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OPPI BRIEFS

PREPARATION OF 5,10,11,11a-TETRAHYDRO-1H, 3H-THIAZOLO[2,3-c]-AND 5,10,11,11a-TETRAHYDRO-1H, 3H-THIAZOLO[4,3-c]-[1,4]BENZODIAZEPINES

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Pages 652-655 | Received 09 Apr 2002, Published online: 11 Feb 2009

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  • The enantiomeric purity was determined by 1H NMR with (+)-(S)-2,2,2-trifluoro-1-(9-anthryl)-ethanol as a chiral solvent. The corresponding (R)-enantiomer had ‘α’20 D-113.8° (c 0.488, CH2Cl2

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