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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 15
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Original Articles

Synthesis of Quadruply Carbon-13 Labeled Tetramethyltetrathiaful Valene

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Pages 2677-2685 | Received 19 Oct 1999, Published online: 16 Feb 2011

References

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  • Chlorotrimethylsilane (250 mL) was heated with water (1 mL) to reflux until the evaporation of HCl stopped. After addition of calcium hydride, the mixture was heated to reflux for one hour and then distilled
  • Sodium dispersion (Aldrich, 40 wt % in mineral spirits) was washed in a Schlenk flask with dry hexanes (3 × 60 mL) and dry ether (2 × 60 mL), dried in vacuo and stored in a drybox

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