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Original Articles

Formylation of Secondary Amines with Dialkyl Acetals of Dimethylformamide

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Pages 625-634 | Received 21 Feb 1980, Accepted 10 Mar 1980, Published online: 19 Dec 2006

References

  • Thenot , J. P. and Horning , E. C. 1972 . Anal. Lett. , 5 : 519 Callery, P.S., Stogniew, M., and Geelhaar, L.A., Biomed. Mass Spectrom. i, 23 (1979)
  • Meerwein , H. , Borner , P. , Fuchs , S. , Sasse , H. J. , Schrodt , H. and Spille , J. 1956 . Chem. Ber. , 89 : 2060 Meerwein, H., Florian, W., Schon, N. and Stopp, G., Liebigs Ann. 641, 1 (1961)
  • Narasimhachari , N. and Friedel , R. O. 1979 . Anal. Lett. , 12B : 77 ibid 12A, 1293 (1979)
  • Eckhardt , G. , Goebel , K. J. , Tondorf , G. and Goenechea , S. 1974 . Org. Mass Spectrom. , 9 : 1073
  • The formyl hydrogen of dimethylformamide appears at 8.02 ppm(ref. 6) while for dlethylformamide it is at 8.07 ppm (ref. 7)
  • Pouchert , C. J. and Campbell , J. R. 1974 . The Aldrich Library of NMR Spectra , 108 D Milwaukee : Aldrich Chemical Company Inc. .
  • 109 A The Aldrich Library of NMR Spectra
  • Carbonyl absorption in the infrared spectrum of dimethylformamide is at 1670 cm- (ref. 9) and for dibutylformand. de it is at 1665 cm (ref. 10).
  • Pouchert , C. J. 1974 . Aldrich Library of Infrared Spectra , 392 E Milwaukee : Aldrich Chemical Co., Inc. .
  • 392 F Aldrich Library of Infrared Spectra
  • DeJongh , D. C. , Nayar , M. S.B. , Patil , G. and Hanessian , S. 1978 . Tetrahedron , 34 : 1869

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