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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 3, 1973 - Issue 6
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Original Articles

A Facile Synthesis of 5-(2′-Oxoalkyl)-2-Cyclopenten-1-Ones

Pages 441-445 | Received 02 Nov 1973, Published online: 05 Dec 2006

References

  • Plattner , P. A. and Pfau , A. St. 1937 . Helv. Chim. Acta , 20 : 1474 M. Mousseron, R. Richaud, and R. Granger, Bull. Soc. Chim. Fr., 625 (1946); R. L. Frank, R. Armstrong, J. Kwiatek, and H. A. Price, J. Amer. Chem. Soc., 70, 1379 (1948); M. Vandewalle and F. Compernolle, Bull. Soc. Chim. Belges., 76, 43 (1967); J. Grimaldi and M. Bertrand, Tetrahedron Lett., 3269 (1969); J. Grimaldi and M. Bertrand, Bull. Soc. Chim. Fr., 957 (1971); W. C. Agosta and A. B. Smith, III, J. Amer. Chem., Soc., 93, 5513 (1971)
  • Chiusoli , G. P. , Dubini , M. , Ferraris , M. , Guerrieri , F. , Merzoni , S. and Mondelli . 1968 . J. Chem. Soc.(c) , : 2889 In a preparation of methyl hexa-2,5-dienoate, 2-oxo-cyclopent-3-enylacetate and 4-oxo-5-(2-oxocyclopent-3-enyl) valerate were obtained in low yields as by-products []
  • Bobbitt , J. M. and K.-P. , Segebarth . Cyclopentanoid Terpene Derivatives Edited by: Taylor , W. I. and Battersby , A. R. Vol. 1969 , New York, N. Y. : Marcel Dekker, Inc. . Chapter 1
  • Depuy , C. H. , Isaks , M. , Eilers , K. L. and Morris , G. F. 1964 . J. Org. Chem. , 29 : 3503
  • Satisfactory ir, nmr and high resolution mass spectra were obtained for all the products
  • All yields quoted are for isolated compounds. No attempt has been made to optimize yields
  • Attempted purification of this material by either distillation or column chromatography resulted in its partial decomposition to give 7

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