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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 4, 1974 - Issue 1
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Original Articles

Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol

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Pages 61-62 | Received 28 Jan 1974, Published online: 05 Dec 2006

References

  • Hydrochloric acid and trimethylchlorosilane were used
  • Larson , G. L. and Hernandez , A. 1973 . J. Org. Chem. , 38 : 3935
  • Carbon tetrachloride, chloroform, methylene chloride, benzene and tetrahydrofuran were used
  • The ketone precurser to the trimethylsilyl enol ether
  • Isolated yield of the hemithio ketal. All compounds showed satisfactory ir and pmr spectra and glc traces
  • Djerassi , C. and Gorman , M. 1953 . J. Amer. Chem. Soc. , 75 : 3704
  • Wilson , G. E. Jr. , Huang , M. G. and Schloman , W. W. Jr. 1968 . J. Org. Chem. , 33 : 2133

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