklu , U. 2006 . Sorption and preconcentration of vanadium, chromium, manganese and lead on silica gel modified with 3‐mercaptopropyl trimethoxysilane . Instrumentation Science and Technology , 34 ( 3 ) : 359 – 366 .
  • Ekinci , C. and Koklu , U. 2000 . Determination of vanadium, manganese, silver and lead by graphite furnace atomic absorption after preconcentration on silica gel modified with 3‐aminopropyltriethoxysilane . Spectrochimica Acta Part B. , 55 : 1491 – 1495 .
  • Goswami , A. and Singh , A. K. 2002 . Silica gel functionalized with resacetophenone:synthesis of a new chelating matrix and its application as metal ion collector for their flame atomic absorption spectrometric determination . Analytica Chimica Acta , 454 : 229 – 240 .
  • Ince , H. , Akman , S. and Koklu , U. 1992 . Sorption and preconcentration of copper and cadmium on silica gel modified 3‐aminopropyltriethoxysilane. Fresenius . J. Anal. Chem. , 342 : 560 – 562 .
  • Jal , P. K. , Patel , S. and Mishra , B. K. 2004 . Chemical modification of silica surface by immobilization of functional groups for extractive concentration of metal ions . Talanta , 62 : 1005 – 1028 .
  • Korn , M. G.A. , Andrade , J. B. , Jesus , D. J. , Lemos , V. A. , Bandeira , M. L.S.F. , Santos , W. N.L. , Bezerra , M. A. , Amorim , F. A.C. , Souzaand , A. S. and Ferreira , S. L.C. 2006 . Separation and preconcentration procedures for the determination of lead using spectrometric techniques: a review . Talanta , 69 : 16 – 24 .
  • Mahmoud , M. E. , Soayed , A. A. and Hafez , O. F. 2003 . Selective solid phase extraction and preconcentration of heavy metals from seawater by physically and chemically immobilized 4‐amino‐3‐hydroxy‐2‐(2‐chlorobenzene)‐azo‐1‐naphtalene sulfonic acid silica gel . Microchimica Acta , 143 ( 1 ) : 65 – 70 .
  • Minczewski , J. , Chwastowska , J. and Dybczynski , D. 1982 . Separation and Preconcentration Methods in Inorganic Trace Analysis 61 – 67 . Chichester : Ellis Horword .
  • Prado , A. G.S. , Sales , J. A.A. , Carvalho , R. M. , Rubim , J. C. and Airoldi , C. 2004 . Immobilization of 5‐amino‐1,3,4‐thiadiazole‐thiol onto silica gel surface by heterogeneous and homogenous routes . Journal of Non‐Crystalline Solids , 333
  • Ralph , I. K. 1979 . The Chemistry of Silica, Chapter 6 Wiley‐Interscience .
  • Soliman , E. M. , Mahmoud , M. E. and Ahmed , S. A. 2002 . Reactivity of thioglycolic acid physically and chemically bound to silica gel as new selective solid phase extractors for removal of heavy metal ions from natural water samples . Inter. J. Environ. Anal. Chem. , 82 ( 6 ) : 403 – 413 .
  • Tewari , P. K. and Singh , A. K. 2002 . Preconcentration of lead with amberlite XAD‐2 and Amberlite XAD‐7 based chelating resins for its determination by flame atomic absorption spectrometry . Talanta , 56 : 735 – 744 .
  • Tuzen , M. , Soylak , M. and Elci , L. 2005 . Multi‐element pre‐concentration of heavy metal ions by solid phase extraction on chromorsorb 108 . Analytica Chimica Acta , 548 : 101 – 108 .
  • Tuzen , M. and Soylak , M. 2004 . Column system using diaion HP‐ MG for determination of some metal ions by flame atomic absorption spectrometry . Analytica Chimica Acta , 504 : 325 – 334 .
  • Vankatesh , G. , Singh , A. K. and Venkataramani , B. 2004 . Silica gel loaded with o‐dihydroxybenzene: design, metal sorption equilibrium studies and application to metal enrichment prior to determination by Flame Atomic Absorption Spectrometry . Microchimica Acta , 144 : 233 – 241 .
  • Zougagh , M. , Pavon , J. M.C. and Torres , A. G. 2005 . Chelating sorbents based on silica gel and their application in atomic spectrometry . Anal. Bioanal. Chem. , 381 : 1103 – 1113 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.