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LIQUID CHROMATOGRAPHY

Development and Validation of a Dispersive Solid Phase Extraction Liquid Chromatography Mass Spectrometry Method with Electrospray Ionization for the Determination of Multiclass Pesticides and Metabolites in Meat and Milk

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Pages 2526-2541 | Received 24 Mar 2013, Accepted 29 Apr 2013, Published online: 01 Oct 2013

REFERENCES

  • Anagnostopoulos , C. J. , P. Aplada Sarli , K. Liapis , S. A. Haroutounian , and G. E. Miliadis . 2012 . Validation of 2 variations of the QuEChERS method for the determination of multiclass pesticide residues in cereal based infant foods by LC-MS/MS . Food Anal. Method. 5 : 664 – 683 .
  • Anagnostopoulos , C. J. , P. Aplada Sarli , G. E. Miliadis , and S. Haroutounian . 2010 . Validation of the QuEChERS method for the determination of 25 priority pesticide residues in cereal based baby foods by gas chromatography with electron capture and nitrogen phosphorous detection . Hellen. Plant Protect. J. 3 ( 2 ): 1 – 80 .
  • Argauer , R. J. , K. I. Eller , R. M. Pfeil , and R. T. Brown . 1997 . Determining ten synthetic pyrethroids in lettuce and ground meat by using ion-trap mass spectrometry and electron-capture gas chromatography . J. Agric. Food Chem. 45 : 180 .
  • Barbini , D. A. , F. Vanni , S. Girolimetti , and R. Dommarco . 2007 . Development of an analytical method for the determination of the residues of four pyrethroids in meat by GC–ECD and confirmation by GC–MS . Anal. Bioanal. Chem. 389 : 1791 – 1798 .
  • Bogialli , S. , R. Curini , A. Di Corcia , A. Laganà , M. Nazzari , and S. M. Tonci . 2004 . Rapid assay for analyzing residues of carbamate insecticides in bovine milk: hot water extraction followed by liquid chromatography–mass spectrometry . J. Chromatogr. A 1054 : 351 – 357 .
  • Di Muccio , A. , P. Pelosi , I. Camoni , D. Attard Barbini , R. Dommarco , T. Generali , and A. Ausili . 1996 . J. Chromatogr. A 754 : 497 – 506 .
  • Doong , R. A. , and C. Y. Lee . 1999 . Determination of organochlorine pesticide residues in foods using solid-phase extraction clean-up cartridges . Analyst 1 : 124 – 1287 .
  • EFSA . 2006 . Conclusion regarding the peer review of the pesticide risk assessment of the active substance: carbaryl . EFSA Scientific Report 80 : 1 – 71 .
  • EU Pesticide Database . 2013 . http://ec.europa.eu/sanco_pesticides/public/index.cfm?event=homepage&CFID=7619061&CFTOKEN=22346621&jsessionid=080467a952d16f71247aTR
  • European Commission (EC) . 1997a . Appendix A: Metabolism and Distribution in Plants . 7028/IV/95-rev.3, 22/7/97, available at http://ec.europa.eu/food/plant/plant_protection_products/guidance_documents/docs/app-a.pdf
  • European Commission (EC) . 1997b . Appendix F: Metabolism and Distribution in Domestic Animals . 7030/VI/95 rev. 3, 22/7/97, available at: http://ec.europa.eu/food/plant/plant_protection_products/guidance_documents/docs/app-f.pdf
  • European Commission (EC) . 2002a . Commission Decision 2002/657/EC 2002 of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results . Off. J. Eur. Commun. L221 : 8 – 36 .
  • European Commission (EC) . 2002b . Commission Directive 2002/63/EC of 11 July 2002 establishing Community methods of sampling for the official control of pesticide residues in and on products of plant and animal origin and repealing Directive 79/700/EEC . Off. J. Eur. Commun. L 187 : 30 – 43 .
  • European Commission (EC) . 2005 . Regulation No 396/2005 of the European Parliament and of the council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC . Off. J. Eur. Commun. L70 : 1 – 16 .
  • European Commission (EC) . 2007 . Commission Decision 2007/355/EC 2007 of 21 May 2007 concerning the non-inclusion of carbaryl in Annex I to Council Directive 91/414/EEC and the withdrawal of authorisations for plant protection products containing that substance . Off. J. Eur. Commun. L133 : 40 – 41 .
  • European Commission (EC). 2011. Method Validation and Quality Control Procedures for Pesticide Residues Analysis in Food and Feed . Document No SANCO/12495/2011, available at: http://ec.europa.eu/food/plant/plant_protection_products/guidance_documents/docs/qualcontrol_en.pdf
  • Ferrer , C. , J. M. Gomez , J. F. Garcıa-Reyes , I. Ferrer , E. M. Thurman , and A. A. R. Fernandez . 2005 . Determination of pesticide residues in olives and olive oil by matrix solid-phase dispersion followed by gas chromatography/mass spectrometry and liquid chromatography/tandem mass spectrometry . J. Chromatogr. A 1069 (2): 183 – 194 .
  • Garrido-Frenich , A. , P. Plaza-Bolanos , and J. L. Martinez-Vidal . 2007 . Multiresidue analysis of pesticides in animal liver by gas chromatography using triple quadrupole tandem mass spectrometry . J. Chromatogr. A 1153 : 194 – 202 .
