Analysis of Cyclosporin A and Main Degradation Impurities by Cyclodextrin–Modified Micellar Electrokinetic Chromatography

REFERENCES

• Bendazzoli , C. , E. Mileo , M. Lucarini , S. Olmo , V. Cavrini , and R. Gotti . 2010 . Capillary electrophoretic study on the interaction between sodium dodecyl sulfate and neutral cyclodextrins . Microchim. Acta 171 : 23 – 31 .
   Web of Science ®Google Scholar
• Borel , J. F. , C. Feuer , and H. U. Gubler . 1976. Biological effects of cyclosporin A: A new anti-lymphocite agent. Agents Act. 6: 468–475.
   PubMedGoogle Scholar
• Calne , R. Y. , S. Thirus , P. McMaster , G. N. Craddock , D. J. G. White , D. B. Evans , D. C. Dunn , B. D. Pentlow , and K. Rolles . 1978 . Cyclosporin A in patients receiving renal allografts from cadaver donors . Lancet 312 : 1323 – 1327 .
   Google Scholar
• Chen , S.-H. , H.-L. Wu , S.-L. Lin , and S.-M. Wu . 2000 . Micellar electrokinetic capillary chromatography of cyclosporin A in a commercial preparation . J. Liq. Chrom. 23 : 2761 – 2772 .
   Web of Science ®Google Scholar
• Cifuentes , A. , J. L. Bernal , and J. Diez-Masa . 1997 . Determination of critical micelle concentration values using capillary electrophoresis instrumentation . Anal. Chem. 69 : 4271 – 4274 .
   Web of Science ®Google Scholar
• Copper , C. L. , and M. J. Sepaniak . 1994 . Cyclodextrin-modified electrokinetic capillary chromatography separations of benzopyrene isomers: correlation with computationally derived host-guest energies . Anal. Chem. 66 : 147 – 154 .
   Web of Science ®Google Scholar
• Djordjevic , N. M. , F. Fitzpatrick , and F. Houdiere . 2001 . Separation of peptides utilizing ultrahigh-temperature micellar electrokinetic chromatography . Electrophoresis 22 : 2389 – 2402 .
   Google Scholar
• Friis , G. J. , and H. Bungaard . 1992 . Kinetics of degradation of cyclosporin A in acidic aqueous solution and its implication in its oral absorption . Int. J. Pharm. 82 : 79 – 83 .
   Web of Science ®Google Scholar
• Husek , A. 1997 . High-performance liquid chromatographic analysis of cyclosporin A and its oral solutions . J. Chromatogr. A 759 : 217 – 224 .
   PubMed Web of Science ®Google Scholar
• Jegorov , A. , L. Cvak , A. Husek , P. Šimek , A. Heydová , J. Ondráček , S. Pakhomova , M. Hušák , B. Kratochvíl , P. Sedmera , and V. Havlíček . 2000 . Synthesis and crystal structure determination of cyclosporin H . Collect. Czech. Chem. Commun. 65 : 1317 – 1328 .
   Web of Science ®Google Scholar
• Kumar , M. , S. K. Singhal , and A. Singh . 2001 . Development and validation of a stability indicating HPLC assay method for cyclosporine in cyclosporine oral solution USP . J. Pharm. Biomed. Anal. 25 : 9 – 14 .
   PubMed Web of Science ®Google Scholar
• Lucangioli , S. E. , E. Kenndler , A. Carlucci , V. P. Tripodi , S. L. Scioscia , and C. N. Carducci . 2003 . Relation between retention factors of immunosuppresive drugs in microemulsion electrokinetic chromatography with biosurfactants and octanol-water partition coefficients . J. Pharm. Biomed. Anal. 33 : 871 – 878 .
   PubMed Web of Science ®Google Scholar
• Magni , F. , C. Arcelloni , R. Paroni , I. Fermo , P. A. Bonini , M. Del Puppo , A. Manzocchi , and M. Galli Kienli . 1994 . Open-chain peptides obtained by acidic hydrolytic cleavage of cyclosporin A . Biol. Mass Spectr. 23 : 514 – 518 .
   Google Scholar
• Malaekeh-Nikouei , B. , H. Nassirli , and N. Davies . 2007 . Enhancement of cyclosporine aqueous solubility using α- and hydroxypropyl β-cyclodextrin mixtures . J. Incl. Phenom. Macrocycl. Chem. 59 : 245 – 250 .
   Web of Science ®Google Scholar
• Mileo , E. , P. Franchi , R. Gotti , C. Bendazzoli , E. Mezzina , and M. Lucarini . 2008 . An EPR method for measuring the rate of distribution of organic substrate between cyclodextrin, micelles and water . Chem. Comm. 11 : 1311 – 1313 .
   Web of Science ®Google Scholar
• Miyake , K. , F. Hirayama , and K. Uekama . 1999 . Solubility and mass and nuclear magnetic resonance spectroscopic studies on interaction of cyclosporin A with dimethyl-α- and β-cyclodextrins in aqueous solution . J. Pharm. Sci. 88 : 39 – 45 .
   PubMed Web of Science ®Google Scholar
• Mueller , W. , and B. Hermann . 1979 . Cyclosporin A for psoriasis . N. Engl. J. Med. 301 : 555 .
   PubMed Web of Science ®Google Scholar
• Nishi , H. , T. Fukuyama , and S. Terabe . 1991 . Chiral separation by cyclodextrin-modified micellar electrokinetic chromatography . J Chromatogr. 553 : 503 – 516 .
   Web of Science ®Google Scholar
• Nunes Bonifacio , F., M. Giocanti , J. P. Reynier , B. Lacarelle , and A. Nicolay . 2009 . Development and validation of HPLC method for the determination of cyclosporin A and its impurities in Neoral® capsules and its generic versions . J. Pharm. Biomed. Anal. 49 : 540 – 546 .
   PubMed Web of Science ®Google Scholar
• Oliyai , R. , and V. J. Stella . 1992. Kinetics and mechanism of isomerization of cyclosporin A. Pharm. Res. 9: 617–622.
   Web of Science ®Google Scholar
• Pyell , U. 2006 . Electrokinetic Chromatography. Theory, Instrumentation and Applications . Chichester , UK : Wiley .
   Google Scholar
• Sievert , H.-J. P. , and A. C. J. H. Drouen . 1993 . Spectral matching and peak purity . In Diode Array Detection in HPLC, Chromatographic Science Series , Vol. 62 , eds. L. Huber and S. A. George . New York : Marcell Dekker, Inc .
   Google Scholar
• Terabe , S. , Y. Miyashita , Y. Ishihama , and O. Shibata . 1993 . Cyclodextrin-modified micellar electrokinetic chromatography: Separation of hydrophobic and enantiomeric compounds . J. Chromatogr. 636 : 47 – 55 .
   Web of Science ®Google Scholar
• Tickle , D. C. , G. N. Okafo , P. Camilleri , R. F. D. Jones , and A. K. Kirby . 1994 . Glucopyranoside-based surfactants as pseudostationary phases for chiral separations in capillary electrophoresis . Anal. Chem. 66 : 4121 – 4126 .
   Web of Science ®Google Scholar