355
Views
6
CrossRef citations to date
0
Altmetric
Original Articles

Microwave Digestion for Colorimetric Determination of Total Si in Plant and Mineral Samples

, , , , & ORCID Icon
Pages 840-847 | Received 12 Feb 2015, Accepted 05 Dec 2017, Published online: 08 Feb 2018

References

  • Biel, K. Y., V. V. Matichenkov, and I. R. Fomina. 2008. Protective role of silicon in living systems. In Functional foods for chronic diseases: Advances in the development of functional foods, ed D. M. Martirosyan, Vol. 3, 208–31. Richardson, Texas, USA: Copyright © by D&A Inc.
  • Bocharnikova, E. A., and V. V. Matichenkov. 2014. Silicon fertilizers: Agricultural and environmental impacts. In Fertilizers: Components, uses in agriculture and environmental impacts, ed F. Lopez-Valdez, and F. Fernandez-Luqueno, 183–98. N.Y.: Nova Sci. Publishers.
  • Bunting, W. E. 1944. The determination of soluble silica in very low concentration. Industrial and Engineering Chemistry Analysis Ed 16:612–15. doi:10.1021/i560134a006.
  • Eaton, A. D., L. S. Clesceri, and A. E. Greenberg. 1995. Standard methods for the examination of water and wastewater, 19th ed. Washington, DC: American Public Health Assn.
  • Elliot, C. L., and G. H. Snyder. 1991. Autoclave-induced digestion for the colorimetric determination of silicon in rice straw. Journal of Agricultural and Food Chemistry 39:1118–19. doi:10.1021/jf00006a024.
  • Epstein, E. 1994. The anomaly of silicon in plant biology. Proceedings of the National Academic Sciences USA 91:11–17. doi:10.1073/pnas.91.1.11.
  • Epstein, E. 1999. Silicon. Annual Review of Plant Physiology and Plant Molecular Biology 50:641–64. doi:10.1146/annurev.arplant.50.1.641.
  • Epstein, E. 2009. Silicon: Its manifold roles in plants. Annals of Applied Biology 155:155–60. doi:10.1111/j.1744-7348.2009.00343.x.
  • Formento, M. L., S. Spadacini, and R. T. Ceserani. 1994. Flameless atomic-adsorption spectrometry after acid microwave digestion – A precise and sensitive method for determination of ruthenium in biological samples. Analysis 22:158.
  • Hallmark, C. T., L. P. Wilding, and N. E. Smeck. 1982. Silicon in methods of soil analysis. In Part 2: Chemical and microbiological properties, eds. D. R. Keeney, and D. W. Nelson, 263–74. Madison, Wisc.: ASA.
  • Haysom, M. B., and Z. A. Ostatek-Boczynski. 2006. Rapid, wet oxidation procedure for the estimation of silicon in plant tissue. Communications in Soil Science and Plant Analysis 37 (15–20):2299–306. doi:10.1080/00103620600819420.
  • Iler, R. K. 1979. The Chemistry of Silica. New York: Wiley.
  • Kraska, J. E., and G. A. Breitenbeck. 2010. Simple, robust method for quantifying silicon in plant tissue. Communications in Soil Science and Plant Analysis 41 (17):2075–85. doi:10.1080/00103624.2010.498537.
  • Krushevska, A., R. M. Barnes, and C. Amarasiriwaradena. 1993. Decomposition of biological samples for inductively coupled plasma atomic emission spectrometry using an open focused microwave digestion system. The Analyst 118:1175. doi:10.1039/an9931801175.
  • Krushevska, A. P., and R. M. Barnes. 1994. Determination of low silicon concentrations in food and coral soil by inductively coupled plasma atomic emission spectrometry. Journal of Analytical Atomic Spectrometry 9:981–84. doi:10.1039/ja9940900981.
  • Lajunen, L. H. J., J. Piispanen, and E. Saari. 1992. Microwave dissolution of plant samples for AAS analysis. Atomic Spectroscopy 13:127.
  • Le Blond, J. S., S. Strekopytov, C. Unsworth, and B. J. Williamson. 2011. Testing a new method for quantifying Si in silica-rich biomass using HF in a closed vessel microwave digestion system. Analysis Methods 3:1752–58. doi:10.1039/c1ay05144j.
  • Liu, N., U. Jorgensen, and P. E. Laerke. 2013. Quality determination of biomass for combustion: A new high-throughput microwave digestion method prior to elemental analysis by inductively coupled plasma-optical emission spectroscopy. Energy & Fuels: An American Chemical Society Journal 27:7485–88. doi:10.1021/ef4016747.
  • Mager, W., F. Krikowa, D. Wruck, H. Louie, T. Nguyen, and W. Y. Huang. 2002. Determination of total phosphorus and nitrogen in turbid waters by oxidation with alkaline potassium peroxodisulfate and low pressure microwave digestion, autoclave heating or the use closed vessels in a hot water bath: Comparison with Kjeldahl digestion. Analytical Chimica Acta 463:283–93. doi:10.1016/S0003-2670(02)00346-X.
  • Matichenkov, V. V. 2007. Soil gradation on the plant-available Si. Agrochemistry [Rus] 7:22–30.
  • Mullin, J. B., and J. P. Riley. 1955. The colorimetric determination of silicate with special reference to sea and natural waters. Analytica Chimica Acta 12:162–76. doi:10.1016/S0003-2670(00)87825-3.
  • Pougnet, M. A. B., N. G. Schnautz, and A. M. Walker. 1992. Development and application of a microwave digestion pressure vessel. South African Journal of Chemistry 25:86.
  • Rimmelin-Maury, P., T. Moutin, and B. Queguiner. 2007. A new method for nanomolar determination of silicic acid in seawater. Analytica Chimica Acta 587:281–86. doi:10.1016/j.aca.2007.01.055.
  • Shimizu, M. 2001. Silicon(IV) Fluoride. In Encyclopedia of reagents for organic synthesis, eds. A. S. Rao, and H. R. Mohan. John Wiley & Sons.
  • Snyder, G. H. 2001. Methods for silicon analysis in plant, soil, and fertilizers. In Silicon in agriculture. Studies in plant science, ed L. E. Datnoff, G. H. Snyder, and G. H. Korndorfer, 185–96. 8 ed. Amsterdam: Elsevier.
  • Snyder, G. H., V. V. Matichenkov, and L. Datnoff. 2006. Silicon. In Handbook of plant nutrition, eds. A. V. Barker, and D. J. Pilbeam, 551–68. Massachusetts University.
  • Taber, H. G., D. Shogren, and G. Lu. 2002. Extraction of silicon from plant tissue with dilute HCl and HF and measurement by modified inductive coupled argon plasma procedures. Communications in Soil Science and Plant Analysis 33 (9–10):1661–70. doi:10.1081/CSS-120004306.
  • van der Vorm, P. D. J. 1987. Dry ashing of plant material and dissolution of the ash in HF for the colorimetric determination of silicon. Communications in Soil Science and Plant Analysis 18 (11):1181–89. doi:10.1080/00103628709367893.
  • Wilson, M. A., R. Burt, W. C. Lynn, and L. C. Klameth. 1997. Total elemental analysis digestion method evaluation on soils and clays. Communications in Soil Science and Plant Analysis 28:407–26. doi:10.1080/00103629709369800.
  • Yoshida, S., D. A. Forno, J. H. Cock, and K. A. Gomez. 1976. Laboratory manual for physiological studies of rice, 3rd ed. Los Banos, Laguna, Philippines: Interactional Rice Research Institute.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.