  • Garrido-Frenich , A. , R. Romero-Gonzalez , J. L. Martinez-Vidal , P. Plaza-Bolanos , L. Cuadros-Rodriguez , and M. A. Herrera-Abdo . 2006 . Characterization of recovery profiles using gas chromatography-triple quadrupole mass spectrometry for the determination of pesticide residues in meat samples . J. Chromatogr. A 1133 : 315 – 321 .
  • Gelsomino , A. B. , B. Petrovicova , S. Tiburtini , E. Magnani , and M. Felici . 1997 . Determination of organochlorine pesticides in water by microwave assisted-headspace/hollow fiber liquid-phase microextraction/gas chromatography/tandem mass spectrometer . J. Chromatogr. A 782 ( 1 ): 105 – 122 .
  • Jongenotter , G. A. , M. A. T. Kerkhoff , H. C. M. Van der Knaap , and B. G. M. Vandeginste . 1997 . Automated on-line GPC-GC-FPD involving co-solvent trapping and the on-column interface for the determination of morganophosphorus pesticides in olive oils . J. High Res. Chromatogr. 22 : 17 – 23 .
  • Khalid , I. S. , and E. M. A. M. Alaa . 2008 . Organochlorine pesticide residues in camel, cattle and sheep carcasses slaughtered in Sharkia Province . Egypt Food Chem. 108 : 154 – 164 .
  • Kuivinen , J. , and S. Bengtsson . 2002 . Solid-phase extraction and cleanup of organophosphorus pesticide residues in bovine muscle with gas chromatographic detection . J. Chromatogr. Sci. 40 : 392 .
  • Le Faouder , J. , E. Bichon , P. Brunschwig , R. Landelle , F. Andre , and B. Le Bizec . 2007 . Transfer assessment of fipronil residues from feed to cow milk . Talanta. 73 : 710 – 717 .
  • Lehotay , S. J. , and K. Maotovska . 2005 . Evaluation of two fast and easy methods for pesticide residue analysis in fatty food matrixes . J. AOAC Int. 88 : 2 – 2 .
  • Liapis , K. , S. N. Kolokouri , M. A. Koupparis , and G. E. Miliadis . 2010 . A system suitability test for LC-TOF MS instruments and a validation of a method using high resolution/high mass accuracy LC-TOF MS system for pesticides residue analysis. European Pesticide Residue Workshop 2010, Strasbourg: Commun des Laboratoires du MINEFE Laboratoire de Strasbourg, p. 48.
  • Long , A. R. , M. M. Soliman , and S. A. Barker . 1991 . Matrix solid phase dispersion (MSPD) extraction and gas chromatographic screening of nine chlorinated pesticides in beef fat . J. Assoc. Off. Anal. Chem. 74 : 493 – 496 .
  • McNaught , A. D. , and A. Wilkinson . 1997 . IUPAC Compendium of Chemical Terminology: The Gold Book, , 2nd Ed. Blackwell Science Ltd . http://old.iupac.org/goldbook/M03759.pdf
  • Ministry of Rural Development, and Food . 2013 . List of Authorized Plant Protection Products & Biocides by Category or Active Substance . http://wwww.minagric.gr/syspest/syspest_menu_eng.aspx
  • Pagliuca , G. , T. Gazzotti , E. Zironi , and P. Sticca . 2005 . Residue analysis of organophosphorus pesticides in animal matrices by dual column capillary gas chromatography with nitrogen–phosphorus detection . J. Chromatogr. A 1071 : 67 – 70 .
  • Payá , P. , M. Anastassiades , D. Mack , I. Sigalova , B. Tasdelen , J. Oliva , and A. Barba . 2007 . Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection . Anal. Bioanal. Chem. 389 : 1697 – 1714 .
  • Romero-González , R. , F. A. Garrido , J. L. Martínez Vidal , O. D. Prestes , and S. L. Grio . 2011. Simultaneous determination of pesticides, biopesticides and mycotoxins in organic products applying a quick, easy, cheap, effective, rugged and safe extraction procedure and ultra-high performance liquid chromatography–tandem mass spectrometry. J. Chromatogr. A 1218: 1477–1485.
  • Schenck , F. J. , and D. J. Donoghue . 2000 . Determination of organochlorine and organophosphorus pesticide residues in eggs using a solid phase extraction clean-up . J. Agric. Food Chem. 48 : 6412 – 6415 .
  • Trufelli , H. , P. Palma , G. Famiglini , and A. Cappiello . 2011 . An overview of matrix effects in liquid chromatography–mass spectrometry . Mass Spectrom. Rev. 30 : 491 – 509 .
  • Tsiplakou , E. , C. J. Anagnostopoulos , K. Liapis , S. A. Haroutounian , and G. Zervas . 2010 . Pesticides residues in milks and feedstuff of farm animals drawn from Greece . Chemosphere 80 ( 5 ): 504 – 512 .
  • Van Drooge , B. , M. Rafael , I. Vives , I. Cardiel , and R. Guitart . 2007 . Organochlorine residue levels in livers of birds of prey from Spain: Inter-species comparison in relation with diet and migratory patterns . Environ. Pollut. 153 ( 1 ): 13 – 24 .
  • Vreuls , J. J. , R. J. J. Swen , V. P. Goudriaan , M. A. T. Kerkhoff , G. A. Jongenotter , and U. A. Th. Brinkman . 1996 . Automated on-line gel permeation chromatography-gas chromatography for the determination of organophosphorus pesticides in olive oil . J. Chromatogr. A 750 : 275 .
  • Walters , S. M. 1990 . Clean-up techniques for pesticides in fatty foods . Anal. Chim. Acta 236 : 77 – 82 .

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