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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 2, 1972 - Issue 4
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Original Articles

Curtius Degradation Utilizing Trimethylsilyl Azide. A facile isocyanate synthesis

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Pages 227-230 | Received 23 May 1972, Published online: 26 Jan 2007

References

  • Washburne , S. S. , Peterson , W. R. Jr. and Berman , D. A. in press . J. Org. Chem. ,
  • Cason , J. 1955 . Org. Syn., Coll. Vol. , 3 : 169
  • Washburne , S. S. and Peterson , W. R. Jr. 1971 . J. Organometal. Chem. , 33 : 153
  • All compounds prepared in this study gave satisfactory elemental and spectral analyses
  • Hunphlett , W. J. and Wilson , C. V. 1961 . J. Org. Chem. , 26 : 2507
  • Siefken , W. 1949 . Ann. , 562 : 75
  • It: 2945, 2910, 2850, 2260, 1643, 1462, 1355, and 720 cm−1. Nmr: 0 0.90 (3H, t), 1.28 (14K, m), 2.05 (4H, m), 2.75 (2K, t), 3.21 (2H, t), and 5.30 (4H, t)
  • Zbiral , E. and Nestler , G. 1970 . Tetrahedron , 26 : 2945
  • Ulrich , H. , Tucker , E. and Sayigh , A. A. R. 1967 . J. Org. Chem. , 32 : 4052
  • Smith , P. A. S. 1946 . Org. Reactions , 3 : 337
  • Identical with an authentic sample from Aldrich Chemical Co.

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